• 제목/요약/키워드: thermal behaviour

검색결과 229건 처리시간 0.028초

저온에서 (Ba,Sr)$TiO_3$ 박막의 UV를 이용한 RTP에 관한 연구 (Low temperature UV-assisted rapid thermal processing of (Ba,Sr)$TiO_3$ thin films)

  • 조광환;강종윤;윤석진;이영백
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.234-234
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    • 2008
  • Chemically homogeneous $Ba_{0.6}Sr_{0.4}TiO_3$ (BST) sols were synthesized using barium acetate, strontium acetate, and titanium isoproxide as starting materials. BST thin films of thickness 340 nm were deposited on Pt/$TiO_2/SiO_2$/Si and alumina substrates using spin coating method. The technique used for the processing of these films was Ultraviolet (UV) sol-gel photoannealing, using phto-sensitivity precursor solutions and UV-assisted rapid thermal processing(UV-RTP). The crystallization behaviour of the BST sols and thin films was studied by differential thermal analysis (DTA) and X-ray diffraction (XRD). Variation of permittivity and dielectric loss were measured in LCR-meter, model HP 4394A.

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THERMAL EFFECTS ON THE STRAIN ENERGY RELEASE RATE FOR EDGE DELAMINATION IN CRACKED LAMINATED COMPOSITES

  • Soutis, C.;Kashtalyan, M.
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2001년도 제16회 학술발표회 논문초록집
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    • pp.1-6
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    • 2001
  • In this paper, edge delaminations in cracked composite plates are analytically investigated. A theoretical model based upon a sub-laminate approach is used to determine the strain energy release rate, $G^{ed}$, in [$\pm$$\theta_m$/$90_n$]$_s$ carbon/epoxy laminates loaded in tension. The analysis provides closed-form expressions for the reduced stiffness due to edge delamination and matrix cracking and the total energy release rate. The parameters controlling the laminate behaviour are identified. It is shown that the available energy for edge delamination is increased notably due to transverse ply cracking. Also thermal stresses increase substantially the strain energy release rate and this effect is magnified by the presence of matrix cracking. Prediction for the edge delamination onset strain is presented and compared with experimental data. The analysis could be applied to ceramic matrix composite laminates where similar mechanisms develop, but further experimental evidence is required.

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Al 6061합금의 마찰교반접합시 접합부의 열거동에 관한 연구 (A Study on the Thermal Behavior of Friction Stir Welding in hi 6061 Alloys)

  • 방한서;김흥주;고민성;김규훈
    • Journal of Welding and Joining
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    • 제20권4호
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    • pp.534-537
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    • 2002
  • In the various industry such as shipbuilding and automobile, etc., Al-alloys are used to reduce weight and improve economical efficiency, and they are mainly utilized in the process of Friction Stir Welding (FSW). A number of studies have been carried out on the metallurgical characteristics of friction stir welding In Al-alloys. However, research on the thermal behavior of FSW by using numerical analysis is not sufficient in the domestic and abroad. In this paper, therefore, numerical simulation was used to find out thermal behaviour of FSW by finite element method. We considered heat source that occurred by friction between tool shoulder including pin and base metal. To confirm the result of simulation, macrostructure is examined and compared after welding. The result of numerical simulation shows that Al-alloy is welded under a melting point of Al around pin by FSW.

염산처리 작잠견사의 가수분해거동 (Hydrolsis Behaviour of Antheraea pernyi Silk Fiber Treated with HCI)

  • 권해용;이광길;이용우;여주홍;엄인철
    • 한국잠사곤충학회지
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    • 제40권2호
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    • pp.163-168
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    • 1998
  • Hydrolysis rate and activation energy of Antheraea pernyi silk fiber treated with HCI were examined. Thermal decomposition temperature and surface morphology were also investigated by using differential scanning calorimeter and scanning electron microscope. As the concentration of hydrochloric acid and the treatment temperature increased, the hydrolysis occurred more rapidly. The activation energy of Antheraea pernyi, 74.0 kJ/mol, was higher than that of Bombyx mori, 58.1 kJ/mol. As the concentration of hydrochloric acid increases, the activation energy of Antheraea pernyi decreased from 74.0 kJ/mol to 62.0 kJ/mol. The shape of acid-resistance fraction of Antheraea pernyi became more distroyed and was transformed from fiber to powdered form with an increase of hydrolysis rate. The thermal decomposition temperature of Antheraea pernyi was 360.8$^{\circ}C$ until the hydrolysis rate was 81.8 wt%, but ti decreased to 347.0$^{\circ}C$ when the hydrolysis rate was 93.8 wt%.

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용접 잔류음력을 고려한 강구조물의 피로강도평가 (A Numerical Estimation of Fatigue Strength of Welded Steel Structures with Residual Stresses)

  • 정흥진;유병찬
    • 한국전산구조공학회:학술대회논문집
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    • 한국전산구조공학회 2007년도 정기 학술대회 논문집
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    • pp.265-270
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    • 2007
  • According to previous research, welding-induced residual stresses in steel structures can significantly affect the fatigue behaviour. Usually, high tensile residual stresses up to the yield strength are conservatively assumed at the weld toes. This conservative assumption can result in misleading fatigue assessments. Thee welding-induced residual stresses need be known in advance for a reliable fatigue assessment, which becomes possible to an increasing extent by numerical welding simulation. In this study, a fatigue Analysis technique for steel structures with welding induced residual stress is presented. First, We calculate the history of temperature according with welding process. Secondly, residual stress with a welding thermal history was evaluated by non-linear thermal stress analysis and lastly, fatigue strength is estimated with modified Goodman equation which can consider the effect of mean stress level.

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Poly(butylene succinate) ionomer의 결정화 거동과 분해 (Crystallization behaviour and Degradation of Poly(butylene succinate) ionomer)

  • Han, Sang-Il;Kim, Dong-Kuk;Im, Seung-Soon
    • 한국섬유공학회:학술대회논문집
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    • 한국섬유공학회 2003년도 봄 학술발표회 논문집
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    • pp.79-82
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    • 2003
  • An ionomer is defined as an ion-containing polymer with a small amount (usually up to 10-15 mol%) of ionic groups along the backbone chains or as pendant groups. Ionomers have been extensively studied because of the significant changes in their physical properties due to the formation of ionic aggregates, such as enhanced mechanical properties, high melt viscosity, and increased thermal properties.$\^$1-5/ Although there have been many studies of ionomers, the crystallization behaviour of degradable ionomers is still not understood. (omitted)

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Pseudomonas delafieldii가 생성하는 다당류의 레올로지 특성 (Rheological Properties of Biopolymer Produced by Pseudomonas delafieldii)

  • Yoo, Jin-Young;Chung, Dong-Hyo
    • 한국미생물·생명공학회지
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    • 제17권5호
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    • pp.475-480
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    • 1989
  • Pseudomonas delafieldii이 배양액으로부터 분리한 다당류 용액의 물성을 검토하였다. 본 다당류는 매우 점도가 높은 의가소성 물질로 1% 용액의 겉보기 점도는 42sec$^{-1}$에서 1769mpaㆍs이었다. 이 용액은 pH에 대한 안정성은 있으나 열 안정성은 보이지 않았다. 이 용액의 유동 활성에너지는 4.44kacl/mole 이고, 농도의존성은 double 1logarithm으로 포현되었다.

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자동차용 폴리머 복합재료의 변형과 강도에 관한 연구 (A study on deformation and strength of polymer composites using automobiles)

  • 신재훈;임재규;박한주
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 추계학술대회논문집A
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    • pp.238-243
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    • 2000
  • The effect of the temperature, the fatigue and the test speed on DEN(double edged notch) specimen which was made by the pp-rubber composites during fracture was stuied. DEN specimen was made on PP-rubber composites through the injection molding. With increasing temperature the fracture strength is linearly decrease and the fracture energy is first increase by $0^{\circ}C$ and after that decrease. In the same temperature the fracture strength during increasing the notch radius is hardly increase. The fracture behaviour at low and high test speed is different entirely. At high test speed plastic region is small and fracture behaviour was seen to brittle fracture tendency. The deformation mechanism of polypropylene-rubber composites during fracture was studied by SEM fractography. A strong plastic deformation of the matrix material ahead of the notch/crack occured. The deformation seem to be enhanced by a thermal blunting of the notch/crack.

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Dynamics of multilayered viscoelastic beams

  • Roy, H.;Dutt, J.K.;Datta, P.K.
    • Structural Engineering and Mechanics
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    • 제33권4호
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    • pp.391-406
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    • 2009
  • Viscoelastic materials store as well as dissipate energy to the thermal domain under deformation. Two efficient modelling techniques reported in literature use coupled (thermo-mechanical) ATF (Augmenting Thermodynamic Fields) displacements and ADF (Anelastic Displacement Fields) displacements, to represent the constitutive relationship in time domain by using certain viscoelastic parameters. Viscoelastic parameters are first extracted from the storage modulus and loss factor normally reported in hand books with the help of Genetic Algorithm and then constitutive relationships are used to obtain the equations of motion of the continuum after discretizing it with finite beam elements. The equations of motion are solved to get the frequency response function and modal damping ratio. The process may be applied to study the dynamic behaviour of composite beams and rotors comprising of several viscoelastic layers. Dynamic behaviour of a composite beam, formed by concentric layers of steel and aluminium is studied as an example.

Effect of damage on permeability and hygro-thermal behaviour of HPCs at elevated temperatures: Part 2. Numerical analysis

  • Gawin, D.;Majorana, C.E.;Pesavento, F.;Schrelfer, B.A.
    • Computers and Concrete
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    • 제2권3호
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    • pp.203-214
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    • 2005
  • In the Part 1 paper (Gawin, et al. 2005) some experimental results concerning micro-structural tests, permeability measurements and stress-strain tests of four types of High Performance Concrete, exposed to elevated temperatures (up to $700^{\circ}C$) are presented and discussed. On the basis of these experimental results parameters of the constitutive relationships describing influence of damage and temperature upon material intrinsic permeability at high temperature were determined. In this paper the effects of various formulations of damage-permeability coupling on results of computer simulations are analysed and compared with the results obtained by means of the previously proposed approach, that does not take into account the thermo-chemical concrete damage directly. Numerical solutions are obtained using the recently developed fully coupled model of hygro-thermal and damage phenomena in concrete at elevated temperatures. High temperature effects are considered by means of temperature and pressure dependence of several material parameters. Based on the mathematical model, the computer code HITECOSP was developed. Material parameters of the model were measured by several European laboratories, which participated in the "HITECO" research project. A model problem, concerning hygro-thermal behaviour and degradation of a HPC structure during fire, is solved. The influence of two different constitutive descriptions of the concrete permeability changes at high temperature, including thermo-chemical and mechanical damage effects, upon the results of computer simulations is analysed and discussed.