약학회지 (YAKHAK HOEJI)
- 제37권3호
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- Pages.286-289
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- 1993
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- 0377-9556(pISSN)
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- 2383-9457(eISSN)
메틸 5-히드록시 디나프토 [1, 2-2', 3'] 푸란-7, 12 디온 6-카복시레이트의 미량분석
Micro-Analysis of Methyl 5-Hydroxydinaphtho[1, 2-2', 3'] furan-7, 12-dione-6-carboxylate
초록
UV and high performance liquid chromatographic methods for the quantitative analysis of methyl 5-hydroxy-dinaphtho [1,2-2',3'] furan-7,12-dione-6-carboxylate(MHDDC) in urine and blood were developed. The correlation coefficients of the calibration curves of MHDDC in chloroform, methanol and dioxane solution were 0.999, 0.997 and 0.998, respectively. MHDDC was resolved within 15 min and had a detection limit of 2-5ng at S/N=3 by using a reversed-phase column with two solvents (MeOH, HAc).
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