• Title/Summary/Keyword: viscometer

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Rheological Properties of Cement Paste Blended Blast Furnace Slag or Fly Ash Powder (고로슬래그 및 플라이 애시 분말을 혼합한 시멘트 페이스트의 유동특성)

  • Song, Jong-Taek;Park, Hyo-Sang;Byun, Seung-Ho;Yoo, Dong-Woo
    • Journal of the Korean Ceramic Society
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    • v.45 no.6
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    • pp.336-344
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    • 2008
  • Rheological properties of cement pastes containing blast furnace slag (BFS: 3,900, $7,910\;cm^2/g$) or fly ash powder (FA: 4,120, $8,100\;cm^2/g$) according to the ratio of water/binder (W/B) and the dosage of polycarboxylate type superplasticizer (PC) were investigated by a mini slump and a coaxial cylinder viscometer. In this experiment, the ratio of replacing OPC with BFS or FA was 30 wt%, the W/B was from 30 to 70 wt%. As a result, the fluidity of cement paste containing BFS or FA was improved with increasing W/B and the dosage of PC. BFS or FA replaced cement paste with W/B 70% and PC 0.3% showed the highest fluidity. The segregation range of cement paste was occurred below $10\;d/cm^2$ of the yield stress and below 50 cPs of the plastic viscosity by the coaxial cylinder viscometer. And also it was formed that the plastic viscosity and the yield stress of FA replaced cement paste were higher than them of BFS replaced cement paste.

Effect of Temperature and Pressure on the Viscosity of Benzene (벤젠의 점성도에 대한 온도와 압력의 영향)

  • Jeong Rim Kim;Jin Burm Kyong;Mi Hyun Lew
    • Journal of the Korean Chemical Society
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    • v.37 no.12
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    • pp.1003-1009
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    • 1993
  • The viscosities of benzene have been determined at several temperatures and pressures to investigate the effect of temperature and pressure on the viscosity of benzene in liquid phase. When a falling ball viscometer with a constant volume contained a given amount of liquid benzene at desired temperatures and pressures, the viscosities of benzene in the viscometer could be evaluated from the measurements of the falling time of a skinker. The variations of the specific volume and the free volume of liquid benzene with temperature and pressure were, from the results, searched out. Finally, the effects of temperature and pressure on the viscosity of benzene were discussed by means of the variations of free volume with temperature and pressure.

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Effect of PPG, MDI, 2-HEMA and butyl acrylate content on the properties of polyurethane adhesive (폴리우레탄 접착제의 물성에 미치는 PPG, MDI, 2-HEMA 및 butyl acrylate량의 영향)

  • Park, Chan Young
    • Elastomers and Composites
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    • v.49 no.3
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    • pp.245-252
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    • 2014
  • FT-IR measurement and the physical properties of polyurethane adhesive prepared from the polyol, isocyanate, 2-HEMA and other acrylate monomers were examined. The softening point, viscosity, adhesion strength and mechanical properties of the PU adhesives were reviewed by Ring and Ball method, Brookfield viscometer and universal test machine, respectively. Results revealed that increment of both PPG amount and butyl acrylate content decreased softening point, adhesion strength, tensile strength and 100% modulus. However as 2-HEMA and MDI content increased the mechanical properties including tensile strength, 100% modulus increased, and also the viscosity and NCO content increased.

Physicochemical Characteristics of Galactomannan by Fractionation to Evaluate Heterogeneity (불균일 성질을 평가하기 위한 분획화된 galactomannan의 이화학적 특성)

  • Kim, Kyeong-Yee;Lee, Eun-Kyung
    • Korean Journal of Food Science and Technology
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    • v.45 no.4
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    • pp.428-433
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    • 2013
  • Heterogenous samples of locust bean gum (galactomannan) were prepared into homogeneous substances. Locust bean gum was fractioned using ammonium sulfate (14.11-23.08%, w/w). The intrinsic viscosity was obtained by extrapolating reduced viscosity versus concentration by using an Ubbelohde viscometer. The ranges of intrinsic viscosity for fractions that not included protein (F3-F6) and fractions that included protein (F1-F2) were 9.89-8.10 and 8.44-4.59, respectively. Values for Huggins' coefficient (k'), which depends on physical interactions, were 0.46-0.78. Increasing ammonium sulfate concentration was associated with a weak trend towards lower molecular weight and intrinsic viscosity by size-exclusion chromatography (SEC): $M_w$ ranged from 674 to 617 kg/mol and [${\eta}$] from 9.80 to 8.10 dL/g between F3 and F6. The evaluations of those fractions by using SEC and the Ubbelohde viscometer produced very similar values, as predicted. We verified the application of a gradient of ammonium sulfate to precipitate locust bean gum into fractions of different molecular size and show structural variations.

Rheological behavior study of Marine Lubricating oil on the amount of MGO (Marine Gas Oil) dilution (해상용 경유의 희석량에 따른 선박용 윤활유의 유변학적 거동연구)

  • Song, In Chul;Lee, Young Ho;Yeo, Young Hwa;Ahn, Su Hyun;Kim, Dae il
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.22 no.2
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    • pp.240-245
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    • 2016
  • This paper describes the rheological behavior study such as viscosity and change of shear stress regarding marine lubricating oil according to the amount of Marine Gas Oil (MGO) dilution. The viscosity reduction due to fuel dilution is crucially important characteristic to decreasing engine durability because of the abrasion of piston ring or liner. The lubricating oil used in this paper was blended with magnetic stirrer diluted High Sulfur Diesel (HSD, 0.05 wt%) ratio of 3 %, 6 %, 10 %, 15 % and 20 %. The viscosity and shear stress of diluted lubricating oil were measured with the temperature range from $-10^{\circ}C$ to $80^{\circ}C$ using a rotary viscometer (Brookfield Viscometer). As the amount of MGO dilution increasing in lubricating oil, the viscosity and stress of those decreased, because the lubricating oil diluted MGO with low viscosity show the trends to decreased viscosity and shear stress. Especially, the viscosity and shear stress of lubricating oil radically decreased at low temperature ($0{\sim}-10^{\circ}C$) and doesn't effect in MGO dilution at over $40^{\circ}C$. As temperature risen, the reduction of the viscosity and shear stress in lubricating oil shows the Newtonian behavior. The lubricating oil was required to check up periodically to improve engine durability since the viscosity reduction by MGO dilution accelerating the engine abrasion.

A Sduty on the Vulcanization Characteristic of Combined Accelerators in SBR compounds. (SBR의 가황촉진제(加黃促進劑) 병용효과(倂用效果)에 의한 가황특성(加黃特性) 연구(硏究))

  • Choi, Jae-Woon;Lee, Ki-Jong
    • Elastomers and Composites
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    • v.17 no.3
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    • pp.151-158
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    • 1982
  • The purpose of this study is to get comparitive results on the combined accelerator systems comprised of MBT, MBTS, DPG and CBS with TMTD, TMTM, Zn-MDC and DPG to SBR compound. Vulcanization characterstics and physical properties of the combined accelerators have been studied by mean of the Mooney viscometer, tensile testing machine, aging chamber and so on. According to the test results, TMTD with DPG system has shown faster Mooney scorch time than other system. The vulcanizate comprise of Zn-MDC with DPG and TMTD with DPG accelerator system has taken advantage of heat resistance.

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A Rheological Study of Topical Vehicles

  • Min, Shin-Hong;Rhee, Shanghi;Kim, Yong-Bae
    • Archives of Pharmacal Research
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    • v.2 no.2
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    • pp.89-97
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    • 1979
  • To find out the rheological characteristics of several pharamaceutical semisolid products, experiments were carriedout over the temperature range of 20 to 30 .deg.C . From continuous shear rheograms obtained with a Ferranti-Shirley cone and plate viscometer, loop area, shear rates, ryild values, limiting viscosities and activation energies were calculated. The systems were metastable and their viscosity decreased with time. As the temperature was raised, products studied showed a decrease in viscosity and yield value.

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Hydrodynamic Entrance Lengths and Entrance Correction Factors for a POWER-LAW Fluid in a Circular Duct (원관에서 POWER-LAW 유체의 수력학적 입구길이와 입구보정계수에 관한연구)

  • 오광석
    • The Korean Journal of Rheology
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    • v.7 no.3
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    • pp.261-266
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    • 1995
  • 원관에서 power-law 유체에 대하여 수력학적 입구길이와 입구보정계수를 측정할수 있는 새로운 방법이 개발되었다. 유변학적 성질을 측정할수 있는 긴관과 입구보정계수를 측 정할수 있는 짧은 관을 가진 새로운 모세관 점도계를 이용하여 증류수를 실험한 결과 유변 학적 성질과 입구 보정계수가 표준값과 비교하여 1%안의 오차를 얻었다. Power-law 유체 에 대한 해석 및 실험결과(Carbopol 960 용액)도 이미 보고된 값과 $\pm$6% 이내로 잘 일치하 였다.

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A Study on the Effect of Mastication in Solution SBR (용액중합 SBR의 내림효과에 관한 연구)

  • Oh, Jeong-Hoon;Yoon, Dong-Il
    • Elastomers and Composites
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    • v.27 no.4
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    • pp.262-266
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    • 1992
  • A number of tin-containing elastomers are produced commercially by Korea Kumho Petrochemical Co., Ltd. (KKPC) under the Kosyn Sol tradename. The effect of mastication of commercial and laboratory polymerized S-SBR has, been investigated using chemical mixer(ML-500), NMR, GPC and Mooney viscometer. Mastication of polymers containings coupling bonds is affected by the amount of stearic acid, the temperature of mixing and the time length of mixing.

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Synthetic Conditions and Rheological Characteristics of Barium Sulfate (황산바륨의 합성조건과 유동학적 특성)

  • Shin, Wha-Woo;Kim, Jun-Hea;Choi, Kwang-Sik;Chang, Young-Soo;Lee, Kwang-Pyo
    • YAKHAK HOEJI
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    • v.36 no.6
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    • pp.538-547
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    • 1992
  • Optimal synthetic condition of barium sulfate were investigated from the viewpoint of yield and bulkiness according to a randomized complete block design proposed by G.E.P. Box and K.B. Wilson. Barium chloride and magnesium sulfate were utilized as reactants in order to prepare barium sulfate in this study. It was found that optimum temperature range of reactant solutions was $60{\sim}100^{\circ}C$ and the optimum concentration range of the reactant solutions was $10{\sim}17.3%$ and $10{\sim}20%$ respectively, on the viewpoint of yield and bulkiness. The optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum reacting time range was $15{\sim}20$ minutes. The optimum drying temperature range was $110{\sim}130^{\circ}C$ from the viewpoint of yield, but it was $90{\sim}110^{\circ}C$ on the basis of bulkiness. Apparent viscosity of barium sulfate suspensions dispersed in various concentrations of Na. CMC was measured by using Brookfield synchrolectric viscometer model LVT, the relative equation, log ${\eta}_{sp}=A+B.{\phi}$ was examined and the equation was found to agree fairly well. 1 w/v% Na. CMC aqueous solution and 0.1 volume fraction of $BaSO_4$ powder were optimum in the preparation of $BaSO_4$ suspension showing highest viscosity at infinite shearing.

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