• Journal of the Korean Wood Science and Technology
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• 제20권1호
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• pp.38-45
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• 1992

Fine and alkali-swollen structures of native cellulose fibers were investigated by x-ray diffraction methods. The results of fine structures are shown in Table 1. In meridional x-ray diffractograms, the relative intensity ratio R of (002) to (004) for cellulose I was ca. 0.05 and for regenerated cellulose it was ca. 0.45. It was considered that the transformation from cellulose I to cellulose II resulted from the packing or conformational change of cellulose chain. Finally. although cellulose I was not detected in the alkali-swollen celluloses treated for 1 hr to 24 hrs, washing and drying them resulted in the generation of considerable amounts of cellulose I and the amount decreased with increasing alkali duration.

• Journal of the Korean Wood Science and Technology
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• 제18권1호
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• pp.3-9
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• 1990

Expression is on operation of separating liquid from solid liquid mixtures which has long been used on a universal scale in widely divergent fields. In fruit pulps processing and fermentation industries. removal of a portion of the liquid in filler cake is essential to the maximum yields of products. In sewage sludge treatments, dewatering of filter cakes is important to disposal by incineration. transportation. and landfill. In the chemical process industries, drying of wet cakes increases cost, and it is desirable to eliminate as much liquor as possible by non-thermal methods. This paper is mainly concerned with the development of a simplified equation for constant-pressure expression.

• Journal of the Korean Wood Science and Technology
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• 제8권2호
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• pp.9-16
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• 1980

Papua New Guinea(PNG)산(産) TAUN재(材)를 이용한 합판제조 조건을 확립하였다. Taunwo(材)는 목질(木質)이 다양(多樣)하고 건조후 함수 분포가 균일(均一)치 못하여 퇴적(堆積)양생시키므로써 적정 함수분포를 유지할 수가 있었다. 또한 조직이 치밀하여 접착제와의 친화성이 낮아 집착불량이 용이하게 발생되기 쉬운 재(材)이나 제호시 수지율을 높여 도포하므로서 접착불량을 제거할 수가 있었다. Taun재(材)는 lauan재(材)나 kapur(材)와 혼합접합(混合接合) 하여도 접착력은 양호한 결과를 보였다.

• Journal of the Korean Wood Science and Technology
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• 제37권5호
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• pp.459-464
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• 2009

This study was conducted to find the relationship between the moisture content and basic density of green lumber and the final moisture content of kiln dried lumber. The possibility of using a ultrasonic nondestructive testing technology was investigated. Four matched 2-foot long boards were kiln-dried for 12, 24, 36 and 48 hours. Twenty three slices were cut to examine the distribution of moisture content along the length. It was revealed that the green weight was a better estimator of the final moisture content of the kiln-dried board than the green moisture content. The standard deviations of the moisture contents of the slices were not correlated with the final moisture contents of the kiln-dried boards. The two ultrasonic devices used for this study were apparently good tools for NDT.

• Journal of the Korean Wood Science and Technology
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• 제29권3호
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• pp.73-82
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• 2001

The ESEM could be used in investigating the fibrous networks developed during handsheet-forming processes with the exception of the stages relating to the actual dispersion of the fibers and the drying of formed sheets. Also the cross-sectional images of swollen fibers were generated with the ESEM but the information given by the images was rarely fresh compared to the CLSM images. The LTSEM was extremely useful in generating images of the microfibrillar structure of a wet fiber with great resolution. However, pretreatment required in the LTSEM chamber was somewhat tedious due to the time consumed in sublimation of ice and sputter coating. For observation of lamellar structure of a hydrated fiber, the LTSEM exhibited greatly detailed structure with high resolution. Finally ESEM and LTSEM should be used in a finite field such as observation of surface morphology in detail.

• Journal of the Korean Wood Science and Technology
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• 제30권3호
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• pp.12-17
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• 2002

The extracellular invertase (EC 3.2.1.26) (Candida utilis) preparation was obtained from the liquid medium after desalting and freeze drying. This prepared enzyme was used for the comparative purification on 4 activated matrices by liquid column affinity chromatography method. In this method there were used controlled porous glass (CPG) silanized covalently activated by keratin, silanized silica gel and silica gel covalently covered by keratin. It was found that the invertase purification process was better using both CPG matrices (silanized CPG and keratin activated CPG) than these with two silica gel supports. Also the elution coefficient of the invertase from the two CPG columns was about 93 to 94%. Two silica gel supports found to be superior in terms of purification efficiency. The invertase purification process was confirmed by PAGE electrophoresis.

• 한국지반환경공학회 논문집
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• 제15권10호
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• pp.29-34
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• 2014

본 연구에서는 다공성 실리카를 사용하여 시멘트계 고화재의 유해성을 개선한 경화토의 기후변화에 대한 강도특성을 규명하기 위하여 습윤건조 반복시험을 수행하여 경화토가 기후영향을 받기 전과 후의 강도특성을 규명하고자 한다. 본 연구에 사용된 경화토는 주위에서 쉽게 구할 수 있는 화강풍화토 및 우드칩을 사용하였으며, 일축압축시험을 위한 공시체는 지름 50 mm, 높이 100 mm의 크기로 혼합토 중량대비 실리카의 혼합비율을 5 %, 10 %, 15 %로 변화시키고 각 단계별로 우드칩을 0.5 %, 1.0 %, 1.5 % 혼합하여 제작하고 7, 14, 28일 동안 상온으로 양생시킨 후 습윤건조 반복과정을 0, 3, 6, 12 cycle을 반복하여 역학적인 특성을 평가하였다. 또한 습윤건조 전후의 상대동탄성계수 변화를 평가하기 위하여 각 사이클이 종료되면 동탄성시험을 수행하였다.

• Journal of the Korean Wood Science and Technology
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• 제45권4호
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• pp.456-462
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• 2017

Japanese anise (Illicium anisatum L.) twigs were collected and ground after drying, then immersed with 50% aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform ($CHCl_3$), ethylacetate (EtOAc) and $H_2O$, and then freeze-dried after condensation. A portion of EtOAc soluble fraction (5.7 g) was chromatographed on a Sephadex LH-20 column with various aqueous $MeOH-H_2O$. Compound 2 and compound 3 were isolated from fraction 8 and 5, respectively. Compound 1 and compound 4 were isolated after rechromatography of fraction 7. The isolated compounds were elucidated as (+)-catechin (1), taxifolin (2), taxifolin-3-O-${\beta}$-D-(+)-xylopyranose (3) and quercitrin (4) by spectral and literature data, and by comparison with the authentic samples. Of the isolated compounds, taxifolin (2), taxifolin-3-O-${\beta}$-D-(+)-D-xylopyranose (3) and quercitrin (4) were isolated, for the first time, from the extracts of japanese anise twigs.

• 임산에너지
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• 제18권2호
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• pp.62-69
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• 1999

목재 세포벽중의 셀룰로오스의 알칼리 팽윤구조는 리그닌에 의해 크게 영향을 받는다. 본 연구에서는 알칼리 팽윤특성에 관한 리그닌의 영향을 명확히 하기 위하여 신갈나무의 정상재 및 부후재를 이용하여 X선 회절법과 자외선 현미경법에 의해 검토하였다. 그 결과, 목재 셀룰로오스는 고농도의 알칼리 수용액 중에서 머서화 처리를 하여도 결정변태가 일어나지 않으며 탈리그닌 후에도 결정의 변화는 없었다. 즉, 목재세포벽중의 셀롤로오스 결정은 리그닌의 존재에 의해 알칼리 팽윤이 억제되어 결정의 변태는 발생하지 않으며 탈리그닌 후에도 결정의 구조는 변화되지 않는 것으로 생각되었다.

• Journal of the Korean Wood Science and Technology
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• 제26권3호
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• pp.48-52
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• 1998

Residues such as walnut, pinenut and peanut shells were used as a filler in adhesive for bonding radiata pine plywood. The nutshell residues were prepared by simply drying to 8% moisture content and grinding the dry material using a laboratory Wiley mill with a $75{\mu}m$ (200 mesh) screen. The nutshells residues were compared to a commercial filler commonly used in adhesives by the structural plywood and laminated veneer lumber industry in the United States. The adhesive mixes were made by following the recommended procedure of Georgia-Pacific Resins, Inc., using phenol-formaldehyde resin. For each filler type, three-ply plywoods, 6 mm nominal thickness and 30 by 30 cm in size, were fabricated at two press times (4 and 5 min) and around 30 minute assembly time. Evaluations of the nutshell residues were carried out by tension shear tests after cyclic boil tests on plywood. The results of the performance test included tension shear strength and wood failure. All plywoods made with the nutshell fillers were comparable to those made with the control filler. These results indicate that nutshell residues would be suitable as filler for plywood adhesives.