• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.731-732
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• 2006

Recently warm compaction techniques are focused on and commercialization of one high-density compaction process in the P/M industry. Another development is a new SEGLESS using a developed lubricant that reduces ejection force at room temperature compaction. It is possible to achieve high-density by reducing lubricant amount. In this paper we confirmed that green density was $7.35g/cm^3$ at 686MPa of compaction pressure when the new SEGLESS was applied to relatively lower temperature warm compaction process, such as $80^{\circ}C$.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.195-196
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• 2006

In recent years, demands for sintered ferrous material with higher strength are increasing. To satisfy these demands, studies and commercial use of the die wall lubrication method, the warm compaction method and the combination of both methods are widely carried out to achieve high density. The die wall lubrication warm compaction method makes it possible to achieve high density by reducing internal lubricant through die wall lubrication, although the method involves several issues such as prolonged cycle time due to lubricant spraying and difficulty in spraying lubricant in the case of compacting with complicated geometry. Meanwhile, the conventional warm compaction method requiring no die wall lubricant application cannot achieve such a high density as in the case of die wall lubrication warm compaction due to higher volume of internal lubricant. However, this report discloses our study result in which the possibility of improving density is exhibited by using a lubricant type with superior dynamic ejection property that can reduce volume of lubricant additive.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.199-200
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• 2006

PM recent developments focus on increasing this technology's competitiveness when compared to wrought materials. Warm compaction allows the replacement of a double press double sinter process with a single warm press and sintering step, thus allowing cost and time savings. Moreover there are added benefits to consider such as reducing work in process and lessening part's logistics cost. This paper presents a successful industrial trial to replace a double press-double sinter process with a warm die compaction and sintering process. The part chosen was a high performance gear containing 0,9% wt. carbon. Sintering was conducted in a belt furnace at $1120^{\circ}C$ in a nitrogen rich atmosphere with rapid cooling process in order to obtain a quasi fully martensitic structure with a minimum of 700HV0,1 and 450HV10 after annealing. The balance between properties and cost is favoured by the use of a singular lubricant developed in a Eureka frame project together with POMETON S.A. and die warm compaction. Warm compaction is only needed to be effective on the gear teeth, in order to achieve the required properties. Therefore only the die is actually heated. This simplified system avoids flow rate problems typically involved when using more elaborate warm compaction equipments.

• 한국분말재료학회지
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• 제14권3호
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• pp.185-189
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• 2007

Various approaches have been proposed to increase the green density. Warm compaction method has been used for the reduction of residual stress, the improvement of magnetic properties and the higher densities. In this work, the effect of warm compaction on green density of Fe powder was investigated. After ball-milling of Fe oxide powder for 30 hours, Fe oxide powder was reduced through the hydrogen reduction process. The pure Fe powder and polymer binder were mixed by 3-D tubular mixer. And then the mixed powder was warm-compacted with various compaction pressure and binder contents. The green density of specimen was added polyvinyl binder was higher than any other specimens.

• 한국도로학회논문집
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• 제11권4호
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• pp.127-132
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• 2009

본 논문은 준고온 첨가제가 혼입된 3 종류(일반아스팔트, SBS 및 SMA)의 아스팔트 혼합물 다짐도 변화에 대한 시험 결과이다. 다짐 특성을 조사 분석하기 위하여 다짐 시간 변화와 준고온 첨가제 함량 변화에 의한 다짐도 측정을 실시하였으며, 다짐 온도를 일반시료에 비하여 $30^{\circ}C$ 및 $50^{\circ}C$를 낮추어 밀도를 비교하였다. 선회 다짐 장비를 사용하여 다짐 횟수 변화에 따른 다짐밀도의 변화를 측정하였다. 다짐시간 경과와 다짐도의 관계는 3 종류의 준고온 첨가제를 일반 아스팔트에 첨가하여 다짐시간 변화와 첨가제 함량 변화에 따른 다짐도를 측정하였다. 온도 저감에 따른 다짐도 비교는 일반 아스팔트 혼합물, 고분자 개질 아스팔트 및 SMA 혼합물 3 종류의 혼합물을 사용하여 시험을 실시하였다. 준고온 아스팔트 혼합물은 다짐온도 저감으로 인하여 일반시료 아스팔트 혼합물과 밀도의 차이가 발생하지 않아서 다짐도가 안정된 상태를 나타냈다. 한편, 혼합물의 종류 및 준고온 첨가제의 종류에 따라 밀도의 차이, 다짐도 변화의 추이 변화가 발견되어 이들 두 인자 사이에 상관관계가 있는 것으로 나타났다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.197-198
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• 2006

The high pressure compaction without internal lubricant and the high green density even with the pore free density were achieved by the newly developed die wall lubricant for warm compaction. This developed die wall lubricated warm compaction followed by high temperature sintering resulted in not only the superior mechanical property but also the low dimensional change. In this paper, the effects of increasing the green density on the sintered density, the dimensional change and the mechanical property are mainly discussed

• Archives of Metallurgy and Materials
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• 제66권3호
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• pp.679-682
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• 2021

The objective of the present research is to develop new admixed lubricants which can be used for high-density sintered iron when processed using warm die and warm compaction. Depending on various lubricants, the effect of compaction temperature on the ejection behavior and sintered properties was studied. Lubricants were prepared by mixing of Zn-stearate and ethylene bis stearamide (EBS) in various compositions. The iron powders blended with lubricants were compacted under the pressure of 700 MPa at various temperatures. The green compacts were sintered at 1120℃ for 30 min. Microstructure, density, hardness, and transverse rupture strength of sintered materials with different lubricants were investigated in detail.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.191-192
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• 2006

The deformation under radial pressure of rectangular dies for metal powder compaction has been investigated by FEM. The explored variables have been: aspect ratio of die profile, ratio between diagonal of the profile and die height, insert and ring thickness, radius at die corners, interference, different insert materials, i. e. conventional HSS, HSS from powders, cemented carbide (10% Co). The analyses have ascertained the unwanted appearance of tensile normal stress on brittle materials, also "at rest", and even some dramatic changes of stress patterns as the die height increases with respect to the rectangular profile dimensions. Different materials behave differently, mainly due to difference of thermal expansion coefficients. Profile changes occur when the dies are heated up to the temperature required for warm compaction. The deformation patterns depend on compaction temperature and thermal expansion coefficients.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.987-988
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• 2006

The processes of P/M affect the properties of sintered gears. The different techniques of P/M lead to the different properties of sintered gears. This paper summarizes new progress in powder metallurgy for sintered gears. These progresses include warm compaction, high velocity compaction, sinter hardening, high temperature sintering, infiltration, CNC powder press and surface densification etc.

• 한국분말재료학회지
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• 제7권1호
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• pp.42-49
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• 2000

Densificationbehavior of conventional austenitic stainless steel powder compacts was studied by comparing the relative density of sintered compact(Ds)with that of green compacts(Dg)prepared with various catbon contents and P/M process. Dg of 304and 316 powders by warm compaction under pressure of 686 MPa at heating temperature of powder(553K) and dies (573K) were 80% and 81%, repectively, whichwere 2 and 3% higher than those of conventional green compacts at the same pressure. Ds of 304 compacts sintered at 1373K in H2 gas has the same value of 84% max. regardless of compacting temperature, and Ds of 316 compacts at the same sintering conditions were 80% by conventional compaction and 83% by warm compaction. Oxygen contents of 304 and 316 sintered compacts were increased 1.43∼2.94% and 0.010∼0.921% higher than those of raw powders and warm green compacts, respectively. In other case, Ds of 316 compacts sintered at 1573K in vacuum had the same value of 86%max. And Ds of 316 compacts at the same sintering conditions were 83% and 86% by conventional and warm compaction, respectively. Oxygen contents of 304 sintered compacts were 0.321% and 0.360%, and in case of 316, they were 0.419% and 0.182% by the respective compating condition. With carbon additions in the range 0.1∼0.6% Ds increased to the extent of 86∼89% in 304 sintered compacts, and to 82∼84% and 85∼87% in 316 according to different two compacting peocesses compared to those of sintered compacts without carbon addition.