• Title/Summary/Keyword: thermal cycles

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AN EXPERIMENTAL STUDY ON THE MEASUREMENT OF MARGINAL LEAKAGE USING A NEUTRON ACTIVATION ANALYSIS (Neutron Activation Analysis를 이용한 Composite Resin의 변연누출 측정에 관한 실험적 연구)

  • Kim, Mi-Ja;Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.13 no.1
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    • pp.185-190
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    • 1988
  • The study was designed to establish quantitative method for assessing the marginal leakage of dental restorations. 18 Class V cavities with $45^{\circ}$ bevel joint were prepared and replicas of these teeth were made with polyethylene wax. and classified with three groups. First group was filled with Scotch bond and silux. Second group was filled with glass ionomer cement:scotchbond/silux. Third group was filled with Dentin-Adhesit/Heliosit. After finishing, all specimens were subjected manually to 100 thermal cycles at $0^{\circ}C$ and $100^{\circ}C$ Samarium nitrate solution, irradiated with flux of $6{\times}12^{12}$ neutrons/$cm^2$/sec for 11 hours, woled for 200 hours, counted with the HpGe detector and the tracer uptake was determined by comparison with a standard of samarium ($10{\mu}g$). The following results were obtained. 1) The group filled with glass ionomer cement base showed least marginal leakage. 2) The group filled with Dentin-Adhesit/Heliosit showed less marginal leakage than the group filled with scotchbond/silux.

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AN EXPERIMENTAL STUDY ON THE MEASUREMENT OF MARGINAL LEAKAGE USING A RADIOACTIVITY (충전후 방사능에 의한 변연누출 측정에 관한 실험적 연구)

  • Kim, Mi-Ja;Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.13 no.1
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    • pp.69-78
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    • 1988
  • The study was designed to establish a more nearly quantitative method for assessing the marginal leakage of dental restorations. 27 Class V cavities with $45^{\circ}$ bevel joint were prepared and classified into 2 groups. One group was filled with Scotchbond and silux. The other group was filled with glass ionomer cement, Scotchbond and silux. After finishing, all specimens were subjected manually to 100 thermal cycles at $0^{\circ}C$ and $100^{\circ}C$ water-bath. They were soaked in a samarium nitrate solution for 3 hours, irradiated with flux of $6{\times}10^{12}$ neutrons/$cm^2$/sec for 11 hours, cooled for 200 hours, counted with the HPGE detector and the tracer uptake was determined by comparison with a standard of samarium (10 ${\mu}g$). The following results were obtained. 1. Both of the two groups showed a considerable amounts of marginal leakage. 2. The group filled without glass ionomer cement base showed more marginal leakage than the group filled with glass ionomer cement base. 3. Neutron Activation Analysis produced a good quantitative method to measure the marginal leakage and samarium was appropriate to measure the marginal leakage of resin restorations using neutron activation analysis.

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Backstepping Control for Multi-Machine Web Winding System

  • Bouchiba, Bousmaha;Hazzab, Abdeldjebar;Glaoui, Hachemi;Med-Karim, Fellah;Bousserhane, Ismail Khalil;Sicard, Pierre
    • Journal of Electrical Engineering and Technology
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    • v.6 no.1
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    • pp.59-66
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    • 2011
  • This work treat the modeling and simulation of non-linear dynamic behavior of a web winding process during traction. We designate by a winding process any system applying the cycles of unwinding, transport, treatment, and winding to various flat products. This system knows several constraints, such as the thermal effects caused by the frictions, and the mechanical effects provoked by metal elongation, that generates dysfunctions due to the influence of the process conditions. Several controllers are considered, including Proportional-integral (PI) and Backstepping control. This paper presents the study of Backstepping controls strategy of the winding system. Our winding system is simulated in MATLAB SIMULINK environment, the results obtained illustrate the efficiency of the proposed control with no overshoot, and the rising time is improved with good disturbances rejections comparing with the classical control law.

Analysis of Degradation Phenomena in Arc-Tube of Ceramic Metal Halide Lamp (세라믹 메탈할라이드 램프의 아크튜브 열화현상 분석)

  • Kim, Woo-Young;Lee, Se-Il;Yang, Jong-Kyung;Jang, Hyeok-Jin;Park, Dae-Hee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.12
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    • pp.996-1001
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    • 2010
  • Recently, the demand of ceramic metal halide lamp has been expanded. Therefore, the lamp with high efficiency and long lifetime are increasing and the evaluation of reliability is needed. In this paper, the degradation phenomena of ceramic metal halide lamp was studied. The lamp was tested for 3000 on/off cycles with each cycle having a duration of 20 minutes on and 20 minutes off based on the accelerated aging experiment based on "Reliability Standards RS C 0085". As result, the corrosion of arc tube and leak was appeared from reaction between inner wall of PCA and chemical elements, and distortion of electrode was resulted from difference of thermal expansion between arc tube of PCA and electrode. Also, the efficiency of lamp was decreased by the change of inner pressure, operation temperature, and driving voltage from wall blackening.

Effect of Annealing Temperature on the Properties of Sputtered Bi3.25La0.75Ti3O12 Thin Films

  • Kang, Hyunil;Song, Joontae
    • Transactions on Electrical and Electronic Materials
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    • v.14 no.3
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    • pp.130-132
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    • 2013
  • $Bi_{3.25}La_{0.75}Ti_3O_{12}$(BLT) thin films were prepared on the Pt(150 nm)/Ti(50 nm)/$SiO_2$/Si substrate using the rf magnetron sputtering method. The BLT thin films were annealed at temperatures ranging from $600^{\circ}C$ to $750^{\circ}C$ using the rapid thermal annealing. The structure and surface morphology of the thin films were characterized by x-ray diffraction and field emission scanning electron microscopy. The hysteresis loop of the BLT thin films showed that the remanent polarization (2Pr) of the film annealed at $700^{\circ}C$ was 10.92 ${\mu}C/cm^2$. The fatigue characteristic of the BLT thin film annealed at $700^{\circ}C$ was shown change polarization up to $1.2{\times}10^9$ switching cycles. We confirmed the excellent remnant polarization (Pr) and fatigue properties compared with other fabrication methods and suggested a good method for BLT thin films fabrications.

Shrinkage and Durability Characteristics of Latex Modified Repair Mortar for Agricultural Concrete Structures (농업용 콘크리트 구조물용 라텍스개질 보수용 모르타르의 수축 및 내구성능 평가)

  • Won, Jong-Pil;Lee, Jae-Young;Park, Chan-Gi;Park, Seong-Gi;Kim, Wan-Young
    • Journal of The Korean Society of Agricultural Engineers
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    • v.49 no.5
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    • pp.23-30
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    • 2007
  • This research was to evaluate the shrinkage and durability performance of latex modified repair mortar and to improve the service lift of the agricultural concrete structures. The shrinkage characteristics of the repair material creates the delamination of repair materials and existing concrete. It may reduce the service life of structures. Also the reduction of durability performance of the repair materials induces the destruction of the repaired concrete structures at early stage. In this research, plastic and drying shrinkage, thermal expansion coefficient for shrinkage properties, durability performance, permeability, repeated freezing and thawing, and resistance of chemical solution test were performed. Test results showed that the latex modified repair mortar indicated the shrinkage amount which the delamination does not happen, and the latex modified repair mortar appeared excellent long-term durability performance which can increase the service life.

Numerical Study on the Effect of Volume Change of Light-Off Catalyst on Light-Off Performance (저온활성촉매변환기의 체적변화가 활성화 성능에 미치는 영향에 관한 수치적 연구)

  • 정수진;김우승
    • Transactions of the Korean Society of Automotive Engineers
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    • v.8 no.6
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    • pp.87-100
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    • 2000
  • HC and CO emissions during the cold start contribute the majority of the total emissions in the legislated driving cycles. Therefore, in order to minimize the cold-start emissions, the fast light-off techniques have been developed and presented in the literature. One of the most encouraging strategies for reducing start-up emissions is to place the light-off catalyst, in addition to the main under-body catalyst, near the engine exhaust manifold. This study numerically consider three-dimensional, unsteady compressible reacting flow in the light-off and under body catalyst to examine the impact of a light-off catalyst on thermal response of the under body catalyst and tail pipe emission. The effect of flow distribution on the temperature distribution and emission performance have also been examined. The present results show that flow distribution has a great influence on the temperature distribution in the monolith at the early stage of warm-up process and the ultimate conversion efficiency of light-off catalyst is severly deteriorated when the space velocity is above $100,000hr^{-1}$.

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Evaluation of incorporating metakaolin to evaluate durability and mechanical properties of concrete

  • Joshaghani, Alireza;Moeini, Mohammad Amin;Balapour, Mohammad
    • Advances in concrete construction
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    • v.5 no.3
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    • pp.241-255
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    • 2017
  • Concrete is known to be the most used construction material worldwide. The environmental and economic aspects of Ordinary Portland Cement (OPC) containing concrete have led research studies to investigate the possibility of incorporating supplementary cementitious materials (SCMs) in concrete. Metakaolin (MK) is one SCM with high pozzolanic reactivity generated throughout the thermal activation of high purity kaolinite clay at a temperature ranging from $500^{\circ}C$ to $800^{\circ}C$. Although many studies have evaluated the effect of MK on mechanical properties of concrete and have reported positive effects, limited articles are considering the effect of MK on durability properties of concrete. Considering the lifetime assessment of concrete structures, the durability of concrete has become of particular interest recently. In the present work, the influences of MK on mechanical and durability properties of concrete mixtures are evaluated. Various experiments such as slump flow test, compressive strength, water permeability, freeze and thaw cycles, rapid chloride penetration and surface resistivity tests were carried out to determine mechanical and durability properties of concretes. Concretes made with the incorporation of MK revealed better mechanical and durability properties compared to control concretes due to combined pozzolanic reactivity and the filler effect of MK.

Immobilization and Stability of Lipase from Mucor racemosus NRRL 3631

  • Adham, Nehad Zaki;Ahmed, Hanan Mostafa;Naim, Nadia
    • Journal of Microbiology and Biotechnology
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    • v.20 no.2
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    • pp.332-339
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    • 2010
  • The lipase from Mucor racemosus NRRL 3631 was partially purified by fractional precipitation using 60% ammonium sulfate, which resulted in a 8.33-fold purification. The partially purified lipase was then immobilized using different immobilization techniques: physical adsorption, ionic binding, and entrapment. Entrapment in a 4% agar proved to be the most suitable technique (82% yield), as the immobilized lipase was more stable at acidic and alkaline pHs than the free enzyme, plus 100% of the original activity was retained owing to the thermal stability of the immobilized enzyme after heat treatment for 60 min at $45^{\circ}C$. The calculated half-lives (472.5, 433.12, and 268.5 min at 50, 55, and $60^{\circ}C$, respectively) and the activation energy (9.85 kcal/mol) for the immobilized enzyme were higher than those for the free enzyme. Under the selected conditions, the immobilized enzyme had a higher $K_m$ (11.11 mM) and lower $V_{max}$ (105.26 U/mg protein) when compared with the free enzyme (8.33 mM and 125.0 U/mg protein, respectively). The operational stability of the biocatalyst was tested for both the hydrolysis of triglycerides and esterification of fatty acids with glycerol. After 4 cycles, the immobilized lipase retained approximately 50% and 80% of its original activity in the hydrolysis and esterification reactions, respectively.

Electrical Properties of Pt/$LiNbO_3$/AIN/Si(100) structures (Pt/$LiNbO_3$/AIN/Si(100) 구조의 전기적 특성)

  • 정순원;정상현;인용일;김광호
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.58-61
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    • 2001
  • Metal-insulator-semiconductor (MIS) C-V properties with high dielectric AIN thin films showed no hysteresis and good interface properties. The dielectric constant of the AIN film calculated from the capacitance at the accumulation region in the capacitance-voltage(C-V) characteristics was about 8. The C-V characteristics of MFIS capacitor showed a hysteresis loop due to the ferroelectric nature of the LiNbO$_3$ thin films. Typical dielectric constant value of LiNbO$_3$ film of MFIS device was about 23. The memory window width was about 1.2V at the gate voltage of $\pm$5 V ranges. Typical gate leakage current density of the MFIS structure was the order of 10$^{-9}$ A/cm$^2$ at the range of within $\pm$500 kV/cm. The ferroelectric capacitors showed no polarization degradation up to about 10$^{11}$ switching cycles when subjected to symmetric bipolar voltage pulse(peak-to-peak 8V, 50% duty cycle) in the 500kHz.

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