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http://dx.doi.org/10.9721/KJFST.2015.47.3.321

Optimization of Calcium Acetate Preparation from Littleneck Clam (Ruditapes philippinarum) Shell Powder and Its Properties  

Park, Sung Hwan (Department of Food and Nutrition, Gyeongsang National University)
Jang, Soo Jeong (Nutrition Education Major/Graduate School of Education, Gyeongsang National University)
Lee, Hyun Ji (Department of Food and Nutrition, Gyeongsang National University)
Lee, Gyoon-Woo (Department of Food and Nutrition, Gyeongsang National University)
Lee, Jun Kyu (Department of Seafood Science and Technology, Gyeongsang National University)
Kim, Yong Jung (Department of Seafood Science and Technology, Gyeongsang National University)
Kim, Jin-Soo (Department of Seafood Science and Technology, Gyeongsang National University)
Heu, Min Soo (Department of Food and Nutrition, Gyeongsang National University)
Publication Information
Korean Journal of Food Science and Technology / v.47, no.3, 2015 , pp. 321-327 More about this Journal
Abstract
The optimal condition for preparation of powdered calcium acetate (LCCA) which has high solubility, from calcined powder (LCCP) of the littleneck clam shell by response surface methodology (RSM) was examined. Increased molar ratio of LCCP led to reduced solubility, yield, color values, and overall quality. The critical values of multiple response optimization of independent variables were 2.57 M of acetic acid and 1.57 M of LCCP. The actual values (pH 7.0, 96.1% for solubility, and 220.9% for yield) under the optimized condition were similar to the predicted values. LCCA showed strong buffering capacity between pH 4.89 and 4.92 on addition of ~2 mL of 1 N HCl. The calcium content and solubility of LCCA were 21.9-23.0 g/100 g and 96.1-100.1%, respectively. The FT-IR and XRD patterns of LCCA were identified as calcium acetate monohydrate, and FESEM images revealed an irregular and rod-like microstructure.
Keywords
littleneck clam; shellfish; calcined powder; calcium acetate; X-ray diffraction;
Citations & Related Records
Times Cited By KSCI : 3  (Citation Analysis)
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