• Title/Summary/Keyword: thermal evaporation

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A Study on Development of PLD Process for PM OLED Device Manufacture (PM OLED 디바이스 제작을 위한 PLD 공정 개발에 관한 연구)

  • Lee, Eui-Sik;Lee, Byoung-Wook;Kim, Chang-Kyo;Hong, Jin-Su;Park, Sung-Hoon;Moon, Soon-Kwun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.264-266
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    • 2005
  • Manufacture of OLED device used thermal evaporation method. However thermal evaporation method has many defect as thermal damage of substrate, difficult of dopant rate control and low utilization of organic materials. so we suggest PLD(Pulsed Laser Deposition) method that solution of these problems. PLD method has many advantage as without thermal damage, easy indicate of deposition rate per one pulse and good utilization of organic materials. In this paper we apply the PLD method for manufacture of device so we present high efficiency device manufacture using PLD method that has good deposition uniformity, surface rough and deposition rate.

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Different morphologies of three dimensional ZnO structures synthesized by thermal evaporation method without a catalyst (촉매를 사용하지 않는 열 기화법으로 다양한 형태의 ZnO 3차원 구조체 합성)

  • Bang, Sin Young;Tran, Van Khai;Oh, Dong Keun;Maneeratanasarn, Prachuporn;Choi, Bong Geun;Ham, Heon;Kim, Kyoung Hun;Shim, Kwang Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.23 no.1
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    • pp.8-13
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    • 2013
  • ZnO with different morphologies can be used various application depending on their shapes. Different morphologies of ZnO structures were synthesized by a catalysis-free thermal evaporation process. Their morphologies were dependent on the distance from the source to substrate on the same processing condition; in the result were products morphologies of the hollow, cage and star. Their shapes and crystalinity were evaluated by SEM and XRD, respectively. This work demonstrates what kind of growth factors would be involved in the final structure morphologies.

Structural characteristics of ZnO nanostructures synthesized by the thermal evaporation method (열증착법으로 합성된 ZnO 나노 구조체의 구조적 특성)

  • Bang, Sin-Young;Kim, Woo-Sik;Chung, Jun-Ho;Choi, Bong-Geun;Shim, Kwang-Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.2
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    • pp.81-86
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    • 2008
  • ZnO nanowires were synthesized by the thermal evaporation method and their growth mechanisms were confirmed by the characterization of the structural features depending on the growth conditions. The increase of vaporization temperature accelerates the growth rate and morphologies of ZnO nanowires were drastically changed at the temperature over 1000$^{\circ}C$, because of changed $CO/CO_2$ partial pressure. Au particles play their role on growth of ZnO nanowire as catalyst at growth temperature over 700$^{\circ}C$. The synthesized ZnO nanowires exhibit blue emission at 380 nm.

Microstructure and CO Gas Sensing Properties of Ag-CuO-SnO2 Thin Films Prepared by Co-Evaporation and Thermal Oxidation (공증발과 열산화로 제조한 Ag-CuO-SnO2 박막에서 미세조직과 CO 가스 감지특성)

  • Ji, In-Geol;Han, Kyu-Suk;Oh, Jae-Hee;Ko, Tae-Gyung
    • Journal of the Korean Ceramic Society
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    • v.46 no.4
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    • pp.429-435
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    • 2009
  • In this study, we investigated microstructure and the CO gas sensing properties of Ag-CuO-$SnO_2$ thin films prepared by co-evaporation and subsequently thermal oxidation at air atmosphere. The sensitivity of a Cu-Sn films, thermally oxidized at $600^{\circ}C$, is strongly affected by the amount of Cu. At Cu:7 wt%-Sn:93 wt%, the film exhibited a maximum sensitivity of ${\sim}2.3$ to CO gas of 1000 ppm at $300^{\circ}C$. In contrast, the sensitivity of a Sn-Ag film did not change significantly with the amount of Ag. An enhanced sensitivity of ${\sim}3.7$ was observed in the film with a composition of Ag:3 wt%-Cu:4 wt%-Sn:93 wt%, when thermally oxidized at $600^{\circ}C$. In addition, this thin film shows a response time of ${\sim}80$ sec and a recovery time of ${\sim}450$ sec to 1000 ppm CO gas. The results demonstrate that the CO sensitivity of the Ag-CuO-$SnO_2$ thin films may be closely associated with coexistence of $SnO_2$ and SnO phase, decrease in average particle size, and a porous microstructure. We also suggest that co-evaporation and followed by thermal oxidation is a very simple and effective method to prepare oxide gas sensor thin films.

Effect of Refrigerated and Thermal Storage on the Volatile Profile of Commercial Aseptic Korean Soymilk

  • Kim, Hun;Cadwallader, Keith R.;Jeong, Eun-Jeong;Cha, Yong-Jun
    • Preventive Nutrition and Food Science
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    • v.14 no.1
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    • pp.76-85
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    • 2009
  • This study determined the effect of refrigerated and thermal storage on the volatile profile of commercial aseptic soymilk. Volatile components in commercial aseptic soymilk stored either under refrigerated ($4^{\circ}C$) or thermal ($55^{\circ}C$) conditions for 30 days were periodically analyzed by combined solvent-assisted flavor evaporation-gas chromatography-mass spectrometry (SAFE-GC-MS). The concentrations of most of the volatile components, including aldehydes, ketones, alcohols, acids, nitrogen- and sulfur-containing compounds, alkylfurans, furan derivatives and phenolic compounds, were affected to a greater extent by thermal storage compared with refrigerated storage. Profound increases in some volatile compounds with low odor detection thresholds, such as hexanal, octanal, (E)-2-octenal, (E,E)-2,4-decadienal, 1-octen-3-ol, 3-ethyl-2,5-dimethylpyrazine, 2,3-diethyl-5-methylpyrazine, 2-pentylfuran, 4-hydroxy-2,5-dimethyl-3(2H)-furanone, dimethyl trisulfide, guaiacol, 4-vinylguaiacol and 4-vinylphenol, were observed in thermal stored soymilk. The volatile profile changes caused by thermal storage may influence the aroma quality of thermal-stored aseptic soymilk.

A Study on the growth of Si(001)/X(500$\AA$)/Zn(1000$\AA$) double layers deposited by thermal evaporation process. (열증착방법에 의해 제조된 Si(100)/X(500$\AA$)/Zn(1000$\AA$) 이중박막 성장에 관한 연구)

  • 신동원;정순종;이동윤;민복기;정원섭;송재성
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.1026-1029
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    • 2001
  • Zinc films have been deposited onto various buffer layers, Al, Al-Cu, Ag and Ag-Al, by vacuum evaporation method in order to investigate the film microstructure and its consequence on the film growth. Zn films were grown onto Al buffer layers with faster rates than on Ag buffer layers, because of the presence of preferred growth orientation. Especially, in the Zn film formation on the Ag layers, intermetallic compounds AgZn was formed to cause the different growth orientation from Zn film obtained on the Al layers.

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Thermal Analysis of a Liquid Hydrogen Vessel (액체수소 저장용기의 열해석)

  • Kim, Seo Young;Kang, Byung Ha
    • Transactions of the Korean hydrogen and new energy society
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    • v.8 no.2
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    • pp.57-65
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    • 1997
  • Thermal analysis has been performed to design a high-performance $LH_2$ vessel with about 1% per day evaporation loss. Analysis includes the combined insulations of MLI(Multi-Layer Insulation) and VCS (Vapor-Cooled Shield) under high vacuum. Combined insulation of MLI and VCS shows the existence of optimal location of VCS to minimize evaporation loss. Comparison of parallel-type DVCS (Double Vapor-Cooled Shield) and serial-type DVCS is also made to show the effectiveness of the system. The results indicate that the serial-type DVCS vessel is better than the parallel-type DVCS vessel with respect to overall evaporation loss. The combined insulation of SVCS (Single Vapor-Cooled Shield) with a partial MLI can give a similar performance characteristics compared to that with MLI and DVCS.

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Simulation of Physical Chemistry Phenomena Inside a Naturally Smoldering Cigarette (자연 연소중인 궐련내에서 일어나는 물리화학적 현상의 시뮬레이션)

  • 오인혁;김기환;정경락
    • Journal of the Korean Society of Tobacco Science
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    • v.20 no.1
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    • pp.87-94
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    • 1998
  • After we made the computer source code with mathematical model of Muramatsu et al. that was expressed by the set of simultaneous first-order ordinary differential equations in evaporation-pyrolysis zone of cigarette, we simulated the distribution profiles of temperature and density of flue-cured tobacco. Those equations were solved numerically with the Runge-Kutta-Gill algorithm assuming step size of 0.025mm by Muramatsu at at,, but in this study the advanced algorithm of Runge-Kutta 4th Order assuming step size of 0.0005mm. The initial conditions and physical parameters of Muramatsu et at. were used for solving them. The calculated values corresponded well with results of Muramatsu et al., especially the gradient of the temperature profile increased with smoldering speed and the thickness of the evaporation-pyrolysis zone decreased with increasing of smoldering speed. On the other hand, the temperature gradient decreased with increasing of the effective thermal-conductivity value and the thickness of the evaporation-pyrolysis zone increased with the effective thermal-conductivity value.

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Thermal Analysis of Reinforced Concrete Members at High Temperature (고온하에서 철근콘크리트부재의 온도해석)

  • Lee, Tae-Gyu
    • Proceedings of the KSR Conference
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    • 2008.11b
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    • pp.1102-1105
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    • 2008
  • In this paper, the prediction method of internal temperature for high strength concrete members at high temperature is presented. Finite element method is employed to facilitate thermal analysis for any position of member. In case of water evaporates inside the concrete member by high temperature, the evaporation heat that absorb surrounding temperature is occurred. This effect of the evaporation heat is applied. And the model equations of the material characteristics of high strength concrete by high temperature are proposed. To demonstrate the validity of this numerical procedure, the prediction by the proposed algorithm is compared with the test results of other researchers. The proposed algorithm is good agreement with experimental results including the phenomenon that temperature by the evaporation heat is lost.

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