한국군사과학기술학회지 (Journal of the Korea Institute of Military Science and Technology)

  • 제11권2호
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  • Pages.95-100
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  • 2008
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  • 1598-9127(pISSN)
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  • 2636-0640(eISSN)
한국군사과학기술학회 (The Korea Institute of Military Science and Technology)
권호 표지

수포작용제(HD) 분석을 위한 단일방울 미세농축법 연구

Single Drop Microextraction for Analysis of Mustard Gas(HD)

  • 박양기 (국군화생방방호사령부 화학방어연구소) ;
  • 김성기 (국군화생방방호사령부 화학방어연구소) ;
  • 손병훈 (국군화생방방호사령부 화학방어연구소) ;
  • 박명주 (국군화생방방호사령부 화학방어연구소)
  • 발행 : 2008.04.30
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초록

A fast, simple, inexpensive, and reproducible sample preparation for extraction and analysis of HD in water was studied using single-drop microextraction(SDME) and GC-MS. Operation parameters, such as extraction solvent, extraction time were optimized. The optimized conditions were $1\{mu}L$ trichloroethylene and 10 min extraction time. In these conditions, about 42 times higher enrichment factor(EF) was obtained. The detection limit of HD was $1\{mu}g/L$, and the precision expressed as relative standard deviation was about 9.0%.

키워드

참고문헌

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