• Title/Summary/Keyword: wet processing

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Aspect Ratio Behavior of Grinding Particles with Variation of Particle Size by Wet Grinding (습식분쇄에 의한 입자크기 변화에 따른 분쇄입자의 종횡비 거동)

  • Choi, Jin Sam
    • Korean Journal of Materials Research
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    • v.30 no.5
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    • pp.223-230
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    • 2020
  • As a case study on aspect ratio behavior, Kaolin, zeolite, TiO2, pozzolan and diatomaceous earth minerals are investigated using wet milling with 0.3 mm media. The grinding process using small media of 0.3 pai is suitable for current work processing applications. Primary particles with average particle size distribution D50, ~6 ㎛ are shifted to submicron size, D50 ~0.6 ㎛ after grinding. Grinding of particles is characterized by various size parameters such as sphericity as geometric shape, equivalent diameter, and average particle size distribution. Herein, we systematically provide an overview of factors affecting the primary particle size reduction. Energy consumption for grinding is determined using classical grinding laws, including Rittinger's and Kick's laws. Submicron size is obtained at maximum frictional shear stress. Alterations in properties of wettability, heat resistance, thermal conductivity, and adhesion increase with increasing particle surface area. In the comparison of the aspect ratio of the submicron powder, the air heat conductivity and the total heat release amount increase 68 % and 2 times, respectively.

Maskless Pattern Fabrication on Si (100) Surface by Using Nano Indenter with KOH Wet Etching (나노인덴터와 KOH 습식 식각 기술을 병용한 Si(100) 표면의 마스크리스 패턴 제작 기술)

  • 윤성원;신용래;강충길
    • Transactions of Materials Processing
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    • v.12 no.7
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    • pp.640-646
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    • 2003
  • The nanoprobe based on lithography, mainly represented by SPM based technologies, has been recognized as potential application to fabricate the surface nanostructures because of its operational versatility and simplicity. The objective of the work is to suggest new mastless pattern fabrication technique using the combination of machining by nanoindenter and KOH wet etching. The scratch option of the nanoindenter is a very promising method for obtaining nanometer scale features on a large size specimen because it has a very wide working area and load range. Sample line patterns were machined on a silicon surface, which has a native oxide on it, by constant load scratch (CLS) of the Nanoindenter with a Berkovich diamond tip, and they were etched in KOH solutions to investigate chemical characteristics of the machined silicon surface. After the etching process, the convex structure was made because of masking effect of the affected layer generated by nano-scratch. On the basis of this fact, some line patterns with convex structures were fabricated. Achieved patterns can be used as a mold that will be used for mass production processes such as nanoimprint or PDMS molding process. All morphological data of scratch traces were scanned using atomic force microscope (AFM).

Rheological perspectives of industrial coating process

  • Kim, Sun-Hyung;Kim, Jae-Hong;Ahn, Kyung-Hyun;Lee, Seung-Jong
    • Korea-Australia Rheology Journal
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    • v.21 no.2
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    • pp.83-89
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    • 2009
  • Coating process plays an important role in information technology such as display, battery, chip manufacturing and so on. However, due to complexity of coating material and fast deformation of the coating flow, the process is hard to control and it is difficult to maintain the desired quality of the products. Moreover, it is hard to measure the coating process because of severe processing conditions such as high drying temperature, high deformation coating flow, and sensitivity to the processing variables etc. In this article, the coating process is to be re-illuminated from the rheological perspectives. The practical approach to analyze and quantify the coating process is discussed with respect to coating materials, coating flow and drying process. The ideas on the rheology control of coating materials, pressure and wet thickness control in patch coating process, and stress measurement during drying process will be discussed.

Consolidation of Iron Nanopowder by Nanopowder-Agglomerate Sintering at Elevated Temperature

  • Lee, Jai-Sung;Yun, Joon-Chul;Choi, Joon-Phil;Lee, Geon-Yong
    • Journal of Powder Materials
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    • v.20 no.1
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    • pp.1-6
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    • 2013
  • The key concept of nanopowder agglomerate sintering (NAS) is to enhance material transport by controlling the powder interface volume of nanopowder agglomerates. Using this concept, we developed a new approach to full density processing for the fabrication of pure iron nanomaterial using Fe nanopowder agglomerates from oxide powders. Full density processing of pure iron nanopowders was introduced in which the powder interface volume is manipulated in order to control the densification process and its corresponding microstructures. The full density sintering behavior of Fe nanopowders optimally size-controlled by wet-milling treatment was discussed in terms of densification process and microstructures.

Spent Fuel Processing Technologies for Waste Recycling (폐기물 재활용을 위한 사용후핵연료 처리기술)

  • Park, Byung Heung;Kim, Ki-Sub
    • Journal of Institute of Convergence Technology
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    • v.2 no.1
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    • pp.7-12
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    • 2012
  • Spent fuels are discharged from nuclear reactors as a result of power generations. The spent fuels would be considered as a useful resources because the main constituent is uranium and some other actinides are included in them. In order to utilize the resources chemical processes should be developed to treat the spent fuels and obtain uranium and other actinides to be fueled in a fast reactor. The technologies are categorized into wet and dry processes. In this study, the current status of such technologies is summarized to give a insight and a deep understanding on nuclear fuel cycles.

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Synthesis of spherical silica aerogel powder by emulsion polymerization technique

  • Hong, Sun Ki;Yoon, Mi Young;Hwang, Hae Jin
    • Journal of Ceramic Processing Research
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    • v.13 no.spc1
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    • pp.145-148
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    • 2012
  • Spherical silica aerogel powders were fabricated via an emulsion polymerization method from a water glass. A water-in-oil emulsion, in which droplets of a silicic acid solution are emulsified with span 80 (surfactant) in n-hexane, was produced by a high power homogenizer. After gelation, the surface of the spherical silica hydrogels was modified using a TMCS (trimethylchlorosilane)/n-hexane solution followed by solvent exchange from water to n-hexane. Hydrophobic silica wet gel droplets were dried at 80 ℃ under ambient pressure. A perfect spherical silica aerogel powder between1 to 12 ㎛ in diameter was obtained and its size can be controlled by mixing speed. The tapping density, pore volume, and BET surface area of the silica aerogel powder were approximately 0.08 g·cm-3, 3.5 ㎤·g-1 and 742 ㎡·g-1, respectively.

Rice pasta containing cultivar 'Saemimyeon' with high amylose contents and methods thereof

  • Cho, Jun Hyeon;Lee, Ji Yoon;Lee, Jong Hee;Son, Young Bo;Shin, Dong Jin;Han, Sang Ik;Song, You Chun;Park, Dong Soo;Oh, Myung Kyu
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2017.06a
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    • pp.253-253
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    • 2017
  • Recently, strong interest in the well-being and healthy food trends lead a spreading of rice processing products such as rice noodles, rice breads, and rice cakes. However, most of rice varieties developed in Korea showed very limited processing properties in processing of noodles compare to that of wheat flour. Moreover, low competitiveness as a raw processing materials due to high price give poor evaluations for rice noodles processing. To cope those barriers, 'Saemimyeon' a Tongil type high yielding variety with a high amylose contents was developed in RDA. 'Saemimyeon' showed about 10~32 % of increase in yield as 7.08MT/ha and 26.7% of high amylose contents together with easy grinding property of 65.7% of high chalkiness ratio. The both of milled as well as brown rice of 'Saemimyeon' were well fit for processing properties in rice pasta where the contents of rice flour for rice pasta was 99% (1% of Tapioka starch was intermixed in to the rice flour). A spaghetti type for wet noodles and macaroni type for dry noodles were developed, respectively. Each of pasta were showed relatively more or less an equal quality and panel test compare to that of durum wheat pasta products. Finally, rice pasta products could suggest an alternative idea for a new rice processing items where rice noodles market was stagnant.

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The Processing control of NiCuZn Ferrite (I) - Mixing and Size Reduction of Raw Materials by Wet Ball Milling. (NiCuZn Ferrite의 제조공정 제어 (제1보) - 습식 볼밀링에 의한 다성분 원료의 혼합 및 분쇄 공정의 고찰)

  • 류병환;김선희;최경숙;고재천
    • Journal of the Korean Magnetics Society
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    • v.5 no.6
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    • pp.928-936
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    • 1995
  • In this research, the processing control of NiCuZn Ferrite has been developed. The mixing and the size reduction of raw materials have been proceeded. In order to produce NiCuZn Ferrite, highly concentrated slurry with fixed ratio and wet ball milling were used. First, the dispersion behavior of raw mixture at the region of pH4~pH11 has been studied. Using wet ball milling operation, the best conditions of mixing and size reduction have been determined. Further more, the most suitable conditions, such as, dispersant kind, dispersant amount, milling time, and slurry concentration have been studied. The poly acrylic ammonium salt (PAN) was chosen as a suitable dispersant to have effective dispersion in basic region. The slurry of raw mixture without dispersant, showed high viscosity and poor grindability. As 0.7 wt% of PAN was added, the concentrated slurry (up to 55 vol%) was possible, and showed well grindability. After 18 h ball milling of 30 vol% of mixture slurry with 0.7 wt% of PAN, the average particle size and specific surface area of raw mixture were $0.54\mu\textrm{m}$ and $12.92m^{2}/cc$, respectively. The ball milled raw mixture, calcined at $700^{\circ}C$ for 3h, was totally changed into NiCuZn Ferrite with spinel phase.

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Detection of Dimer of Rhodamine 6G Perchlorate Doped in Ormosil (Ormosil에 침투된 Rhodamine 6G Perchlorate의 이중합체의 검출)

  • Kim, Goo-Dae;Lee, Dong-A;Moon, Ji-Woong;Park, Kyung-Su
    • Analytical Science and Technology
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    • v.10 no.3
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    • pp.225-229
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    • 1997
  • The stability of Rhodamine 6G Perchlorate(Rh6GP) doped in organically modified silicate(Ormosil) was investigated after the Ormosil was synthesized by sol-gel process. The composition of the Ormosil which makes organic dye molecules stable and dimer-free was decided from comparing absorption peaks of dye molecules in sol state, in wet gel and in completely dried gel. The stable and dimer-free Rh6GP doped in the Ormosil was achieved in the 0.1 molar ratio of HCl/TEOS.

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Application of computer vision for rapid measurement of seed germination

  • Tran, Quoc Huy;Wakholi, Collins;Cho, Byoung-Kwan
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2017.04a
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    • pp.154-154
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    • 2017
  • Root is an important organ of plant that typically lies below the surface of the soil. Root surface determines the ability of plants to absorb nutrient and water from the surrounding soil. This study describes an application of image processing and computer vision which was implemented for rapid measurement of seed germination such as root length, surface area, average diameter, branching points of roots. A CCD camera was used to obtain RGB image of seed germination which have been planted by wet paper in a humidity chamber. Temperature was controlled at approximately 250C and 90% relative humidity. Pre-processing techniques such as color space, binarized image by customized threshold, removal noise, dilation, skeleton method were applied to the obtained images for root segmentation. The various morphological parameters of roots were estimated from a root skeleton image with the accuracy of 95% and the speed of within 10 seconds. These results demonstrated the high potential of computer vision technique for the measurement of seed germination.

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