Journal of Hydrogen and New Energy (한국수소및신에너지학회논문집)

The Korean Hydrogen and New Energy Society (한국수소및신에너지학회)
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Evaluation of Polymer Glass Transition Temperature Using HP-DSC in Hydrogen Atmosphere

수소 환경하에서의 고압시차주사 열량계를 이용한 고분자재료의 유리전이온도 평가

  • KIM, DAEHO (Korea Research Institute of Standards and Science) ;
  • LEE, SANGHYUN (Korea Research Institute of Standards and Science)
  • Received : 2021.04.19
  • Accepted : 2021.04.27
  • Published : 2021.04.28
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Abstract

Evaluation of the thermal properties of a polymer is important for application of hydrogen infrastructure. This study describes the process of measurement of the glass transition temperature using high-pressure differential scanning calorimeter (HP-DSC) in hydrogen condition. Pressure stability of HP-DSC was evaluated up to 8 MPa in hydrogen gas and temperature calibration was carried out in the range from -92℃ to 232℃ using the reference materials. Glass transition temperature of commercial EPDM polymer was measurued at 0.2, 2, 3, 5 MPa in hydrogen condition.

Keywords

Acknowledgement

본 연구는 한국표준과학연구원 '수소스테이션 신뢰성 평가기술 개발(21011088)' 과제의 지원을 받아 진행되었습니다.

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