• 제목/요약/키워드: three phases

검색결과 1,414건 처리시간 0.03초

Preparation of Ultrafine Au-Pb Particles by Gas-evaporation Technique

  • Ohno, Takehisa;Funaguchi, Hironori
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.158-159
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    • 2006
  • Ultrafine Au-Pb particles prepared by two method, (1) simultaneous evaporation of Au and Pb in inert gas and (2) subsequent vapor condensation of Pb in a differentially evacuated tube onto flying Au nanoparticles prepared by gasevaporation technique, were observed by electron microscopy. In the method (1), the particles that grew at the region where the two smoke masses converged, consisted of alloy phases. In the method (2), the particles consisted of two or three phases of Au, $Au_2Pb$, $AuPb_2$ and Pb phases in turn from the inner part, Pb-rich particles being composed of only two phases of $AuPb_2$ and Pb.

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Investigation on the Sintering Behavior of P/M Al-Zn-Mg-Cu Alloy

  • Shahmohammadi, M.;Simchi, A.;Danninger, H.;Arvand, A.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.536-537
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    • 2006
  • In the present work, the sintering behavior of high strength Al-5.6Zn-2.5Mg-1.6Cu (in wt.%) alloy compacts prepared from elemental powders was investigated. Microstructural evaluation was accompanied by XRD and DSC methods in order to determine the temperature and chemical composition of the liquid phases formed during sintering. It was found that three transient liquid phases are formed at 420, 439 and 450 $^{\circ}C$. Microstructural study revealed the progressive formation of sintered contacts due to the presence of the liquid phases, although the green compact expands as a result of the melt penetration along the grain boundaries. While Zn melts at ${\sim}420\;^{\circ}C$, the intermetallic phases formed between Al and Mg were found to be responsible for the formation of liquid phase and the dimensional change at higher temperatures.

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Chiral Recognition Models of Enantiomeric Separation on Cyclodextrin Chiral Staionary Phases

  • 이선행;김병학;이영철
    • Bulletin of the Korean Chemical Society
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    • 제16권4호
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    • pp.305-309
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    • 1995
  • The enantiomeric separation of several amino acid derivatives by reversed-phase liquid chromatography using two (R)-and (S)-naphthylethylcarbamate-β-cyclodextrin(NEC-β-CD) bonded stationary phases was studied to illustrate the chiral recognition model of the enantiomeric separation. The retention and enantioselectivity of the chiral separations with (R)-and (S)-NEC-β-CD bonded phases were compared with similar separations with the native β-CD stationary phases. Especially, the enantioselectivity and elution orders between the derivatized amino acid enantiomers are carefully examined. These results can be illustrated by the chiral recognition models involving inclusion complexation, π-π interaction, and/or hydrophobic interaction. Inclusion complexation and hydrophobic interaction of the naphthyl group of the NEC moiety seem to be major chiral recognition components in the enantiomeric separation of 2,4-dinitrophenyl amino acids and dabsyl amino acids on (R)-and (S)-NEC-β-CD columns. For dansyl amino acids, only the inclusion complexation is the dominant factor. Three different chiral recognition models containing π-π interaction, inclusion complexation and hydrogen bonding were proposed for the separation of the 3,5-dinitrobenzoyl amino acid enantiomers, depending on the size and shape of amino acids.

정확성 평가결과에 따른 태권도 평원 품새 동작의 운동학적 분석 (Kinematic Analysis of Accuracy Evaluation of Pyeongwon Poomsae)

  • 조용명;류재균;김영숙
    • 한국운동역학회지
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    • 제25권4호
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    • pp.431-440
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    • 2015
  • Objective : The purpose of this study was to investigate the relations between accuracy score and the motions which are performed in PyeongWon Poomsae, thereby developing objectivity in accuracy evaluations for Poomsae competitions. Method : The subjects were six male Poomsae players (age: $21.2{\pm}1.17yrs$, height: $173.4{\pm}3.95cm$, weight: $67.7{\pm}7.65kg$). A three-dimensional motion analysis was performed on the subjects using six high-speed cameras (60 frames/sec) and subjects' performed motions were evaluated by 5 evaluators. The entire Pyeong Poomsae was divided into 13 events and 9 phases; there were three pairs of symmetric phases among them: front kick & turning side kick phases (3PH, 3-1PH), arm motion & stance phases (4PH, 4-1PH), side kick with Hakdari-stance phases (5PH, 5-1PH). Performance time, change and range of COM, height of vertex, and foot of side kicks were analysed. The Data was analysed utilizing correlation analysis. Results : There was a positive correlation between accuracy score and the difference between right and left range of COM (X direction) at 4PH (r=0.921, p=0.009). Conclusion : The results of our study indicate that it is necessary to consider some of objective criterion such as performance time, COM range, and symmetrical movements in accuracy evaluations of Poomsae competitions.

Mg-Zn-Y 합금에서 준결정 및 준결정 유사상 (Quasicrystals And Related Approximant Phases in Mg-Zn-Y)

  • 박은수;옥재범;김원태;김도향
    • Applied Microscopy
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    • 제32권1호
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    • pp.31-37
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    • 2002
  • [ $Mg_{68}Zn_{28}Y_4$ ] 합금의 응고 조직은 primary solidification phase, primary solidification phase로부터 성장된 ${\alpha}-Mg$ dendrite, 그리고 응고 말기에 형성된 eutectic structure의 세 가지형태 조직으로 구성되어져 있다. Primary solidification phase에는 매우 큰 정도의 phason strain이 존재하고 있으며, $a=27.2{\AA}\;and\;{\alpha}=63.43^{\circ}$의 격자상수를 갖는 1/1 rhombohedral approximant가 존재한다. 이와 같은 rhombohedral approximant의 구조는 six dimensional face centered hyper-cubic lattice에 phason strain을 도입함에 의해 얻어질 수 있다. Decagonal phase는 icosahedral phase로부터 방위 관계를 가지며 형성되며, $Mg_4Zn_7$는 decagonal phase로부터 방위관계를 가지며 성장한다. 이는 세 상간에 구조적 유사성이 존재하고 있음을 의미하며, 응고시 용질원자의 분배에 의해 이들 세 상이 순서대로 형성되어진다.

Exploring Teachers' Perceived Beliefs regarding Teaching Practice based on Lesson Study Context

  • Changsri, Narumon;Inprasitha, Maitree;Pattanajak, Auijit
    • 한국수학교육학회지시리즈D:수학교육연구
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    • 제16권1호
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    • pp.67-77
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    • 2012
  • This study aimed to explore teachers' perceived beliefs regarding teaching practice in the context of three-year Professional Development Project (ProDev) implementing lesson study incorporating Open Approach. The data were collected through questionnaire distributing to the teachers in three schools. Qualitative data were collected through participatory observation on teaching practice and interviewing members of lesson study team. The findings revealed that teacher's perceived beliefs regarding teaching practice could be categorized into three categories according to 3 phases of lesson study as the followings: 1) Perceived beliefs related to collaboratively designing research lessons 2) Perceived beliefs related to collaboratively observing their friend teaching the research lesson 3) Perceived beliefs related to collaboratively doing post-discussion or reflection on the activities of the two phases.

An Investigation about Dynamic Behavior of Three Point Bending Specimen

  • Cho, Jae-Ung;Han, Moon-Sik
    • 한국자동차공학회논문집
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    • 제8권4호
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    • pp.149-157
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    • 2000
  • Computer simulations of the mechanical behavior of a three point bend specimen with a quarter notch under impact load are performed. The case with a load application point at the side is considered. An elastic-plastic von Mises material model is chosen. Three phases such as impact bouncing and bending phases are found to be identified during the period from the moment of impact to the estimated time for crack initiation. It is clearly shown that no plastic deformation near the crack tip is appeared at the impact phase. However it is confirmed that the plastic zone near the crack tip emerges in the second phase and the plastic hinge has been formed in the third phase. Gap opening displacement crack tip opening displacement and strain rate are compared with rate dependent material(visco-plastic material). The stability during various dynamic load can be seen by using the simulation of this study.

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지리(地理) 정보(情報) 시스템을 위한 삼단계(三段階) 데이터베이스 설계(設計) (Three-Phase Database Design for a Geographic Information System)

  • 옥한석;김갑열;김창환;김상욱;신재호;양재웅
    • 산업기술연구
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    • 제18권
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    • pp.343-353
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    • 1998
  • Effective design of a database is essential for operating application systems efficiently. This paper discusses database design for a geographic information system. This goals of database design are multiple: to satisfy the information content requirements of the specified users and applications; to provide a natural and easy-to-understand structuring of the information; and to support processing requirements and any performance objectives such as response time, processing time, and storage space. Database design is a very complex process and is decomposed in three phases: conceptual, logical, and physical design. In this paper, we first collect and analyze the requirements for a geographic information system. We also perform database design for these requirements through the three design phases systematically. Our results would contribute to the effective construction of a database for a geographic information system.

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고농도 산소 공급량 변화에 따른 남/녀 혈중 산소 포화도의 차이 (Differences of Blood Oxygen Saturation between Male and Female due to Change of Supply Rate of Highly Concentrated Oxygen)

  • 이정한;최미현;김지혜;이수정;양재웅;정순철;임대운;이동형;민병찬
    • 산업경영시스템학회지
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    • 제32권4호
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    • pp.203-207
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    • 2009
  • The purpose of this study was to examine differences between male and female in blood oxygen saturation due to 93% oxygen administration of the three levels (1L/min, 3L/min, 5L/min). Ten healthy male ($25.0{\pm}1.8$ years) and ten female ($23.7{\pm}1.9$ years) college students were selected as the subjects for this study. The experiment consisted of three runs, i.e., the three levels of 93% oxygen administration, respectively. The each run consisted of three phases, i.e., Rest 1 (5 min), Hyperoxia (10 min), and Rest 2 (5 min). Blood oxygen saturation were measured throughout the three phases. By increasing the supply rate of highly concentrated oxygen, rising rate of blood oxygen saturation was increased. Blood oxygen saturation of female was higher than male regardless of supply rate of highly concentrated oxygen and phases.

Fault Tolerant Operation of CHB Multilevel Inverters Based on the SVM Technique Using an Auxiliary Unit

  • Kumar, B. Hemanth;Lokhande, Makarand M.;Karasani, Raghavendra Reddy;Borghate, Vijay B.
    • Journal of Power Electronics
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    • 제18권1호
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    • pp.56-69
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    • 2018
  • In this paper, an improved Space Vector Modulation (SVM) based fault tolerant operation on a nine-level Cascaded H-Bridge (CHB) inverter with an additional backup circuit is proposed. Any type of fault in a power converter may result in a power interruption and productivity loss. Three different faults on H-bridge modules in all three phases based on the SVM approach are investigated with diagrams. Any fault in an inverter phase creates an unbalanced output voltage, which can lead to instability in the system. An additional auxiliary unit is connected in series to the three phase cascaded H-bridge circuit. With the help of this and the redundant switching states in SVM, the CHB inverter produces a balanced output with low harmonic distortion. This ensures high DC bus utilization under numerous fault conditions in three phases, which improves the system reliability. Simulation results are presented on three phase nine-level inverter with the automatic fault detection algorithm in the MATLAB/SIMULINK software tool, and experimental results are presented with DSP on five-level inverter to validate the practicality of the proposed SVM fault tolerance strategy on a CHB inverter with an auxiliary circuit.