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http://dx.doi.org/10.13103/JFHS.2017.32.2.141

Determination of Carbendazim in Commercial Agricultural Products by LC-MS/MS  

Hwang, Lae-Hwong (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Lee, Sung-Deuk (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Kim, Jeong-Gon (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Kim, Ji-Young (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Park, So-Hyun (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Kim, Ji-Hae (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Park, Jung-Hyun (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Han, Chang-Ho (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Kim, Mu-Sang (Seoul Metropolitan Government Research Institute of Public Health and Environment)
Publication Information
Journal of Food Hygiene and Safety / v.32, no.2, 2017 , pp. 141-146 More about this Journal
Abstract
A rapid and precise method using LC-MS/MS was developed for carbendazim analysis in agricultural products. This compound was extracted with acetonitrile from agricultural products and cleaned up by solid-phase extraction procedure. The limit of detection and quantification were 0.001 mg/kg and 0.004 mg/kg, respectively. The mean recoveries and precision from 4 agricultural products, soybean sprout and mungbean sprout were in the range of 83.3-86.4% and 0.2-3.0% spiked at 1.0 mg/kg and those were in the range of 77.3-90.1% and 1.3-3.8% spiked at 0.02 mg/kg. The present method is faster and more precise compared with the multi-residue method of Korean Food Code. Therefore, we conclude that this method is suitable for carbendazim determination in a wide range of agricultural products.
Keywords
Carbendazim; Pesticide; LC-MS/MS; Agricultural products;
Citations & Related Records
Times Cited By KSCI : 4  (Citation Analysis)
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