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  • Title/Summary/Keyword: thermoluminescence (TL)

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Thermally assisted IRSL and VSL measurements of display glass from mobile phones for retrospective dosimetry

  • Discher, Michael;Kim, Hyoungtaek;Lee, Jungil
    • Nuclear Engineering and Technology
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    • v.54 no.2
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    • pp.429-436
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    • 2022
  • Investigations of retrospective dosimetry have shown that components of mobile phones are suitable as emergency dosimeters in case of radiological incidents. For physical dosimetry, components can be read out using optically stimulated luminescence (OSL), thermoluminescence (TL) and phototransferred thermoluminescence (PTTL) methods to determine the absorbed dose. This paper deals with a feasibility study of display glass from modern mobile phones that are measured by thermally assisted (Ta) optically stimulated luminescence. Violet (VSL, 405 nm) and infrared (IRSL, 850 nm) LEDs were used for optical stimulation and two protocols (Ta-VSL and Ta-IRSL) were tested. The aim was to systematically investigate the luminescence properties, compare the results to blue stimulated Ta-BSL protocol (458 nm) and to develop a robust measurement protocol for the usage as an emergency dosimeter after an incident with ionizing radiation. First, the native signals were measured to calculate the zero dose signal. Next, the reproducibility and dose response of the luminescence signals were analyzed. Finally, the signal stability was tested after the storage of irradiated samples at room temperature. In general, the developed Ta-IRSL and Ta-VSL protocols indicate usability, however, further research is needed to test the potential of a new protocol for physical retrospective dosimetry.

Detection of Gamma-irradiated Imported Foods (Perilla seeds, Almonds, and Soybeans) by Using PSL, TL, and ESR (PSL, TL 및 ESR 분석을 통한 수입산 들깨, 아몬드 및 대두의 방사선 조사 여부 판별 특성)

  • Han, In-Jun;Yoon, Young-Min;Choi, Soo-Jeong;Song, Beom-Seok;Kim, Jae-Kyung;Park, Jong-Heum;Lee, Ju-Woon;Kim, Jae-Hun;Kim, Kyu-Heon;Cho, Tae-Yong;Yoon, Hae-Sung;Han, Sang-Bae;Lee, Jung-Eun
    • Journal of Radiation Industry
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    • v.6 no.4
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    • pp.305-310
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    • 2012
  • This study examined radiation detection properties of imported perilla seeds, almonds, and soybeans. Food samples were irradiated at doses of 0.5, 1, 2, and 4 kGy and analyzed by photo-stimulated luminescence (PSL), thermoluminescence (TL), and electron spin resonance (ESR). The results of PSL showed that photon counts of irradiated perilla seeds and soybeans were 32,959counts60sec1 and 7,234counts60sec1, respectively, at an irradiation dose of 0.5 kGy, and the photon count of irradiated almonds was 5,581counts60sec1 at an irradiation dose of 1 kGy. The results of TL showed that this technique is useful for detecting irradiated samples; the TL ratios (TL1/TL2) measured for the food samples at an irradiation dose of 0.5 kGy were 0.2301 for perilla seeds, 0.4595 for almonds, and 0.4827 for soy beans. Lastly, results of ESR spectroscopy for only soybeans revealed specific signals derived from free radicals captured in the cellulose. In conclusion, PSL, TL, and ESR methods can be used for the detection of gamma-irradiated soybean samples, whereas gamma-irradiated perilla seeds and almonds can be confirmed by a serial detection with a TL method after PSL.

Absolute Age Determination of Gangmun-dong Sites Gangneung, Gangwon-Do-Radiocarbon and Thermoluminescence Dating - (강릉 강문동 유적의 절대연대측정 - 방사성탄소연대 및 열발광연대 -)

  • Kang, Hyung-Tae;Chung, Kwang-Yong
    • Journal of Conservation Science
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    • v.18 s.18
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    • pp.97-104
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    • 2006
  • Absolute ages for three pieces of organic materials such as wood and shell were determined with radio-carbon concentrations and two potsherds with thermoluminescence measurements. Radiocarbon contents of each sample were compared with those of modern standard oxalate(NBS SRM4990C) and calculated radiocarbon ages of them. Quartz grains with diameter of 90150μm were extracted from potsherds and used for measuring the archaeodose. Annual dose were calculated with measuring the alpha count rates and water contents and analysing K2O concentration of both potsherds and soils. Radiocarbon ages of organic materials were in the ranges of 42C BC and Quartz grain techniques for thermoluminescence dating showed 170 BC ud 210 BC respectively. It was found that the results of radiocarbon dating and TL dating were accorded with each other. But the deviations of TL dating have shown 13% and 20% respectively. It need to reduce the deviations.

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High Thermoluminescence Properties of Dy+Ce, and Dy+Na Co-Doped MgB4O7 for a Light Tracer Application (비화공식 예광탄 응용을 위한 Dy+Ce 및 Dy+Na 이중 도핑된 MgB4O7의 높은 열발광 특성)

  • Jinu Park;Nakyung Kim;Jiwoon Choi;Youngseung Choi;Sanghyuk Ryu;Sung-Jin Yang;Duck Hyeong Jung;Byungha Shin
    • Korean Journal of Materials Research
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    • v.33 no.1
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    • pp.15-20
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    • 2023
  • 'Tracers' are bullets that emit light at the backside so that the shooter can see the trajectory of their flight. These light-emitting bullets allow snipers to hit targets faster and more accurately. Conventional tracers are all combustion type which use the heat generated upon ignition. However, the conventional tracer has a fire risk at the impact site due to the residual flame and has a by-product that can contaminate the inside of the gun and lead to firearm failure. To resolve these problems, it is necessary to develop non-combustion-type tracers that can convert heat to luminance, so-called 'thermoluminescence (TL)'. Here, we highly improve the thermoluminescence properties of MgB4O7 through co-doping of Dy3++Ce3+ and Dy3++Na+. The presence of doping materials (Dy3+, Ce3+, Na+) was confirmed by XPS (X-ray photoelectron spectroscopy). The as-synthesized co-doped MgB4O7 was irradiated with a specific radiation dose and heated to 500 ℃under dark conditions. Different thermoluminescence characteristics were exhibited depending on the type or amounts of doping elements, and the highest luminance of 370 cd/m2 was obtained when Dy 10 % and Na 5 % were co-doped.

Quality Evaluation and Physical Identification of Irradiated Dried Fruits (감마선 조사 건조과일의 품질평가 및 물리적 판별)

  • Jung, Jae-Hoon;Jung, Yoonmi;Jo, Deokjo;Kwon, Joong-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.41 no.11
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    • pp.1559-1564
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    • 2012
  • Raisins (Thailand), dried mangos (Philippines), and dried figs (Iran) were gamma-irradiated (0~5 kGy), and their quality and detection characteristics were investigated. Microbiological characteristics were at safe levels when samples were irradiated at higher than 3 kGy. In color change after irradiation, dried mangoes were the most sensitive. Photostimulated luminescence (PSL) measurement was not applicable to dried fruits, showing negative or intermediate values for the irradiated samples. Thermoluminescence (TL) measurement was good for dried figs, exhibiting a glow curve in range of 150200C, where the signal intensity was dependent on the irradiation dose. Electron spin resonance (ESR) measurement was suitable for raisins and dried mangos, resulting in dose-dependent radiation-induced sugar radical signals.

Design of a Badge Filter System for Measurement of Hp(10) with the New Type of TL Dosimeter CaSO4:Dy,P (신형 TL 선량계인 CaSO4:Dy,P를 이용한 Hp(10) 측정용 배지의 필터체계 설계)

  • Kim, H.K.;Kwon, J.W.;Lee, J.K.;Kim, J.L.
    • Journal of Radiation Protection and Research
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    • v.28 no.2
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    • pp.79-85
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    • 2003
  • This study was intended to estimate Hp(10) recommended by the ICRU using the CaSO4:Dy,P element developed in the KAERI. For the estimation of Hp(10), TL response should be compensated properly through the energy range using filter materials since CaSO4:Dy,P is of severe photon energy dependent response. Various experiments and computations using Monte Carlo Code were carried out for designing filter satisfying the performance requirements of the ISO related to TL dosimeter. Under the completed filter, the relative response of CaSO4:Dy,P showed 0.751.0 for photons in the range of 20662keV. Especially it was possible to reduce the thickness of front filter and simplify the filter combination with rear filter of larger diameter and to considerably improve angular dependence by introducing taper to the filler.

Monitoring microbiological contamination, pre-decontamination, and irradiation status of commercial dried laver (Porphyra sp.) products (시판 유통 김의 미생물 오염도, 사전 살균처리 및 전자선 조사 여부 확인)

  • Lee, Eun-Jin;Kim, Gui-Ran;Lee, Hye-Jin;Kwon, Joong-Ho
    • Korean Journal of Food Science and Technology
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    • v.49 no.1
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    • pp.20-27
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    • 2017
  • Eighteen commercial laver (Porphyra sp.) products were purchased from Korean market and were monitored for their microbial contamination, pre-decontamination, and luminescence properties. The laver samples showed considerable variation in their microbial contamination, from 10107CFU/g of total aerobic counts, <10102CFU/g of coliforms in 4 dried laver samples, and <10106CFU/g of yeasts and molds except in 3 samples. In addition, 102CFU/g of Bacillus cereus was found in one sample. DEFT/APC analysis was suitable for demonstrating whether the samples were pre-decontaminated or not, with DEFT/APC values lower than 2.0 log for non-heated samples and 1.0-8.5 log for heatprocessed samples. In photostimulated luminescence (PSL) calibration, 15 samples irradiated at 1 kGy showed positive (irradiated) values more than 5000 PCs. Furthermore, thermoluminescence (TL) analysis by separating the marker minerals from samples revealed the potential to be employed in identifying irradiation status by determining 1st TL glow at 125175C and TL ratio (TL1/TL2) of all the samples.

Study on Application of the Physical Detection Methods for Electron Beam-Irradiated Agricultural Products (전자선 조사된 농산물의 물리적 검지 방법의 적용에 관한 연구)

  • Kim, Dong Yong;Park, Yong Dae;Jin, Chang Hyun;Choi, Dae Seong;Yook, Hong-Sun;Jeong, Il Yun
    • Journal of Radiation Industry
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    • v.4 no.3
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    • pp.221-226
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    • 2010
  • Physical detection methods, photostimulated luminescence (PSL), thermoluminescence (TL) and electron spin resonance (ESR) were applied to detect electron beam-irradiated agricultural products, such as red pepper, black pepper, raisin, walnut, beef seasoning and pistachio. The absorbed irradiation doses for representative samples were controled at 0, 1, 3, 5 and 10 kGy. PSL values for non-irradiated samples were <700 counts/60s (lower threshold, T1) except beef seasoning, whereas those of irradiated samples were more than 5,000 photon counts, upper threshold (T2) in black pepper, raisin, and beef seasoning and intermediates values of T1T2 in red pepper, walnut, and pistachio. Minerals seperated from the samples for TL measurement showed that non-irradiated samples except pistachio (TL ratio, 0.12) were characterized by no glow curves situated at temperature range of 50400C with TL ratio (0.01~0.08), while irradiated samples except pistachio at only 1 kGy (TL ratio, 0.08) indicated glow curve at about 150250C with TL ratio (0.28~3.10). ESR measurements of irradiated samples showed any specific signals to irradiation. The samples of both red pepper and pistachio were produced specific signals derived from cellulose radicals as well as single line signals for black pepper and walnut, and multiple signals derived from crystalline sugar radicals for raisin and beef seasoning. In conclusion, The ESR methods can apply for detection of pistachio exposed to electron beam but PSL and TL are not suitable methods. Furthermore, TL and ESR suggeted that both techniques were more useful detection method than PSL to confirm whether red pepper, walnut and beef seasoning samples have been exposed to electron beam.

A Study of Fundamental Characteristics for Mg2SiO4 : Tb Phosphor (Mg2SiO4 : Tb 소자의 기본 특성에 관한 연구)

  • Park, Myeong-Hwan;Park, Chong-Sam;Kwon, Duk-Moon;Lee, Joon-Il
    • Journal of radiological science and technology
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    • v.19 no.2
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    • pp.79-83
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    • 1996
  • The thermoluminescence(TL) response in changing annealing condition, triboluminescence, and darkroom temperature for Mg2SiO4:Tb phosphor are examined. The experimental results are summerized as follows : 1. The uniformity of TL intensity is better In the disinfected Mg2SiO4 : Tb than in contaminated one. 2. The triboluminescence of Mg2SiO4 : Tb is almost not detected even if numbers of Mg2SiO4 : Tb falling are increased. 3. The fading effect of Mg2SiO4 : Tb is scarcely affected by freezing room. The followings are resulted from the study. The disinfected Mg2SiO4 : Tb phosphor should be used in the dose measurement and the immediate reading for Mg2SiO4 : Tb after exposure is better. And if the reading is not immediately taken, a law darkroom temperature for Mg2SiO4 : Tb storage is recommended.

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Detection Characteristics of Gamma-Irradiated Korean Medicinal Herbs by Using PSL, TL, and ESR (PSL, TL 및 ESR 분석에 의한 감마선 조사 한약재의 검지 특성)

  • Yang, Hee-Sun;Park, Yong-Dae;Jin, Chang-Hyun;Choi, Dae-Seong;Chung, Hyung-Wook;Byun, Myung-Woo;Jeong, Il-Yun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.37 no.11
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    • pp.1529-1533
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    • 2008
  • The detection characteristics of gamma-irradiated (010.0kGy) medicinal herbs (Platycodon grandiflorum, Acanthopanax chiisanensis) were investigated by photostimulated luminescence (PSL), thermoluminescence (TL), and electron spin resonance (ESR). The results of the PSL, a first screening method in comparison with the TL, showed photon counts greater than 5,000 counts/60 s (positive) in the irradiated samples, while the non-irradiated samples yielded photon counts less than 700 counts/60 s (negative). The TL was also applied for the detection method of irradiated medicinal herbs and showed that the non-irradiated sample revealed a glow curve with a low intensity, while the irradiated samples showed a higher intensity. These results were normalized by re-irradiating the mineral grains with a irradiation dose of 1.0 kGy, and a second glow curve was recorded. The ratio of the intensity of the first glow curve (TL1) to that after the normalization dose (TL2) was determined and compared with the recommended threshold values. TL ratio (TL1/TL2) was below 0.007 for the non-irradiated sample and higher than 0.1 for all irradiated samples (above 1.0 kGy). ESR spectroscopy revealed specific signals (6.065 mT) derived from free radicals in cellulose containing irradiated medicinal herbs. The P. grandiflorum showed clearer signals than A. chiisanensis. From the results of our studies, the PSL, TL, and ESR determinations were found to be suitable for the detection of irradiated medicinal herbs such as P. grandiflorum and A. chiisanensis.