DOI QR코드

DOI QR Code

Advanced Methodologies for Manipulating Nanoscale Features in Focused Ion Beam

  • Kim, Yang-Hee (Advanced Analysis Center, Korea Institute of Science and Technology (KIST)) ;
  • Seo, Jong-Hyun (Advanced Analysis Center, Korea Institute of Science and Technology (KIST)) ;
  • Lee, Ji Yeong (Advanced Analysis Center, Korea Institute of Science and Technology (KIST)) ;
  • Ahn, Jae-Pyoung (Advanced Analysis Center, Korea Institute of Science and Technology (KIST))
  • Received : 2015.12.03
  • Accepted : 2015.12.10
  • Published : 2015.12.30

Abstract

Nanomanipulators installed in focused ion beam (FIB), which is used in the lift-out of lamella when preparing transmission electron microscopy specimens, have recently been employed for electrical resistance measurements, tensile and compression tests, and in situ reactions. During the pick-up process of a single nanowire (NW), there are crucial problems such as Pt, C and Ga contaminations, damage by ion beam, and adhesion force by electrostatic attraction and residual solvent. On the other hand, many empirical techniques should be considered for successful pick-up process, because NWs have the diverse size, shape, and angle on the growth substrate. The most important one in the in-situ precedence, therefore, is to select the optimum pick-up process of a single NW. Here we provide the advanced methodologies when manipulating NWs for in-situ mechanical and electrical measurements in FIB.

Keywords

References

  1. Chou C Y, Seo J H, Hao Y H, Ahn J P, Paek E, Cho M H, Choi I S, and Hwang G S (2015) Anomalous stagewise lithiation of gold-coated silicon nanowires: a combined in situ characterization and firstprinciples study. ACS Appl. Mater. Interfaces. 7, 46976-16983.
  2. Giannuzzi L A, Drown J L, Brown S R, Irwin R B, and Stevie F A (1998) Applications of the FIB lift-out technique for TEM specimen preparation. Microscopy Res. Tech. 41, 285-290. https://doi.org/10.1002/(SICI)1097-0029(19980515)41:4<285::AID-JEMT1>3.0.CO;2-Q
  3. Hoffmann S, Ostlund F, Michler J, Fan H J, Zacharias M, Christiansen S H, and Ballif C (2007) Fracture strength and Young's modulus of ZnO nanowires. Nanotechnology 18, 205503. https://doi.org/10.1088/0957-4484/18/20/205503
  4. Jung M S, Seo J H, Moon M W, Choi J W, Joo Y C, and Choi I S (2015) A bendable Li- ion battery with a nano-hairy electrode direct integration scheme on the polymer substrate. Adv. Energy Mater. 5, 1400611. https://doi.org/10.1002/aenm.201400611
  5. Kristian M, Thomas W, Axel K, and Peter B (2006) Pick-and-place nanomanipulation using microfabricated grippers. Nanotechnology 17, 2434-2441. https://doi.org/10.1088/0957-4484/17/10/002
  6. Roh J H, You Y H, Ahn J P, and Hwang J (2012) Electrical characterization of electronic materials using FIB-assisted nanomanipulators. Appl. Micro. 4, 223-227.
  7. Schilling A, Adams T, Bowman R M, and Gregg J M (2007) Strategies for gallium removal after focused ion beam patterning of ferroelectric oxide nanostructures. Nanotechnology 18, 035301. https://doi.org/10.1088/0957-4484/18/3/035301
  8. Seo J H, Chou C Y, Tsai Y H, Cho Y, Seong T Y, Lee W J, Cho M H, Ahn J P, Hwang G S, and Choi I S (2015) Ultrafast chemical lithiation of single crystalline silicon nanowires: in situ characterization and fi rst principles modeling. RSC Adv. 5, 17438-17443. https://doi.org/10.1039/C4RA14953J
  9. Seo J H, Park H S, Yoo Y, Seong T Y, Li J, Ahn J P, Kim B, and Choi I S (2013) Origin of size dependency in coherent-twin-propagation-mediated tensile deformation of noble metal nanowires. Nano Lett. 13, 5112-5116. https://doi.org/10.1021/nl402282n
  10. Seo J H, Yoo Y, Park N Y, Yoon S W, Lee H, Han S, Lee S W, Seong T Y, Lee S C, Lee K B, Cha P R, Park H S, Kim B S, and Ahn J P (2011) Superplastic deformation of defect-free Au nanowires via coherent twin propagation. Nano Lett. 11, 3499-3502. https://doi.org/10.1021/nl2022306
  11. Yoon H, Kim S, Lee S, In J, Kim J, Ryoo H, Noh J H, Ahn J P, Jo Y, Choo J, and Kim B (2013) Three-dimensionally kinked high-conduction CoGe nanowire growth induced by rotational twinning. J. Mater. Chem. C 1, 6259-6264. https://doi.org/10.1039/c3tc31214c
  12. Yoon S W, Seo J H, Seong T Y, Kwon H, Lee K B, and Ahn J P (2012) Effects of Pt junction on electrical transport of individual ZnO nanorod device fabricated by focused ion beam. J. Nanosci. Nanotech. 12, 1466-1470. https://doi.org/10.1166/jnn.2012.4696