• 제목/요약/키워드: wet mixing

검색결과 179건 처리시간 0.032초

MA 316L ODS 및 Wet 316L ODS 스테인리스강에서 충격에너지에 미치는 소결 공정의 영향 (Effects of the Sintering Variable on Impact Energy in MA 316L ODS and Wet 316L ODS Stainless Steels)

  • 김성수;한창희;장진성
    • 한국분말재료학회지
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    • 제17권2호
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    • pp.113-122
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    • 2010
  • Two kinds of oxide-dispersion-strengthened (ODS) 316L stainless steel were manufactured using a wet mixing process(wet) and a mechanical alloying method (MA). An MA 316L ODS was prepared by a mixing of metal powder and a mechanical alloying process. A wet 316L ODS was manufactured by a wet mixing with 316L stainless steel powder. A solution of yttrium nitrate was dried after being in the wet 316L ODS alloy. The results showed that carbon and oxygen were effectively reduced during the degassing process before the hydroisostatic process (HIP) in both alloys. It appeared that the effect of HIP treatment on increase in impact energy was pronounced in the MA 316L ODS alloy. The MA 316L ODS alloy showed a higher yield strength and a smaller elongation, when compared to the wet 316L ODS alloy. This seemed to be attributed to the enhancement of bonding between oxide and matrix particles from HIP and to the presence of a finer oxide of about 20 nm from the MA process in the MA 316L ODS alloy.

건습식 혼합공정을 이용한 유연소재 상 전자파 차폐용 다층막 코팅 (Multilayer Coatings on Flexible substrate for Electromagnetic Shielding by Using Dry/Wet Hybrid Processes)

  • 이훈성;이명훈
    • 한국표면공학회지
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    • 제50권5호
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    • pp.373-379
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    • 2017
  • Dry processes like evaporation and sputtering in vacuum chamber are difficult to make a uniform, large area and high quality film on thin PET substrate because of PET degradation and bad adhesion. On the other hand, wet processes like electro or electroless plating have complex processes and require high environmental cost. In this study, we successfully prepared $2{\mu}m$ Zn/Cu/Ni multilayers coated on $12{\mu}m$ polyethylene terephthalate (PET) substrate by using dry-wet mixing processes. Their surface electric resistances were evaluated around $0.2{\Omega}$ by using 4 probe measurements. Furthermore, their corrosion resistance also evaluated by natural potential test and compared with other wet, dry and mixing process samples.

일부 합성피혁 근로자들의 Dimethylformamide, Methyl Ethyl Ketone, Toluene 노출에 따른 요중 대사물질 (Urinary Metabolites of Dimethylformamide, Methyl Ethyl Ketone, and Toluene exposed Workers in Synthetic Leather Factories)

  • 최호춘;김강윤;안선희;이영자;정규철
    • 한국산업보건학회지
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    • 제11권2호
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    • pp.135-144
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    • 2001
  • This study was performed to measure airborne dimethylformamide(DMF), methyl ethyl ketone(MEK) and toluene and their urinary metabolites concentrations and to determine the relationship between airborne and urinary concentration. Airborne samples and their urinary metabolites were measured 98 male workers who work for 8 synthetic leather factories in a portion of Kyoung-In area. Urine samples were collected at end-of-shift to estimate the exposure levels. 1. The concentration of airborne DMF by process was 8.81 ppm for wet-mixing, 15.05 ppm for wet-coating, 6.03 ppm for dry-mixing, 5.58 ppm for dry-coating, 5.37 ppm for printing, and 9.03 ppm for total. There was statistically significant difference by process. Urinary NMF concentrations of wet-mixing, wet-coating, dry-mixing, dry-coating and printing were $90.55mg/{\ell}$, $79.80mg/{\ell}$, $39.86mg/{\ell}$, $25.23mg/{\ell}$, and $38.15mg/{\ell}$, respectively, and total geometric mean was $56.24mg/{\ell}$. There was significant difference by process. 2. The concentration of airborne MEK by process was 1.89 ppm for wet-mixing, 1.96 ppm for wet-coating, 10.33 ppm for dry-mixing, 29.24 ppm for dry-coating, 14.98 ppm for printing, and 4.87 ppm for total. There was statistically significant difference by process. Urinary MEK concentrations of wetmixing, wet-coating, dry-mixing, dry-coating and printing were $0.93mg/{\ell}$, $0.70mg/{\ell}$, $3.29mg/{\ell}$, $3.29mg/{\ell}$, and $1.06mg/{\ell}$, respectively, and total geometric mean was $1.25mg/{\ell}$. There was statistically significant difference by process. Urinary MEK 3. The concentration of airborne toluene by process was 0.35ppm for wet-mixing, 0.42ppm for wet-coating, 2.95ppm for dry-mixing, 11.67ppm for dry-coating, 4.88ppm for printing, 1.24ppm for total. There was statistically significant difference by process. Urinary hippuric acid concentrations of wet-mixing, wet-coating, dry-mixing, dry-coating and printing were 0.24g/g creatinine, 0.21g/g creatinine, 0.34g/g creatinine, 0.52g/g creatinine, and 0.29g/g creatinine, respctively and total geometric mean was 0.28g/g creatinine. There was statistically significant difference by process. 4. No. of exceeded KPEL was 40 workers(40.8%) for DMF(10ppm), 1 worker(1.0%) for MEK(200ppm), and no worker for toluene(100ppm). No. of exceeded KBEI was 62 workers(63.3%) for urinary NMF($40mg/{\ell}$), 29 workers(29.6%) for urinary MEK, 1 worker(1.0%) for urinary hippuric acid. 5. The regression equations were Log(NMF)=0.4094*Log(DMF)+1.3587(r=0.4516) for DMF, Log(MEKU)=0.1859*Log(MEK)-0.0324(r=0.3303) for MEK, Log(HA)=0.2106*Log(Toluene)-0.5685(r=0.4497) for toluene. Synthetic leather factory workers expose to 3 kinds of organic solvents which are DMF, MEK and toluene. Their urinary NMF and MEK levels were higher than their concentration levels through respiratory. It seems that the urinary levels were affected skin absorption for working habit and alcohol intake.

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Study on engineering properties of xanthan gum reinforced kaolinite

  • Zhanbo Cheng;Xueyu Geng
    • Computers and Concrete
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    • 제31권6호
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    • pp.501-511
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    • 2023
  • The strengthening efficiency of biopolymer treated soil depends on biopolymer type, concentration ratio, soil type, initial water content, curing time and mixing method. In this study, the physical and mechanical properties of xanthan gum (XG) treated kaolinite were investigated through compaction test, Atterberg limit test, triaxial test and unconfined compression test. The results indicated that the optimum water content (OWC) increased from 30.3% of untreated clay to 33.5% of 5% XG treated clay, while the maximum dry density has a slight increase from 13.96 kg/m3 to 14 kg/m3 of 0.2% XG treated clay and decrease to 2.7 kg/m3 of 5% XG treated clay. Meanwhile, the plastic limit of XG treated clay increased with the increase of XG concentration, while 0.5% XG treated clay can be observed the maximum liquid limit with 79.5%. Moreover, there are the ideal water content about 1.3-1.5 times of the optimum water content achieving the maximum dry density and curing time to obtain the maximum compressive strength for different XG contents, which the UCS is 1.52 and 2.07 times of the maximum UCS of untreated soil for 0.5% and 1% XG treated clay, respectively. In addition, hot-dry mixing can achieve highest UCS than other mixing methods (e.g., dry mixing, wet mixing and hot-wet mixing).

산화물 분산강화형 316L 스테인리스강의 제조와 특성 연구 (Fabrication and Characterization of ODS 316L Stainless Steels)

  • 김민호;류호진;김성수;한창희;장진성;권오종
    • 한국분말재료학회지
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    • 제16권2호
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    • pp.122-130
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    • 2009
  • Austenitic oxide-dispersion-strengthened (ODS) stainless steel was fabricated using a wet mixing process without a mechanical milling in order to reduce contaminations of impurities during their fabrication process. Solution of yttrium nitrate was dried after a wet mixing with 316L stainless steel powder. Carbon and oxygen contents were effectively reduced by this wet processing. Microstructural analysis showed that coarse yttrium silicates of about 150 nm were formed in austenitic ODS steels with a silicon content of about 0.8 wt%. Wet-processed austenitic ODS steel without silicon showed higher yield strength by the presence of finer oxide of about 20 nm.

습식화학 방법에 의한 안정화된 $ZrO_2$의 제조 및 특성에 대한 연구 (Preparation and Characterization of Stabilized $ZrO_2$ by Wet Chemical Methods)

  • 전승범;변수일
    • 한국세라믹학회지
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    • 제16권3호
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    • pp.155-163
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    • 1979
  • This study was to explore the characteristics of 6 mole% CaO stabilized $ZrO_2$ prepared by wet chemical methods. The results of the experiments were as follows: 1. The powder calcined at 1000$^{\circ}$-110$0^{\circ}C$ was partly agglomerated. The morphology of agglomerate was spherical of 0.5-1$\mu{m}$ in size for Hot Petroleum Drying Method, chain-like of 1-2$\mu{m}$ for Freeze Drying Method, and irreqular of 2-3$\mu{m}$ for Coprecipitation Method. 2. Optimum calcining conditions for powder prepared by wet chemical methods were found: 110$0^{\circ}C$, 2h in air for Hot Petroleum Drying Method and Freeze Drying Method, and 100$0^{\circ}C$, 2h in air for Coprecipitation Method. 3. When specimen was calcined at 1000$^{\circ}$-110$0^{\circ}C$ in air for 2h and then sintered at 1$600^{\circ}C$ in air for 4h, the specimens prepared by wet chemical methods showed a high sintered density (94% of theoretical density) and a low open porosity (<0.8%); however, the sintered density of the specimen prepared by Oxide Wet Mixing Method was 90%. 4. The amount of cubic phase of sintered body prepared by wet chemical methods was observed to be higher than the one prepared by Oxide Wet Mixing Method. 5. It was found that Hot petroleum Drying Method, Freeze Drying Method and Coprecipitation Method were nearly the same in respect of the results of stabilization grade and sintered density of CaO-stabilized $ZrO_2$.

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혼합방법에 따른 순환아스팔트 혼합물의 수분저항성 통계검정 평가 (Statistical Evaluation of Moisture Resistance by Mixing Method of Recycled Asphalt Mixtures)

  • 김성운;김영삼;조영진;김광우
    • 한국건설순환자원학회논문집
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    • 제9권2호
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    • pp.167-176
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    • 2021
  • 순환아스팔트 혼합물은 제조 시 믹서에서 혼합되는 동안 노화된 RAP(회수 아스팔트포장재)을 잘 녹이는 것이 중요하다. 순환아스팔트 혼합물은 모든 재료(RAP, 신규 아스팔트 및 신규 골재)를 동시에 믹서에 넣고 혼합하여 생산한다. 동시 혼합(IM)방법으로 제조된 순환아스팔트 혼합물의 경우 RAP에 포함된 노화된 바인더는 신규 바인더와 혼합되는 동안 적절하게 회생되지 못하기 때문에 동일한 혼합물 내에서 신규 골재 주위에 코팅된 바인더보다 더 높은 산화·노화 수준을 나타내며, 큰 강성을 보인다. 본 연구에서는 RAP의 노화된 바인더를 회생시키기 위해서 단계 혼합(SM) 방법을 적용하였다. 첫 번째 단계에서는 RAP과 신규 아스팔트를 혼합한 다음 두 번째 단계에서는 가열된 신규 골재와 함께 혼합하였다. 혼합 방법에 따른 순환아스팔트 혼합물의 수분저항성 개선효과를 비교하기 위해 간접인장강도(ITS)와 인장강도 비(TSR) 시험을 수행하여 SM 방법과 IM 방법 간에 통계적 t- 테스트를 수행했다. 수분저항성을 평가하기 위해서 세 가지 전처리 조건 즉, -18℃ 동결 후 60℃에서 24 시간 수침, 60℃에서 48 시간 수침 및 60℃에서 72 시간 수침 조건을 적용하였다. SM 방법으로 제조한 순환아스팔트 혼합물의 TSR은 IM 방법에 의한 순환아스팔트 혼합물보다 분명히 높았고, SM 방법의 변동계수는 IM보다 낮았다. 또한 통계적 t-test에 의해 SM 방법의 ITSWET이 α = 0.05 수준에서 IM과 유의하게 다른 것으로 관찰되었다. 또한, SM 방법의 ITSWET은 IM과 비교하여 더 가혹한 조건에서 처리할수록 훨씬 개선된 결과를 나타냈다. 따라서 단계 혼합 방법은 기존의 동시 혼합방법으로 생산된 순환아스팔트 혼합물보다 더 높은 수분저항성을 보이고, 보다 더 우수한 순환아스팔트 혼합물을 생산하기 위한 중요한 혼합 방법임을 확인하였다.

습식교반경화토포장의 온도특성 (Temperature Characteristics of Wet-mixing Solidified Soil Pavement)

  • 유지형;이승원;김대성
    • 한국도로학회논문집
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    • 제8권1호
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    • pp.45-54
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    • 2006
  • 1970년대 이후로 국내 건설 산업은 건설위주의 정책으로 지속적인 성장을 이루어 왔지만 이로 인한 환경문제가 심각하게 대두되고 있다. 아스팔트 및 시멘트 콘크리트포장으로 이루어진 도시지역은 열을 흡수하여 국지적인 열섬효과를 만들어 도시지역의 기온을 상승시키는 원인이 되고 있다. 이러한 문제점의 대안으로 최근에 기존 포장에 비해 흡수열량과 방출열량이 적은 흙을 주재료로 하여 특수한 경화재와의 혼합물을 사용한 도로 포장공법이 개발 사용되고 있다. 본 연구에서는 아스팔트콘크리트와 시멘트콘크리트 및 습식교반경화토를 대상으로 시험포장을 실시하고, 현장계측을 통하여 포장형식에 따른 포장체의 온도를 측정하여 온도특성을 규명하였다. 연구 결과, 시험포장에서 계측한 결과를 분석하여 대기온도에 따른 포장표면온도와 포장체 내부에서의 온도를 추정할 수 있는 관계식을 제시하였다. 대기온도 변화에 따른 포장체 내부온도 변화는 아스팔트콘크리트포장에서 가장 큰 변화를 나타내는 반면, 습식교반경화토포장에서는 큰 변화를 보이고 있지 않다. 따라서 기존 포장에 비해 흡수열량과 방출열량이 적은 습식교반경화토를 이용하여 공원 산책로, 농로, 관광지 도로, 자전거전용 도로 등과 같은 도로에 적용하게 되면 도시지역의 기온상승을 방지함과 동시에 인체에 무해하고 환경친화적인 도로를 제공할 수 있을 것으로 판단된다.

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자연하천 해석을 위한 SU/PG 모형의 개발 (SU/PG Model Evaluation for river dynamics)

  • 한건연;박경옥;백창현
    • 한국수자원학회:학술대회논문집
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    • 한국수자원학회 2004년도 학술발표회
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    • pp.1331-1334
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    • 2004
  • Wet/Dry phenomena typically incorporate a number of complex flow mechanism. These include a momentum transfer and turbulent mixing caused by the delivery of water. However currently available one dimensional schemes applicable to wet/dry process cannot effectively simulate such process. Two dimensional finite element model, SU/PG, is used to simulate complex flow in this study. The Wetted Area Method in SU/PG allows elements to transition gradually between wet and dry states. The model is applicable to a straight river reach with irregular bathymetry. Wet/dry calculation using the wetted area method can simulate simple numerical test. The computed results of velocity vectors and water depth agree with those of observed. The methodology Presented in this study will contributed to two-dimensional wet/dry analysis in a river in this country.

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