한국세라믹학회지 (Journal of the Korean Ceramic Society)

  • 제49권4호
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  • Pages.287-294
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  • 2012
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  • 1229-7801(pISSN)
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  • 2234-0491(eISSN)
한국세라믹학회 (The Korean Ceramic Society)
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Carbon Fiber Reinforced Ceramics based on Reactive Melt Infiltration Processes

  • 투고 : 2012.05.22
  • 심사 : 2012.07.16
  • 발행 : 2012.07.31
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초록

Ceramic Matrix Composites (CMCs) represent a class of non-brittle refractory materials for harsh and extreme environments in aerospace and other applications. The quasi-ductility of these structural materials depends on the quality of the interface between the matrix and the fiber surface. In this study, a manufacture route is described where in contrast to most other processes no additional fiber coating is used to adjust the fiber/matrix interfaces in order to obtain damage tolerance and fracture toughness. Adapted microstructures of uncoated carbon fiber preforms were developed to permit the rapid infiltration of molten alloys and the subsequent reaction with the carbon matrix. Furthermore, any direct reaction between the melt and fibers was minimized. Using pure silicon as the reactive melt, C/SiC composites were manufactured with an aim of employing the resulting composite for friction applications. This paper describes the formation of the microstructure inside the C/C preform and resulting C/C-SiC composite, in addition to the MAX phases.

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참고문헌

  1. R. Naslain, R. Pailller, S. Jacques, G. Vignoles, and F. Langlais, "CVI : A Versatile CMC-Processing Technique Revisited," pp. 2-14 in High Temperature Ceramic Materials and Composites. Ed. by W. Krenkel and J. Lamon, AVISO Verlagsgesellschaft mbH, Berlin, 2010.
  2. R.R. Naslain, R. Pailler, X. Bourrat, S. Bertrand, F. Heurtevent, P. Dupel, and F. Lamouroux, "Synthesis of Highly Tailored Ceramic Matrix Composites by Pressure-pulsed CVI," Solid State Ionics, 141-142 541-8 (2001). https://doi.org/10.1016/S0167-2738(01)00743-3
  3. M. Leuchs, "Chemical Vapor Infiltration Processes for Ceramic Matrix Composites: Manufacturing, Properties, Applications," pp. 141-64 in Ceramic Matrix Composites. Ed. by W. Krenkel, Wiley-VCH Verlag GmbH & Co. KGaA., Weinheim, 2008.
  4. Z.S. Rak, "A Process for Cf/SiC Composites Using Liquid Polymer Infiltration," J. Am. Ceram. Soc., 84 [10] 2235-9 (2001).
  5. A. Durán, M. Aparicio, K. Rebstock, and W.D. Vogel, "Reinfiltration Processes for Polymer Derived Fiber Reinforced Ceramics," Key Eng. Mat., 127-131 287-94 (1997). https://doi.org/10.4028/www.scientific.net/KEM.127-131.287
  6. W. Krenkel, "Development of a Cost Efficient Process for the Manufacture of CMC Components," DLR-Research Report 2000-04 (2000).
  7. W. Krenkel, "From Polymer to Ceramics: Low Cost Manufacturing of Ceramic Matrix Composite Materials," Mol. Cryst. and Liq. Cryst., 354 353-64 (2000). https://doi.org/10.1080/10587250008023627
  8. W. Krenkel, "Carbon Fiber Reinforced CMC for High-Performance Structures," Int. J. Appl. Ceram. Technol., 1 [2] 188-200 (2004).
  9. W. Krenkel, B. Heidenreich, and R. Renz, "C/C-SiC Composites for Advanced Friction Systems," Advan. Eng. Mater., 4 [7] 427-36 (2002). https://doi.org/10.1002/1527-2648(20020717)4:7<427::AID-ADEM427>3.0.CO;2-C
  10. J. Sha, J.M. Hausherr, H. Mucha, A. Konschak, and W. Krenkel, "Microstructure Changes Caused by the Interaction of Fiber-Matrix during the Carbonization," pp. 143-48 in High Temperature Ceramic Materials and Composites. Ed. by W. Krenkel and J. Lamon, AVISO Verlagsgesellschaft mbH, Berlin, 2010.
  11. W. Krenkel, "Microstructure Tailoring of C/C-SiC Composites," Cer. Eng. Sci. Proc., 24 [4] 471-6 (2003).
  12. W. Krenkel, "Carbon Fiber Reinforced Silicon Carbide Composites (C/SiC, C/C-SiC)," pp. 117-148 in Handbook of Ceramic Composites. Ed. by N.P. Bansal, Kluwer Academic Publishers, USA, 2005.
  13. C. Devilliers and M. Krödel, "A New Technology for Lightweight and Cost Effective Space Instrument Structures and Mirrors," Proc. SPIE Europe International Symposium "Astronomical Telescopes," Glasgow, June 21-25, 2004.
  14. C. Racault, F. Langlais, R. Naslain, and Y. Kihn, "On the Chemical Vapour Deposition of $Ti_{3}SiC_{2}\;from\;TiCl_{4}-SiCl_{4}-CH_{4}-H_{2}$ Gas Mixtures," J. Mater. Sci., 29 3941-8 (1994). https://doi.org/10.1007/BF00355952
  15. Z.F. Zhang, Z.M. Sun, H. Hashimoto, and T. Abe, "Application of Pulse Discharge Sintering (PDS) Technique to Rapid Synthesis of $Ti_{3}SiC_{2}$ from Ti/Si/C Powders," J. Eur. Ceram. Soc., 22 2957-61 (2002). https://doi.org/10.1016/S0955-2219(02)00044-4
  16. N.F. Gao, Y. Miyamoto, and D. Zhang, "Dense $Ti_{3}SiC_{2}$ Prepared by Reactive HIP," J. Mater. Sci., 34 4385-92 (1999). https://doi.org/10.1023/A:1004664500254
  17. C.-S. Park, F. Zheng, S. Salamone, and R.K. Bordia, "Processing of Composites in the Ti-Si-C System," J. Mater. Sci., 36 3313-22 (2001). https://doi.org/10.1023/A:1017963109176
  18. C.-Y. Lu, X.-W. Yin, and X.-M. Li, "A Novel in-situ Synthesis Route of $Ti_{3}SiC_{2}$-SiC Composite by Liquid Silicon Infiltration," J. Inorg. Mat., 25 [9] 1003-8 (2010). https://doi.org/10.3724/SP.J.1077.2010.10041
  19. M.W. Barsoum, "The $M_{n+1}AX_{n}$ Phases: A New Class of Solids; Thermodynamically Stable Nanolaminates," Prog. Solid St. Chem., 28 201-81 (2000). https://doi.org/10.1016/S0079-6786(00)00006-6
  20. X. Yin, S. He, L. Zhang, S. Fan, L. Cheng, G. Tian, and T. Li, "Fabrication and Characterization of a Carbon Fibre Reinforced Carbon-silicon Carbide-titanium Silicon Carbide Hybrid Matrix Composite," Mat. Sci. Eng. A, 527 835-41 (2010). https://doi.org/10.1016/j.msea.2009.08.069
  21. F. Lenz and W. Krenkel, "Fabrication of Fiber Composites with a MAX Phase Matrix by Reactive Melt Infiltration," IOP Conf. Ser.: Mater. Sci. Eng., 18 2020-30 (2011) (doi:10.1088/1757-899X/18/20/202030).
  22. T. El-Raghy and M.W. Barsoum, "Processing and Mechanical Properties of $Ti_{3}SiC_{2}$: I, Reaction Path and Microstructure Evolution," J. Am. Ceram. Soc., 82 [10] 2849-54 (1999).
  23. Y. Zou, Z.M. Sun, S. Tada, and H. Hashimoto, "Effect of Al Addition on Low-temperature Synthesis of $Ti_{3}SiC_{2}$ powder," J. Alloy Compd., 461 579-84 (2008). https://doi.org/10.1016/j.jallcom.2007.07.090

피인용 문헌

  1. vol.16, pp.6, 2014, https://doi.org/10.1002/adem.201400081
  2. Influence of Thermal Fiber Pretreatment on Microstructure and Mechanical Properties of C/C-SiC with Thermoplastic Polymer-Derived Matrices vol.17, pp.8, 2015, https://doi.org/10.1002/adem.201500193
  3. vol.99, pp.5, 2016, https://doi.org/10.1111/jace.14124
  4. Fibre-reinforced multifunctional SiC matrix composite materials vol.62, pp.3, 2017, https://doi.org/10.1080/09506608.2016.1213939
  5. pp.14381656, 2017, https://doi.org/10.1002/adem.201700590
  6. Synthesis, Characterization and Thermooxidative Properties of Hybrid Block Poly(silane-b-arylacetylene) vol.1004-1005, pp.1662-8985, 2014, https://doi.org/10.4028/www.scientific.net/AMR.1004-1005.527
  7. Heat-Generating Behavior of SiC Fiber Mat Composites Embedded with Ceramic Powder for Heat Conservation vol.56, pp.6, 2012, https://doi.org/10.4191/kcers.2019.56.6.08