DOI QR코드

DOI QR Code

Study on the Manufacturing Process and Characterization of Polyimide Non-woven Filter

Polyimide fiber를 이용한 PI 부직포 필터 제조 및 특성 연구

  • Received : 2022.02.08
  • Accepted : 2022.04.24
  • Published : 2022.04.30

Abstract

In this study, Polyimide (PI) fiber and non-woven fabric were fabricated for the manufacture of PI fiber high-temperature filter. The PI fiber was fabricated in two steps, and poly(amic acid) (PAA) could be manufactured by polymerizing 4,4'-oxydianiline (ODA) as an aromatic amine-based monomer and pyromellitic dianhydride (PMDA) as a solvent with N,N-dimethylacetamide (DMAc). PAA fibers were fabricated by wet spinning, PI fibers were manufactured by imidizing PAA fibers, and the properties of non-woven fabrics were investigated. To confirm the degree of imidization, various tests such as FT-IR analysis and shrinkage, heat resistance, deterioration analysis, maximum operating temperature, chemical resistance and dust collection efficiency were also performed.

Keywords

Acknowledgement

본 연구는 산업통상자원부 산업소재핵심기술개발사업(섬유의류) "사용 온도 240 ℃ 이상 고내열성 폴리이미드계 슈퍼 섬유 및 이를 적용한 내열 필터 개발" (과제번호: 10077584) 과제 지원으로 수행되었습니다.

References

  1. G. W. Meyer, S. J. Pak, Y. J. Lee, and J. E. McGrath, "New High-performance Thermosetting Polymer Matrix Material Systems", J. Polym., 1995, 36, 2303-2309. https://doi.org/10.1016/0032-3861(95)95311-N
  2. J.-H. Chang, K. M. Park, S.-M. Lee, and J. B. Oh, "Two-step Thermal Conversion from Poly(amic acid) to Polybenzoxazole via Polyimide: Their Thermal and Mechanical Properties", J. Polym. Sci., Part B: Polym. Phys., 2000, 38, 2537-2545. https://doi.org/10.1002/1099-0488(20001001)38:19<2537::AID-POLB50>3.0.CO;2-V
  3. X. Fang, Z. Wang, Z. Yang, L. Gao, Q. Li, and M. Ding, "Novel Polyimides Derived from 2,3,3',4'-Benzophenonetetracarboxylic Dianhydride", J. Polym., 2003, 44, 2641-2646. https://doi.org/10.1016/S0032-3861(03)00181-2
  4. K. S. Yang, D. D. Edie, D. Y. Lim, Y. M. Kim, and Y. O. Choi, "Preparation of Carbon Fiber Web from Electrostatic Spinning of PMDA-ODA Poly(amic acid) Solution", J. Carbon, 2003, 41, 2039-2046. https://doi.org/10.1016/S0008-6223(03)00174-X
  5. H. Li, J. Liu, K. Wang, L. Fan, and S. Yang, "Synthesis and Characterization of Novel Fluorinated Polyimides Derived from 4,40-[2,2,2-trifluoro-1-(3,5-ditrifluoromethylphenyl) ethylidene]diphthalic Anhydride and Aromatic Diamines", J. Polym., 2006, 47, 1443-1450. https://doi.org/10.1016/j.polymer.2005.12.074
  6. X.-L. Wang, Y.-F. Li, C.-L. Gong, T. Ma, and F.-C. Yang, "Synthesis and Properties of New Pyridine-bridged Poly(ether-imide)s Based on 4-(4-trifluoromethylphenyl)-2,6-bis[4-(4-aminophenoxy)phenyl]pyridine", J. Fluorine Chem., 2008, 129, 56-63. https://doi.org/10.1016/j.jfluchem.2007.08.014
  7. D.-J. Liaw, C.-C. Huang, and W.-H. Chen, "Color Lightness and Highly Organosoluble Fluorinated Polyamides, Polyimides and Poly(amide-imide)s Based on Noncoplanar 2,2'-dimethyl4,4'-biphenylene Units", J. Polym., 2006, 47, 2337-2348. https://doi.org/10.1016/j.polymer.2006.01.028
  8. S. K. Park and R. J. Farris, "Dry-jet Wet Spinning of Aromatic Polyamic Acid Fiber Using Chemical Imidization", J. Polym., 2001, 42, 10087-10093. https://doi.org/10.1016/S0032-3861(01)00576-6
  9. J. Yin, Y.-F. Ye, L. Li, Y.-L. Zhang, Y. Huang, and Z.-G. Wang, "Study on the Preparation and Properties of Copolyimides Based on Hexafluoroisopropylidene Bis(3,4-phthalic anhydride) and 1,12-di(4-aminophenoxy)dodecane", Eur. Polym. J., 1999, 35, 1367-1373. https://doi.org/10.1016/S0014-3057(98)00203-1
  10. Q. H. Zhang, M. Dai, M. X. Ding, D. J. Chen, and L. X. Gao, "Mechanical Properties of BPDA-ODA Polyimide Fibers", Eur. Polym. J., 2004, 40, 2487-2493. https://doi.org/10.1016/j.eurpolymj.2004.06.020
  11. W. M. Edwards, U.S. Patent, 3,179,614 (1965).
  12. R. S. Irwin, U.S. Patent, 3,415,782 (1968).
  13. T. E. Snkhanova, Y. G. Baklagina, V. V. Kudryavtsev, A. Maricheva, and F. Lednicky, "Morphology, Deformation and Failure Behaviour of Homo- and Copolyimide Fibres: 1. Fibres from 4,4'-oxybis(phthalic anhydride) (DPhO) and p-phenylenediamine (PPh) or/and 2,5-bis(4-aminophenyl)-pyrimidine (2,5PRM)", J. Polym., 1999, 40, 6265-6276. https://doi.org/10.1016/S0032-3861(99)00039-7
  14. T. Kaneda, T. Katsur, K. Nakagawa, H. Makino, and M. Horio, "High-strength-high-modulus Polyimide Fibers I. One-Step Synthesis of Spinnable Polyimides", J. Appl. Polym., 1986, 32, 3133-3149. https://doi.org/10.1002/app.1986.070320121
  15. K. Nagaoka, U.S. Patent, 4,448,957 (1984).
  16. C. H. Ju, J. C. Kim, and J. H. Chang, "Synthesis and Characterization of Colorless Polyimide Nanocomposite Films", J. Appl. Polym. Sci., 2007, 106, 4192-4201. https://doi.org/10.1002/app.26987
  17. H. S. Jin, J. C. Kim, and J. H. Chang, "Synthesis and Characterization of Colorless Polyimide Nanocomposite Films Containing Pendant Trifluoromethyl Groups", Macromol. Res., 2008, 16, 503-509. https://doi.org/10.1007/BF03218551
  18. F. Chen, X. Peng, T. Li, S. Chen, X.-F. Wu, D. H. Reneker, and H. Hou, "Mechanical Characterization of Single High-strength Electrospun Polyimide Nanofibres", J. Phys. D: Appl. Phys., 2008, 41, 025308. https://doi.org/10.1088/0022-3727/41/2/025308
  19. R. S. Irwin and W. Sweeny, "Polyimide Fibers", J. Polym. Sci., 1967, 19, 41-48.
  20. H. B. Xiang, Z. Huang, L. Q. Liu, L. Chen, J. Zhu, Z. M. Hu, and J. R. Yu, "Structure and Properties of Polyimide (BTDATDI/MDI co-polyimide) Fibers Obtained by Wet-spinning", Macromol. Res., 2011, 19, 645-653. https://doi.org/10.1007/s13233-011-0709-z
  21. W. Xu, Y. Su, M. Shang, X. Lu, and Q. Lu, "Rapid Synthesis of Polyimide Precursors by Solution Polymerization Using Continuous-flow Microreactors", Chem. Eng. J., 2020, 397, 125361. https://doi.org/10.1016/j.cej.2020.125361
  22. K. Kim and M. Ree, "Isomeric Compositions in Amide Acids and Poly(amic acid)s Derived from 1-(Trifluoromethyl)-2,3,5,6-Benzenetetracarboxylic Dianhydride", J. Polym. Sci., 1998, 36, 1755-1765. https://doi.org/10.1002/(SICI)1099-0518(199808)36:11<1755::AID-POLA8>3.0.CO;2-Q
  23. J. H. Chang and K. M. Park, "Thermal Cyclization of the Poly(amic acid): Thermal, Mechanical, and Morphological Properties", Eur. Polym. J., 2000, 36, 2185-2191. https://doi.org/10.1016/S0014-3057(99)00280-3
  24. X. Zeng, J. Hu, J. Zhao, Y. Hang, and D. Pan, "Investigating the Jet Stretch in the Wet Spinning of PAN Fiber", J. Appl. Polym., 2007, 106, 2267-2273. https://doi.org/10.1002/app.26929