• 대한치과보철학회지
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• 제31권2호
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• pp.165-179
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• 1993

Dicor has not been prescribed routinely, in spite of many advantages, because of esthetic limitations by excessive translucency and external shading. In an attempt to solve these problems, the technique of veneering Dicor by aluminous poreclain has been used and recently Dicor Plus system was developed. The purpose of this study was to evaluate the compatibility between Dicor and several veneering porcelains by measuring the shear bond strength and observing the failure mode and interface appearance with SEM. Total 55 Dicor disks(10.0mm diam. X 3.0mm thickness) were fabricated by lost wax technique and divided into five groups of 11. Veneering porcelains such as Dicor Plus, Vitadur Alpha, Vitadur N, Vivodent, and Ceramco II were built up over the center of the treated Dicor surface using paper tube(5.0mm diam. X 4.0mm height) and fired according to the manufacturesr’instructions. A representative sample from each group was completely embedded in epoxy resin and crosssectioned, and remaining 50 samples were embedded in epoxy resin with the bonded area perpendicular to table base. The shear bond strengths were measured by applying the shear load parallel to Dicor surface close to the bonded area. Failure modes and interface appearances were observed using SEM at 15 and 1000 magnification respectively. The obtained results were as follows : 1. The mean shear bond strengths showed Dicor-Dicor Plus(10.53 MPa); Dicor-Vitadur Alpha(8.84 MPa); Dicor-Vitadur N(7.37 MPa); Dicor-Vivodent(4.28 MPa); Dicor-Ceramco II(0.89 MPa). 2. The shear bond strength of Dicor-CeramcoII was significantly decreased compared with Dicor-Dicor Plus(p<0.01), but had no significant difference compared with Dicor-Vivodent(p>0.01). 3. The shear bond strengths of Dicor-Vitadur Alpha and Dicor-Vitadur N were not significantly different compared with Dicor-Dicor Plus(p>0.01). 4. SEM examination of bond failure modes revealed that Dicor-Dicor plus, Dicor-Vitadur Alpha, Dicor-Vitadur N exhibited cohesive failure within Dicor and Dicor-Vivodent exhibited adhesive failure. And Dicor-Ceramco III exhibited adhesive failure and cohesive failure within CeramcoIII together. 5. SEM examination of interfaces revealed that Dicor-Dicor Plus exhibited the most tight contact and Dicor-Vitadur Alpha, Dicor-Vitadur N exhibited acceptible contacts. But Vivodent exhibited discontinuous gap and Ceramco II exhibited large continuous gap.

• Steel and Composite Structures
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• 제30권6호
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• pp.551-565
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• 2019

A total of 36 carbon steel and stainless steel bolted connections subjected to shear loading at different strain rates was experimentally investigated. The connection specimens were fabricated from carbon steel grades 1.20 mm G500 and 1.90 mm G450, as well as cold-formed stainless steel types EN 1.4301 and EN 1.4162 with nominal thickness 1.50 mm. The connection tests were conducted by displacement control test method. The strain rates of 10 mm/min and 20 mm/min were used. Structural behaviour of the connection specimens tested at different strain rates was investigated in terms of ultimate load, elongation corresponding to ultimate load and failure mode. Generally, it is shown that the higher strain rate on the bolted connection specimens, the higher ultimate load was obtained. The ultimate loads were averagely 2-6% higher, while the corresponding elongations were averagely 8-9% higher for the test results obtained from the strain rate of 20 mm/min compared with those obtained from the lower strain rates (1.0 mm/min for carbon steel and 1.5 mm/min for stainless steel). The connection specimens were generally failed in plate bearing of the carbon steel and stainless steel. It is shown that increasing the strain rate up to 20 mm/min generally has no effect on the bearing failure mode of the carbon steel and stainless steel bolted connections. The test strengths and failure modes were compared with the results predicted by the bolted connection design rules in international design specifications, including the Australian/New Zealand Standard (AS/NZS4600 2018), Eurocode 3 - Part 1.3 (EC3-1.3 2006) and North American Specification (AISI S100 2016) for cold-formed carbon steel structures as well as the American Specification (ASCE 2002), AS/NZS4673 (2001) and Eurocode 3 - Part 1.4 (EC3-1.4 2015) for stainless steel structures. It is shown that the AS/NZS4600 (2018), EC3-1.3 (2006) and AISI S100 (2016) generally provide conservative predictions for the carbon steel bolted connections. Both the ASCE (2002) and the EC3-1.4 (2015) provide conservative predictions for the stainless steel bolted connections. The EC3-1.3 (2006) generally provided more accurate predictions of failure mode for carbon steel bolted connections than the AS/NZS4600 (2018) and the AISI S100 (2016). The failure modes of stainless steel bolted connections predicted by the EC3-1.4 (2015) are more consistent with the test results compared with those predicted by the ASCE (2002).

• 한국마이크로전자및패키징학회:학술대회논문집
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• 한국마이크로전자및패키징학회 2005년도 ISMP
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• pp.201-212
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• 2005

[ $Epoxy/BaTiO_3$ ] composite embedded capacitor films (ECFs) were newly designed fur high dielectric constant and low tolerance (less than ${\pm}15\%$) embedded capacitor fabrication for organic substrates. In terms of material formulation, ECFs are composed of specially formulated epoxy resin and latent curing agent, and in terms of coating process, a comma roll coating method is used for uniform film thickness in large area. Dielectric constant of $BaTiO_3\;&\;SrTiO_3$ composite ECF is measured with MIM capacitor at 100 kHz using LCR meter. Dielectric constant of $BaTiO_3$ ECF is bigger than that of $SrTiO_3$ ECF, and it is due to difference of permittivity of $BaTiO_3\;and\;SrTiO_3$ particles. Dielectric constant of $BaTiO_3\;&\;SrTiO_3$ ECF in high frequency range $(0.5\~10GHz)$ is measured using cavity resonance method. In order to estimate dielectric constant, the reflection coefficient is measured with a network analyzer. Dielectric constant is calculated by observing the frequencies of the resonant cavity modes. About both powders, calculated dielectric constants in this frequency range are about 3/4 of the dielectric constants at 1 MHz. This difference is due to the decrease of the dielectric constant of epoxy matrix. For $BaTiO_3$ ECF, there is the dielectric relaxation at $5\~9GHz$. It is due to changing of polarization mode of $BaTiO_3$ powder. In the case of $SrTiO_3$ ECF, there is no relaxation up to 10GHz. Alternative material for embedded capacitor fabrication is $epoxy/BaTiO_3$ composite embedded capacitor paste (ECP). It uses similar materials formulation like ECF and a screen printing method for film coating. The screen printing method has the advantage of forming capacitor partially in desired part. But the screen printing makes surface irregularity during mask peel-off, Surface flatness is significantly improved by adding some additives and by applying pressure during curing. As a result, dielectric layer with improved thickness uniformity is successfully demonstrated. Using $epoxy/BaTiO_3$ composite ECP, dielectric constant of 63 and specific capacitance of 5.1nF/cm2 were achieved.

• 보존과학회지
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• 제32권3호
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• pp.377-384
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• 2016

철불의 개금 시 표면에 남아 있는 옻칠 제거 방법에는 물리적인 방법과 화학적인 방법을 사용하고 있으나, 표면 손상 및 약품 사용으로 인한 환경오염, 보존과학자의 건강에도 매우 유해하다. 그래서 본 연구에서는 비접촉식이고 친환경적인 Nd:YAG 레이저를 이용하여 옻칠 제거 실험을 실시하였다. 시편은 크기가 $5{\times}5cm$인 철제(Fe 99.9%)시편 표면을 균일하게 연마한 후 생칠을 도포 횟수를 달리하여 각각 $10{\mu}m$, $20{\mu}m$, $30{\mu}m$의 두께 차이로 제작하였다. 본 실험에서 사용된 레이저기기는 Nd:YAG 레이저로, 적외선 영역의 1064 nm(160~800 mJ)와 가시광선 영역인 532nm(50~350 mJ)의 두 가지 파장 모드를 이용하였다. 실험은 레이저 파장 에너지 조사 횟수 등에 따른 시편 표면의 변화를 조사하였다. 레이저 조사 전 후 표면을 실체현미경과 SEM 관찰, 비접촉 표면 조도 측정기, FT-IR 등을 이용하여 옻칠의 제거 및 잔류 여부를 알아보았다. 분석 결과 1064 nm 파장을 이용하여 $1.0J/cm^2$ 밀도에서 표면 손상 없이 $10{\mu}m$, $20{\mu}m$ 두께의 옻칠이 제거됨을 확인할 수 있었다. 이와 같은 결과를 통해 철불 개금 시 잔류하고 있는 옻칠 제거 방법으로 Nd:YAG 레이저가 효율적임을 본 실험을 통해 알 수 있었다. 향후 금속뿐만 아니라 목칠 가구 등 다양한 재질의 연구가 이루어지면 표면 손상 없이 옻칠을 제거 하는데 효과적으로 활용 가능할 것으로 본다.

• 한국전자파학회논문지
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• 제8권2호
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• pp.161-172
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• 1997

본 논문에서는 다충 유전체 위의 주기적인 도체 스트립 구조에 의한 전자파산란 문제를 Fourier-Galerkin 모멘트법으로 수치해석하여 정규화된 반사 및 투과전력을 계산하였다. 도체띠에 유도되는 전류밀도는 적절한 모서리 경계조건을 만족하는 함수와 l종 Chebyshev 다항식의 곱의 급수로 전개하였으며, 각유전체층의 경계 면에 서는 전자계 연속조건을 적용하였다. 산란 전자파는 Floquet 모드 함수를 이용하여 무한개의 급수로 전개하였다. 본 논문에서 제안된 방법의 타당성을 입증하기 위하여 각 유전체층의 비유전율과 두께를 변화시켜 얻어진 정규화된 반사 및 투과전력은 기존의 수치방법 및 논문의 결과와 평가 및 비교하였으며, 이 때 본 논문의 수치결과들은 기존의 수치방볍 및 논문의 결과와 매우 잘 일치하였다. 기하광학적 정규화된 반사 및 투과전력의 급변점 의 위치는 입사각 및 격자 주기 그리고 유전체충의 비유전율 및 두께에 따라 주된 영향을 받음을 알수 있었고, Wood의 변칙이라고 불리우는 이러한 급변점은 고차 모드의 반사전력이 전파모드와 감쇠모드 사이에서 모드 전환이 주된 요인으로 관측되었으며, 국부적인 최소 위치들은 유전체층의 비 유전율이 증가함에 따라 격자주기가 작아지는 좌측방향으로 약간 이동함을 알 수 있었다.

• 한국유변학회:학술대회논문집
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• 한국유변학회 2006년도 춘계 학술발표회 논문집
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• pp.81-84
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• 2006

Slot coating process, in continuous and patch modes, has been applied for the many precise coating products, e.g., flat panel displays and second batteries. However, manufacturing uniform coating products is not a trivial task at high-speed operations because various flow instabilities or defects such as leaking, bubbles, ribbing, and rivulets are frequently observed in this process. It is no wonder, therefore, that many efforts to understand the various aspects of dynamics and coating windows of this process have been made both in academia and industry. In this study, as the first topic, flow dynamics within the coating bead in slot coating process has been investigated using the one-dimensional viscocapillary model by lubrication approximation and two-dimensional model by Flow-3D software. Especially, operability windows in both 1D and 2D cases with various slot die lip designs have been successfully portrayed. Also, effects of process conditions like viscosity and coating gap size on slot coating window have been analyzed. Also, some experiments to find minimum coating thickness and coating windows have been conducted using slot die coater implemented with flow visualization device, corroborating the numerical results. As the second topic, flow dynamics of both Newtonian and Non-Newtonian fluids in patch or pattern slot coating process, which is employed in manufacturing IT products such as secondary batteries, has been investigated for the purpose of optimal process designs. As a matter of fact, the flow control in this system is more difficult than in continuous case because od its transient or time-dependent nature. The internal die and die lip designs for patterned uniform coating products have been obtained by controlling flow behaviors of coating liquids issuing from slot. Numerical simulations have been performed using Fluent and Flow-3D packages. Flow behavior and pressure distribution inside the slot die has been compared with various die internal shapes and geometries. In the coating bead region, efforts to reduce irregular coating defects in head and tail parts of one patterned coating unit have been tried by changing die lip shapes. It has been concluded that optimal die internal design gas been developed, guaranteeing uniform velocity distribution of both Newtonian and shear thinning fluids at the die exit. And also optimal die lip design has been established, providing the longer uniform coating layer thickness within one coating unit.

• 한국가스학회지
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• 제25권6호
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• pp.53-65
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• 2021

수소충전소의 빠른 확장 및 설치와 동시에 수소충전소의 고압수소 충전 압력용기에 대한 안전 검사가 매우 중요하게 이루어져야 한다. 이 중 ASME에 따르면 일정 압력 이상의 수소를 보관하는 용기에 대해서는 수소 취성 검사를 반드시 해야 한다. 수소취성 검사의 주된 시험방법으로 고압의 수소분위기에서 파괴시험 및 피로 파괴시험을 실시해야 하며, 이를 통해 수소 분위기에서 압력용기의 내구한계를 측정하고, 사용한계를 결정하도록 되어 있다. 세부적으로 stress intensity factor(K)로부터 한계균열깊이를 계산하고, da/dN(피로성장율)로부터 사용수명을 결정할 수 있다. API579-1/ ASME FFS-1 part 9에서 crack-like flaws의 모드에 따른 계산방법을 예시하고 있으나, 플레이트, 실린더 등 다양한 형태의 형상에 대하여 균열의 형상, 위치 등에 의하여 대략 55개 모드가 있고, 상당히 복잡한 수식으로 인하여 쉽게 접근을 못한다. 본 연구에서는 엑셀 및 VBA를 통하여 수치해석적으로 파괴역학계산하는 방법을 소개하고자 한다. 또한, 이를 적용하여 압력용기의 두께와 내경이 수명에 미치는 영향을 분석해 보았다.

• 한국강구조학회 논문집
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• 제25권1호
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• pp.15-24
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• 2013

본 논문은 반복하중을 받는 CFT 합성골조의 더블 웨브앵글 접합부의 휨모멘트 내력에 대해 체계적으로 수행된 유한요소 연구로부터 얻은 결과를 제시하고 있다. 합성 부분강접 CFT 접합부의 회전강성, 휨모멘트 내력 및 파괴모드를 연구하기 위하여 3차원 비선형 유한요소 해석이 수행되었다. 부가적인 다양한 구조적 거동은 앵글의 두께 및 고강도 강봉 게이지 거리로 더블 웨브앵글 접합부의 파라미터에 대한 영향을 설명하고 있다. 해석모델의 적합성은 정적 유한요소해석 결과로부터 얻은 모멘트-회전각 곡선을 Richard의 회귀분석을 통하여 비교 분석하였다.

• Structural Engineering and Mechanics
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• 제58권3호
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• pp.577-596
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• 2016

FRP-concrete interfacial mechanical properties determine the strengthening effect of RC beams strengthened with FRP. In this paper, the model experiments were carried out with eight specimens to study the failure modes and the strengthening effect of RC beams strengthened with FRP. Then a theoretical model based on interfacial performances was proposed and interfacial mechanical behaviors were studied. Finite element analysis confirmed the theoretical results. The results showed that RC beams strengthened with FRP had three loading stages and that the FRP strengthening effects were mainly exerted in the Stage III after the yielding of steel bars, including the improvement of the bearing capacity, the decreased ultimate deformation due to the sudden failure of FRP and the improvement of stiffness in this stage. The mechanical formulae of the interfacial shear stress and FRP stress were established and the key influence factors included FRP length, interfacial bond-slip parameter, FRP thickness, etc. According to the theoretical analysis and experimental data, the calculation methods of interfacial shear stress at FRP end and FRP strain at midspan were proposed. When FRP bonding length was shorter, interfacial shear stress at FRP end was larger that led to concrete cover peeling failure. When FRP was longer, FRP reached the ultimate strain and the fracture failure of FRP occurred. The theoretical results were well consistent with the experimental data.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.384.1-384.1
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• 2016

We reported that amorphous silicon (a-Si) thin film provide sample plate exhibiting a multimodality to measure biomolecules by secondary ion mass spectrometry (SIMS) and laser desorption/ionization mass spectrometry (LDI-MS). Kim et al.1 reported that a-Si thin film were suitable to detect small molecules such as drugs and peptides by SIMS and LDI-MS. Recently, bacterial identification has been required in many fields such as food analysis, veterinary science, ecology, agriculture, and so on.2 Mass spectrometry is emerging for identifying and profiling microbiology samples from its advantageous characters of label-free and shot-time analysis. Five species of bacteria - S. aureus, G. glutamicum, B. kurstaki, B. sphaericus, and B. licheniformis - were sampled for MS analysis without lipid extraction in sample preparation steps. The samples were loaded onto the a-Si thin film with a thickness of 100 nm which did not only considered laser-beam penetration but also surface homogeneity. Mass spectra were recorded in both positive and negative ionization modes for more analytical information. High reproducibility and sensitivity of mass spectra were demonstrated in a mass range up to mass-to-charge ratio(m/z) 1200 by applying the a-Si thin film in mentioned above MS. Principle component analysis (PCA) - a popular statistical analysis widely used in data processing was employed to differentiate between five bacterial species. The PCA results verified that each bacterial species were readily distinguished and differentiated effectively from our MS approach. It shows a new opportunity to rapid bacterial profiling and identification in clinical microbiology. More details will be discussed in the presentation.