• Title/Summary/Keyword: zone annealing

Search Result 44, Processing Time 0.029 seconds

A Study of defect distribution and profiles of MeV implanted phosphorus in silicon (실리콘에 MaV로 이온주입된 인의 결함분포와 profile에 관한 연구)

  • 정원채
    • Electrical & Electronic Materials
    • /
    • v.10 no.9
    • /
    • pp.881-888
    • /
    • 1997
  • This study demonstrats the profiles of phosphorus ions in silicon by MeV implantation(1∼3 MeV). Implanted profiles could be measured by SIMS(Cameca 4f) and compared with simulation results(TRIM program and analytical description method only using on Pearson function). The experimental result in the peak concentration region has a little bit deviation from simulation data. By RBS and Channeling measurements the defect distribution of implanted samples could be measured and spectrum are calibrated depth with RUMP simulation By XTEM measurement the thickness of defect zone also could be measured. Finally thermal annealing for the electrical activation of implanted ions carried out by RTA(rapid thermal annealing). The concentration-depth profiles after heat treatment was measured by SR(spreading resistance)-method.

  • PDF

Nb doped strontium titanate single crystal growth by floating zone method (Floating zone법에 의한 Nb를 첨가한 strontium titanate 단결정 성장)

  • Jeon, Byong-Sik;Cho, Hyun;Orr, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.5 no.3
    • /
    • pp.215-222
    • /
    • 1995
  • Nb doped strontium titanate single crystals were grown by the floating zone method. The doping amount of $Nb_2O_5$ was 0.2 wt %. Those crystals were grown in air and N z atmosphere and the growth rate was 5 mmlhr and rotation speed of upper and lower shaft was 30 rpm. The shapes of melt - feed rod interface depending on sintering temperatures were observed. In air atmosphere, the flow rate of air was 1.5 ${\ell}/min$ and in $N_2$ atmosphere, that of $N_2$ gas was 0.5 ${\ell}/min$. As grown crystals were analyseQ by XRD, Laue back - reflection and chemical etching. After annealing in $N_2$ atmosphere, resistivities of crystals were measured and the activation energies of each samples were calculated.

  • PDF

Effect of Annealing on the Mechanical properties of Fe-6.5wt% Si Alloy (Fe-6.5wt% Si 합금의 역학 특성에 미치는 어닐링 효과)

  • Yun, Yeong-Gi;Yun, Hui-Seok;Hong, Seong-Gil
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.24 no.12
    • /
    • pp.2909-2916
    • /
    • 2000
  • 6.5wt% Si steel is widely known as an excellent magnetic material because its magnetostriction is nearly zero. The AX magnetic properties as magnetostriction of 6.5% Si steel were evaluated and compared with those of conventional 3% Si steel sheet. In this paper, the fracture behavior of the poly crystals and single crystals of Fe-6.5wt%Si alloy has been observed. Single crystals were prepared by Floating Zone(FZ) method, which melts the alloy by the use of high temperature electron beam in pure argon gas condition. And the single crystals were annealed at 500$^{\circ}C$ and 700$^{\circ}C$ respectively and tensile tested at room temperature. According to the result, B2 phase has more good elongation than DO$_3$ phase. It was also found that the fracture surfaces of the single crystals have hairline facets in same direction, and the facets change the direction according to the single crystal phase.

A Study on the Mechanical Properties of Submerged Arc-Welded Zone between Different Kinds of Metal (서브머지드 아크 용접(熔接)에 의한 이종금속(異種金屬) 접합부의 기계적(機械的) 성질(性質)에 관한 연구)

  • Kang, Jai Won;Kim, Hyung Jong
    • Journal of Industrial Technology
    • /
    • v.18
    • /
    • pp.209-216
    • /
    • 1998
  • Some mechanical properties of the submerged arc-welded(SAW) zone between different kinds of metal (SS400+SB450) are investigated and compared with that between same kinds of metal (SS400+SS400 and SB450+SB450). The analysis of the chemical components and observation of the micro-structure by SEM of the weld zone are also carried out. And the effect of the stress relief annealing is examined by comparing tensile strength, elongation, toughness add hardness of SAW specimens before and after the heat treatment.

  • PDF

Comparison analysis of superconducting solenoid magnet systems for ECR ion source based on the evolution strategy optimization

  • Wei, Shaoqing;Lee, Sangjin
    • Progress in Superconductivity and Cryogenics
    • /
    • v.17 no.2
    • /
    • pp.36-40
    • /
    • 2015
  • Electron cyclotron resonance (ECR) ion source is an essential component of heavy-ion accelerator. For a given design, the intensities of the highly charged ion beams extracted from the source can be increased by enlarging the physical volume of ECR zone [1]. Several models for ECR ion source were and will be constructed depending on their operating conditions [2-4]. In this paper three simulation models with 3, 4 and 6 solenoid system were built, but it's not considered anything else except the number of coils. Two groups of optimization analysis are presented, and the evolution strategy (ES) is adopted as an optimization tool which is a technique based on the ideas of mutation, adaptation and annealing [5]. In this research, the volume of ECR zone was calculated approximately, and optimized designs for ECR solenoid magnet system were presented. Firstly it is better to make the volume of ECR zone large to increase the intensity of ion beam under the specific confinement field conditions. At the same time the total volume of superconducting solenoids must be decreased to save material. By considering the volume of ECR zone and the total length of solenoids in each model with different number of coils, the 6 solenoid system represented the highest coil performance. By the way, a certain case, ECR zone volume itself can be essential than the cost. So the maximum ECR zone volume for each solenoid magnet system was calculated respectively with the same size of the plasma chamber and the total magnet space. By comparing the volume of ECR zone, the 6 solenoid system can be also made with the maximum ECR zone volume.

Mechanical Properties and Ultrasonic Characteristic of SS400 and STS304 by Simulated Heats (열재현에 의한 SS300 및 STS304의 기계적 성질 및 초음파 특성)

  • Jeong, Jeong-Hwan;Ahn, Seok-Hwan;Park, In-Duck;Nam, Ki-Woo
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
    • /
    • 2003.10a
    • /
    • pp.127-132
    • /
    • 2003
  • In a today industry, the welding is doing a many portion in structure manufacture. This study is simulated heat of heat-effected zone and researched a mechanical properties and ultrasonic characteristic in used the SS400 and the STS304. As the result mechanical properties of steel that become drawing decreased because of remaining stress by strain gardening according as simulated heat temperature rises, but according as temperature rises in material that do simulated heat after have done annealing, mechanical propensity was improved. The velocity and attenuation become different by effect of remaining stress than effect of material internal microstructure in ultrasonic wave test. In the case of STS304, there was change in mechanical properties by effect that is by strain hardening, but there was no change in material that simulated heat after annealing. When become drawing in ultrasonic waves test, according as simulated heat temperatures rise, change of attenuation coefficient is looked, but material that simulated heat after annealing was no change almost both the volocity and attenuation.

  • PDF

Controlling striated structure in Pt with RF zone refining method (백금 결정 성장시 줄무늬 구조 제어)

  • ;;J. Vuillemin
    • Journal of the Korean Vacuum Society
    • /
    • v.5 no.4
    • /
    • pp.387-390
    • /
    • 1996
  • The study has been performed that the high purity of platinum crystal was grown by rf floating zone refined technique. Direct electric current was also present to examine the controlling striated structure during the sample grown. It has been proved that current and orientation could affect suppression of the striation structure in Pt. Substructure in Pt was thermally unstable and was able to be removed by the annealing technique.

  • PDF

High resistivity Czochralski-grown silicon single crystals for power devices

  • Lee, Kyoung-Hee
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.18 no.4
    • /
    • pp.137-139
    • /
    • 2008
  • Floating zone, neutron transmutation-doped and magnetic Czochralski silicon crystals are being widely used for fabrication power devices. To improve the quality of these devices and to decrease their production cost, it is necessary to use large-diameter wafers with high and uniform resistivity. Recent developments in the crystal growth technology of Czochralski silicon have enable to produce Czochralski silicon wafers with sufficient resistivity and with well-controlled, suitable concentration of oxygen. In addition, using Czoehralski silicon for substrate materials may offer economical benefits, First, Czoehralski silicon wafers might be cheaper than standard floating zone silicon wafers, Second, Czoehralski wafers are available up to diameter of 300 mm. Thus, very large area devices could be manufactured, which would entail significant saving in the costs, In this work, the conventional Czochralski silicon crystals were grown with higher oxygen concentrations using high pure polysilicon crystals. The silicon wafers were annealed by several steps in order to obtain saturated oxygen precipitation. In those wafers high resistivity over $5,000{\Omega}$ cm is kept even after thermal donor formation annealing.

Organic light emitting diodes using Iron(II) and Metal-free Phthalocyanine (Iron(II)과 Metal-free Phthalocyanine의 결정구조 변화에 따르는 유기 발광소자의 발광 특성)

  • 임은주;한우미;이정윤;김명식;이기진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2001.07a
    • /
    • pp.947-950
    • /
    • 2001
  • We report the characteristics of organic light emitting diodes (OLEDS) by controlling the carrier mobility according to the crystalline of Iron(II) Phthalocyanine(Fe-Pc) and metal-free Phthalocyanine (H$_2$-Pc). In order to change the recombination zone, we controlled the hole mobility by changing the crystal structures of Fe-Pc and H$_2$-Pc. OLEDs were constructed with ITO/Fe-Pc/triphenyl-diamine (TPD)/tris-(8-hydroxyquinoline)aluminum (Alq$_3$)/Al and ITO/H$_2$-Pc/triphenyl-diamine (TPD)/tris-(8-hydroxyquinoline)aluminum (Alq$_3$)/Al. The electroluminescent properties were changed according to the heat-treatments of Fe-Pc and H$_2$-Pc. We observed that the recombination zone and the carrier mobility were changed as the higher occupied molecular orbital levels of Fe-Pc and H$_2$-Pc decreased.

  • PDF

Weldability of Al Alloys, Part II :HAZ Cgaracteristics (알루미늄 합금의 용접특성 - part II)

  • 이창희;장래웅
    • Journal of Welding and Joining
    • /
    • v.11 no.1
    • /
    • pp.2-8
    • /
    • 1993
  • A literature review was conducted to gather informations available on the welding metallurgy of aluminum alloys, emphasized on characteristics in the heat affected zone(HAZ). Nominal metallurgical reactions that occur in aluminum alloys provide a basis for understanding aluminum welding metallurgy. However, welding reactions differ to some extent because of the relatively short times involved, and the non-isothermal heating excursed. For non-heat treatable alloys, welding primarily affects these alloys by annealing (recrystallization and growth) and to a less extent, changes in low temperature precipitates. In the case of heat treatable alloys, the resulting HAZ properties depend upon alloy composition, starting temper, heat input and post weld heat treatments.

  • PDF