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http://dx.doi.org/10.4283/JMAG.2015.20.3.221

Microstructure and Magnetic State of Fe3O4-SiO2 Colloidal Particles  

Kharitonskii, P.V. (Saint Petersburg Electrotechnical University "LETI")
Gareev, K.G. (Saint Petersburg Electrotechnical University "LETI")
Ionin, S.A. (Saint Petersburg Electrotechnical University "LETI")
Ryzhov, V.A. (National Research Centre "Kurchatov Institute")
Bogachev, Yu.V. (Saint Petersburg Electrotechnical University "LETI")
Klimenkov, B.D. (Saint Petersburg Electrotechnical University "LETI")
Kononova, I.E. (Saint Petersburg Electrotechnical University "LETI")
Moshnikov, V.A. (Saint Petersburg Electrotechnical University "LETI")
Publication Information
Journal of Magnetics / v.20, no.3, 2015 , pp. 221-228 More about this Journal
Abstract
Colloidal particles consisted of individual nanosized magnetite grains on the surface of the silica cores were obtained by two-stage sol-gel technique. Size distribution and microstructure of the particles were analyzed using atomic force microscopy, X-ray diffraction and Nitrogen thermal desorption. Magnetic properties of the particles were studied by the method of the longitudinal nonlinear response. It has been shown that nanoparticles of magnetite have a size corresponding to a superparamagnetic state but exhibit hysteresis properties. The phenomenon was explained using the magnetostatic interaction model based on the hypothesis of iron oxide particles cluster aggregation on the silica surface.
Keywords
magnetite; silica; colloidal particles; superparamagnetism; longitudinal nonlinear response; magnetostatic interaction;
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