• 한국화재소방학회논문지
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• 제20권4호
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• pp.110-115
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• 2006

폴리우레탄에 인계 화합물을 첨가하여 폴리우레탄폼을 제조하였으며, 인계 화합물이 제조된 폴리우레탄폼의 기계적 물성과 난연성에 미치는 영향에 대하여 고찰하였다. 폴리우레탄과 인계 난연제인 Tri(chloroisopropyl) phosphate(TCPP), Triethyl phosphate(TEP), Trimethyl phosphate(TMP) 각각을 약 $90^{\circ}C$에서 혼합시켜 혼합물로부터 제조된 경질 폴리우레탄폼에 대한 여러 실험을 통하여 기계적 물성뿐만 아니라 난연 효과도 상당히 향상됨을 확인하였다. Cone calorimeter를 이용하여 열방출율(heat release rate, HRR)을 측정하여 난연 첨가제의 함량에 따른 재료별 난연 특성을 평가하였다. 그리고 Scanning Electron Microscope(SEM)을 사용하여 난연제를 첨가하여 만든 폴리우레탄폼의 morphology를 관찰한 결과 순수한 폼과 마찬가지로 매우 균일한 형태의 cell 분포를 가짐을 확인하였다.

• 한국기계가공학회지
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• 제20권6호
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• pp.114-120
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• 2021

This study is focused on the root mean square and peak-to-valley based on the injection conditions of the f-theta lens, one of the main components of laser printers and laser scanning systems. The f-theta lens of an aspherical plastic lens requires ultra-preaction. Injection molding is typically used for the mass production of aspherical plastic lenses. In the injection-molding method, the resin in the lens shape is filled with the resin after melting the plastic pellets at a constant temperature and then cooled. It is necessary to maintain a uniform injection molding system to produce high-quality lenses. These injection-molding systems are influenced by different factors, such as pressure, speed, temperature, mold, and cooling. It is possible to obtain a lens that exhibits the optical characteristics required to achieve harmony. We investigated the root mean square and peak-to-valley caused by variations in temperature, a critical parameter in the melting and cooling of plastic resins generated inside and outside the injection mold.

• 한국기계가공학회지
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• 제20권9호
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• pp.20-27
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• 2021

The effective surface of lens was studied for injection molding process and to enable mass production of f-theta lens, which is the primary component of laser printers and laser scanning systems. Injection molding is an optimal method if f-theta lens is frequently used for the mass production of plastic lenses as an aspherical lens that requires ultra-precision. A uniform injection molding system should be maintained to produce high quality lenses. Additionally, to maintain these injection molding systems, various factors such as pressure, speed, temperature, mold and cooling should be considered. However, a lens with the optical characteristics of an f-theta lens can be obtained. The effects of melting and cooling of plastic resin on the effective surface of f-theta lenses and the numerous factors that affect the injection molding process were studied.

• 대한금속재료학회지
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• 제50권10호
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• pp.763-768
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• 2012

The uniform and highly smooth nanofibers of biocompatible poly(${\varepsilon}$-caprolactone) (PCL) composited with different contents of multiwalled carbon nanotubes (MWCNTs) were successfully prepared by electrospinning. Experimental parameters were MWCNTs addition to a PCL solution and applied voltages. The topographical features of the composite nanofibers were characterized by scanning electron microscopy and its electrical properties were measured by a four-point probe method. The surface resistance gradually decreased with an increasing content of MWCNTs in PCL fibers because of the excellent electrical conductivity of MWCNTs. The nanofiber diameter could be regulated by varying the solution viscosity and voltages. Our results establish that this kind of electrospinning PCL/MWCNTs nanofibers with the control of fiber diameter and electrical conductivity may be a promising candidate for the application of scaffolds in tissue engineering.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.281.1-281.1
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• 2016

Transition metal dichalcogenides (TMDCs) are promising layered structure materials for next-generation nano electronic devices. Many investigation on the FET device using TMDCs channel material have been performed with some integrated approach. To use TMDCs for channel material of top-gate thin film transistor(TFT), the study on high-k dielectrics on TMDCs is necessary. However, uniform growth of atomic-layer-deposited high-k dielectric film on TMDCs is difficult, owing to the lack of dangling bonds and functional groups on TMDC's basal plane. We demonstrate the effect of remote oxygen plasma pretreatment of large area synthesized few-layer MoSe2 on the growth behavior of Al2O3, which were formed by atomic layer deposition (ALD) using tri-methylaluminum (TMA) metal precursors with water oxidant. We investigated uniformity of Al2O3 by Atomic force microscopy (AFM) and Scanning electron microscopy (SEM). Raman features of MoSe2 with remote plasma pretreatment time were obtained to confirm physical plasma damage. In addition, X-ray photoelectron spectroscopy (XPS) was measured to investigate the reaction between MoSe2 and oxygen atom after the remote O2 plasma pretreatment. Finally, we have uniform Al2O3 thin film on the MoSe2 by remote O2 plasma pretreatment before ALD. This study can provide interfacial engineering process to decrease the leakage current and to improve mobility of top-gate TFT much higher.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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• pp.429-429
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• 2008

Li$[Ni_{1/2}Co_{1/2}]O_2$ powder were synthesized from co-precipitation spherical metal oxide, $[Ni_{1/2}Co_{1/2}](OH)_2$. The preparation of metal hydroxide was significantly dependent on synthetic conditions, such as pH, amount of chelating agent, stirring speed, etc. The optimized condition resulted in $[Ni_{1/2}Co_{1/2}](OH)_2$, of which the particle size distribution was uniform and the particle shape was spherical, as observed by scanning electron microscopy. Calcination of the uniform metal hydroxide with LiOH at higher temperature led to a well-ordered layer-structured Li$[Ni_{1/2}Co_{1/2}]O_2$, as confirmed by X-ray diffraction pattern. Also these materials have ${\alpha}-NaFeO_2$ ($R\bar{3}m$) structure. Due to the homogeneity of the metal hydroxide, $[Ni_{1/2}Co_{1/2}](OH)_2$, the final product, Li$[Ni_{1/2}Co_{1/2}]O_2$, was also significantly uniform, i.e., the average particle size was of about 10 to 15 ${\mu}m$ in diameter and the distribution was relatively narrow. As a result, the corresponding tap-density was also high approximately 2.41 $gcm^{-3}$, of which the value is comparable to that of commercialized $LiCoO_2$.

• 한국항공우주학회지
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• 제39권2호
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• pp.106-113
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• 2011

본 논문에서는 균일 열부가 하중을 받는 사각판의 자유 진동특성을 실험을 통하여 연구하였다. 사각판의 재질은 알루미늄, 강재 및 스테인레스 강이고 사각판의 재원은 0.1 $\times$ 0.1 $\times$ 0.002 m 이다. 열부가 하중을 위해 적외선 석영 램프를 사용하였고, 전력조절을 위해 PCS(Power Control System)을 사용하였으며, 주파수 함수를 얻기 위해 비접촉식 진동측정 장비를 사용하였다. 부가한 온도 조건은 상온에서부터 $300^{\circ}C$까지 $50^{\circ}C$간격으로 부가하였다. 경계조건은 번지코드를 사용하여 자유-자유 조건을 구현하였다. 사각판의 전면 전체를 균일하게 가열하였다.

• 대한금속재료학회지
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• 제48권7호
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• pp.625-629
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• 2010

This study investigates the effects of porosity on the thermal stability and the thermal shock resistance of a porous nozzle used for blowing an inert gas. The samples of $Al_2O_3-SiO_2-ZrO_2$ system, which had the apparent porosity of 16~30% and bulk density of $2.6{\sim}3.2g/cm^3$, were prepared by adding different graphite contents (5, 10, 20 wt%) as a pore-forming agent. The thermal shock test was conducted at ${\Delta}T=500$, 1000, and $1400^{\circ}C$ also and the thermal stability was also carried out at 1550, 1600, and $1650^{\circ}C$ for 5 hrs. The specimen contained 10 wt% graphite had uniform pore size distribution, whereas the specimen with 20 wt% graphite showed non-uniform pore size distribution. As a result of thermal shock test, the specimen containing 10 wt% graphite appears to have higher mechanical strength than the other specimens (5, 20 wt% graphite). Both the 5 wt% and 20 wt% graphite specimens developed a non-uniform pore size distribution and cracks that were generated by intensive thermal stress.

• Transactions on Electrical and Electronic Materials
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• 제17권3호
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• pp.139-142
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• 2016

β-AgVO₃ nanorods have been successfully synthesized using a soft chemistry route followed by heat treatment. They were characterized by X-ray diffraction and field emission scanning electron microscopy, and their electrochemical properties were investigated using cyclic voltammetry, impedance spectra, and charge-discharge tests. The results showed that the smooth-surfaced nanorods are very uniform and well dispersed, with diameters of ~100-200 nm and lengths of the order of several macrometers. The nanorods deliver a maximum specific discharge capacity of 275 mAh g^-1 at 30 mA g^-1. They also demonstrated good rate capability with a discharge capacity at the 100^th cycle of 51 mAh g^-1.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2009년도 추계학술대회 논문집
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• pp.159-159
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• 2009

We characterize a flexible self-assembled liquid crystal display (LCD) fabricated from a polyimide (PI) alignment layer with polydimethylsiloxane pixel walls. Ion beam (IB) irradiation aligned LC molecules in the PI layer and bonded two flexible plastic substrates in a one-step assembly of the pixel walls. X-ray photoelectron spectroscopic analysis, Fourier transform infrared spectroscopy, and scanning electron microscopy provided chemical and physical evidence for the formation of stable chemical bonds between the PI layer and the PDMS pixel walls in addition to the important maintenance of a uniform 6 um gap between the two substrates without the use of any epoxy resins or other polymers.