• Title/Summary/Keyword: thermal gel

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Effect of Bicarbonate and Phosphate Buffer Treatments on the Structure and Thermal Stability of Spent Layer Meat (중 탄산 및 인산염 완층액 처리가 노계육의 조직구조 및 열안정성에 미치는 영향)

  • Yi, Song-Sop;Mast, Morris G.
    • Korean Journal of Food Science and Technology
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    • v.23 no.6
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    • pp.695-701
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    • 1991
  • Spent layer breast meat and leg meat samples washed with 0.05 M sodium bicarbonate solution and 0.04 M phosphate buffer(pH 8.3) showed decreases in heat denaturation temperature indicating the destabilization of myofibrillar proteins. The destabilization was attributed to the solubilization of 95 Kdalton and 55 kdalton proteins from the myofibrils observed in gel-electrophoretograms. Transmission electron microscopy further indicated the breakage of Z-lines.

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Ferroelectric Properties of Hetero-Junction SrBi$_2Ta_2O_9$/Pb(Zr,Ti)O$_3$ (이종접합 SrBi$_2Ta_2O_9$/Pb(Zr,Ti)O$_3$박막 케패시터의 강유전 특성)

  • 이광배;김종탁
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.04a
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    • pp.217-221
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    • 1997
  • We have investigated the ferroelectric properties of multi-layered SrBi$_2$Ta$_2$$O_{9}$Pb(Zr,Ti)O$_3$, SBT/PZT, thin film capacitors. Specimens were prepared onto Pt-coated Si wafer by sol-gel method. Ferroelectric properties of these finns could be obtained only for thin SBT layers below 50nm in thickness. The values of dielectric constant and remnant polarization depend mainly on the thickness of SBT layer, which arises from the paraelectric interface layer between SBT and PZT due to the thermal diffusion of Pb. The value of remnant poarization of PZT/SBT is greater than that of SBT, and the plarization fatigue behaviors of PZT/SBT/Pt capacitors are somewhat improved as compared with those of PZT/Pt.t.

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Properties of Spin-On-Glass Siloxane Thin Films Fluorine-doped by CF$_4$ Plasma (CF$_4$ 플라즈마 처리로 불소를 첨가한 실록산 Spin-On-Glass 박막의 특성)

  • 김현중;김기호
    • Journal of the Korean institute of surface engineering
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    • v.34 no.3
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    • pp.258-263
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    • 2001
  • Siloxane thin films were fabricated on a silicon wafer by spin-coating using a siloxane solution made by the sol-gel process. Fluorine was doped using$ CF_4$ plasma treatment. The film was then annealed in-situ state in the nitrogen atmosphere. In order to examine the influence of annealing and fluorine doping on the siloxane thin film, thermogravimetric-differential thermal analysis (TG-DTA), Fourier transform-infrared spectroscopy (FT-IR) and X-ray photoelectron spectroscopy (XPS) were used and the dielectric constant was determined by the high-frequency capacitance-voltage method. Stable siloxane films could be obtained by in-situ annealing in a nitrogen atmosphere after $CF_4$ plasma treatment, and the dielectric value of the film was $\varepsilon$ 2.5.

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Characterization of Cordierite by SEM, Microanalysis X and TEM (SEM, X선 마이크로 분석기, TEM에 의한 코디에라이트의 특성 연구)

  • Han, Byoung-Sung
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.27 no.8
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    • pp.1250-1254
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    • 1990
  • The cordierite (MgO, SiO2, Al2O3) is of great interest for microelectronic packaging of integrated circuits. Its main advantages are low dielectric constant and low thermal expansion. The cordierite precursor is obtained by sol-gel synthesis using organic and inorganic compounds. The obtained cordierite precursor is an amorphous state at about 900\ulcorner. Green and fired cordierite samples were studied by SEM. Microanalysis X and TEM for microscopic properties. The fired cordierite shows forte diminution of Mg in comparison with its value at volume and the deficit of Mg compensates by sugmentation of Al and Si \ulcornercordierite and \ulcornercordierite are present near the surface (< 100) and small quantities of magnesium aluminate (MgAl2O4)is presented spinnel phase.

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Studies of the Mullite-Cordierite Composites as a Substrate Material (기판재료로서의 물라이트-코디어라이트 복합재료에 관한 특성)

  • 김경용;김윤호;정형진;김석수;김병호
    • Journal of the Korean Ceramic Society
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    • v.27 no.3
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    • pp.394-400
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    • 1990
  • Mullite and cordierite were prepared by the sol-gel route. Boehmite, fumed silica and Mg(NO3)2$.$6H2O were their starting materials. Mullite and cordierite powder were mixed by various weight percent. These mixed sols were ball-milled for 48hrs, dried at 100$^{\circ}C$, pressed, cold isostatic pressed and sintered at 1490$^{\circ}C$ for 2hrs. Mullite-cordierite composites sintered at 1490$^{\circ}C$ for 2hrs had>98% of theoretical density. Bending strength of the sintered bodies were 329-249MPa, dielectric constant 7.1-6.7 at 1MHz and thermal expansion coefficient at 800$^{\circ}C$ was matched with Si in the range of 30-35wt% cordierite.

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Construction and Evaluation of $O_3$ Condensation System for Oxide Thin Film (산화 박막 성장을 위한 $O_3$ 농축 시스템의 구축 및 평가)

  • Lim, Jung-Kwan;Ryu, Sun-Jong;Park, Yong-Pil
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.1192-1195
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    • 2003
  • A highly condensed ozone gas be transferred to the superconductor thin film growth chamber because ozone is strong oxidizing gas. In order to obtain high quality oxide thin films, higher ozone concentration is necessary. In this paper an ozone condensation system was evaluated from the viewpoint of an ozone supplier for oxide thin film growth. Ozone was condensed by an adsorption method and the ozone concentration reached 8.5 mol% in 2.5 h after the beginning of the ozone condensation process, indicating high effectiveness of the condensation process. Ozone was continuously desorbed from the silica gel by the negative pressure.

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Microstructure and Magnetic State of Fe3O4-SiO2 Colloidal Particles

  • Kharitonskii, P.V.;Gareev, K.G.;Ionin, S.A.;Ryzhov, V.A.;Bogachev, Yu.V.;Klimenkov, B.D.;Kononova, I.E.;Moshnikov, V.A.
    • Journal of Magnetics
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    • v.20 no.3
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    • pp.221-228
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    • 2015
  • Colloidal particles consisted of individual nanosized magnetite grains on the surface of the silica cores were obtained by two-stage sol-gel technique. Size distribution and microstructure of the particles were analyzed using atomic force microscopy, X-ray diffraction and Nitrogen thermal desorption. Magnetic properties of the particles were studied by the method of the longitudinal nonlinear response. It has been shown that nanoparticles of magnetite have a size corresponding to a superparamagnetic state but exhibit hysteresis properties. The phenomenon was explained using the magnetostatic interaction model based on the hypothesis of iron oxide particles cluster aggregation on the silica surface.

Characterization of Phase Change Materials for Textiles (옥타데칸, 노나데칸 마이크로캡슐 처리직물의 축열.방열 특성)

  • Go, Jae-Hun;Kim, So-Jin;Park, Yun-Cheol
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2008.10a
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    • pp.151-152
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    • 2008
  • PCM has the ability to change their state, these materials absorb energy during the heating process as a body contact and release energy during a reverse cooling process as phase change take place. Using the thermal energy storage of PCM which has a melting point 15 to $35^{circ}C$ is one of the most effective ideas for utilization in textile finish. In this study, microencapsulated PCM(MCPCM) were synthesized by sol-gel method using the octadecane(or nonadecane) as PCM and the silica as microcapsule materials. To develop smart temperature adaptable textile, coating process was applied to textile substrate using a composition included MCPCM.

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Shape-Stabilized Phase Change Materials : Frozen Gels From Polypropylene and n-Paraffin for Latent Heat Storage

  • Kim, Jong-Hwan;Ko, Jae-Wang;Son, Tae-Won
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2009.03a
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    • pp.120-121
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    • 2009
  • We prepared polymer-PCM gels such as prepared frozen gel from polypropylene and n-Paraffin for thermal storage and release materials, their basic properties and possible applications especially in latent heat storage. The preparation methods are used to melting method and absorption method respectively. The composition and properties of prepared frozen gels from polypropylene and n-Paraffin were observed by DSC, FT-IR spectra, ARES and Elemental analysis. We can prepare frozen gels in different temperature for latent heat storage materials as controlling composition of phase change material as well as using different incorporating phase change materials. These frozen gels can be used to latent heat storage materials for several applications.

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Fluorescence Spectroscopic and Atomic Force Microscopic Studies on the Microstructure of Polyimide/Silica-Titania Ternary Hybrid Composites

  • Park, Hae-Dong;Ahn, Ki-Youl;Mohammad A. Wahab;Jo, Nam-Ju;Kim, Il;Kim, Gyuhyun;Lee, Won-Ki;Ha, Chang-Sik
    • Macromolecular Research
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    • v.11 no.3
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    • pp.172-177
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    • 2003
  • Biphenyltetracarboximide-phenylene diamine polyimide/silica-titania ternary hybrid composites were Prepared by thermal imidization and sol-gel reaction. Fluorescence spectroscopic, scanning electron microscopy, and atomic force microscopy studies revealed that the addition of small amount of titania showed profound effects on the microstructure and photophysical behaviors of polyimide/silica hybrid composites, when the content of silica-titania mixture was small or when the ratio of silica to titania in the mixture was high.