분석과학 (Analytical Science and Technology)

  • 제18권6호
  • /
  • Pages.520-528
  • /
  • 2005
  • /
  • 1225-0163(pISSN)
  • /
  • 2288-8985(eISSN)
한국분석과학회 (The Korean Society of Analytical Sciences)
권호 표지

Determination of trace elements in food reference materials by instrumental neutron activation analysis

  • Cho, K.H. (Korea Research Institute of Standards and Science) ;
  • Zeisler, R. (National Institute of Standards and Technology) ;
  • Park, K.W. (Korea Research Institute of Standards and Science)
  • 투고 : 2005.10.24
  • 심사 : 2005.11.11
  • 발행 : 2005.12.26
PDF 다운로드
⟨ 이전 논문 다음 논문 ⟩

초록

Two biological Certified Reference Materials (CRMs), KRISS 108-04-001 (oyster tissue) and 108-05-001 (water dropwort stem), were prepared by Korea Research Institute of Standards and Science (KRISS)during FY '01. The certified values of these materials had been determined by Isotope Dilution Mass Spectrometry (IDMS) for six elements (Cd, Cr, Cu, Fe, Pb and Zn). Additional analytical works are now progressing to certify the concentrations of a number of the environmental and nutrimental elements in these CRMs. The certified values in a CRM are usually determined by using a single primary method with confirmation by other method(s) or using two independent critically-evaluated methods. Instrumental Neutron Activation Analysis (INAA) plays an important role in the determination of certified values as it can eliminate the possibility of common error sources resulting from sample dissolution. In this study INAA procedure was used in determination of 23 elements in these two biological CRMs to acquire the concentration information and the results were compared with KRISS certified values.

키워드

참고문헌

  1. W. May, R. Paris, C. Beck, J. Fassett, R. Greenberg, F. Guenther, G. Kramer, S. Wise, T. Gills, J. Colbert, R. Gettings, and B. MacDonald; Definitions of Terms and Modes Used at NIST for Valued-Assignment of Reference Materials for Chemical Measurements, NIST Special Publication 260-136 (2000)
  2. R. R. Greenberg, R. F. Fleming, and R. Zeisler; Environm. Intern., 10, 129-136 (1984) https://doi.org/10.1016/0160-4120(84)90088-6
  3. R.R. Greenberg, E. A. Mackey, and D. A. Becker; J. Radioanal. Nucl. Chem., 193, 7-14 (1995) https://doi.org/10.1007/BF02041911
  4. E. J. Hwang, et al., Research Report KRISS/IR-2001-073, Korea Research Institute of Standards and Science, Tajeon, Korea (2001)
  5. A. Vertes, S. Nagy and Z. Klencsar(eds.); Handbook of Nuclear Chemistry, Kluwer Academic Publishers, Netherland, 3, 303-362 (2003)
  6. R. Zeisler; J. Radioanal. Nucl. Chem., 244, 507-510 (2000) https://doi.org/10.1023/A:1006722729051
  7. Guide to the Expression of Uncertainties in Measurement, ISBN 92-67-10188-9, 1st edn. ISO, Geneva, Switzerland (1993)