• 대한소아치과학회지
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• 제34권3호
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• pp.398-407
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• 2007

본 연구는 소아 환자의 유동성 복합 레진 수복 시 접착제의 사용 및 중합 여부 그리고 접착제 종류에 따른 수복물 변연의 미세누출과 전단결합강도를 비교함으로써 치료 시간의 단축 가능성을 타진해보고자 시행하였다. 미세누출을 평가하기 위해 우식이 없거나 법랑질에 제한된 우식이 있는 상, 하악 소구치 84개, 전단결합강도 평가를 위해 협설면에 우식이나 결손부가 없는 대구치 70개를 각각 준비하여 사용하였다. 접착 시스템의 종류에 따라 총 7군을 설정하여 I군과 II군은 Single $Bond^{TM}$, III군과 IV군은 AQ Bond $Plus^{TM}$, Ⅴ군과 Ⅵ군은 Prompt L-$Pop^{TM}$ 그리고 접착 시스템을 사용하지 않고 레진을 충전하는 VII군을 대조군으로 설정하였다. 미세누출과 전단결합강도를 측정하여 다음과 같은 결과를 얻었다. 1. 미세누출 평가 결과 Single $Bond^{TM}$를 사용한 I군과 II군이 다른 군에 비하여 낮은 염료 침투를 나타냈다. I군과 II군 사이의 염료 침투 양상은 유사하게 나타났다. 2. 전단결합측정결과 I군과 II군이 다른 군에 비하여 높은 수치를 나타냈으며 통계적 유의차를 보였다(p<0.05). I군과 II군 사이에는 유의차가 없었다(p>0.05). 3. I군과 II군, III군과 IV군, V군과 VI군 사이에는 통계적 유의차가 없었다(p>0.05). 4. VII군은 I, II군과 V, VI군에 비하여 통계적 유의차가 있게 낮은 전단 결합 강도를 보였으며(p<0.05) III, IV군과는 보다 낮은 수치를 보였으나 통계학적 유의차는 없었다(p>0.05).

• 대한치과교정학회지
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• 제27권2호
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• pp.315-326
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• 1997

여러 세라믹 브라켓과 접착제에 따른 전단 결합 강도를 비교하기 위하여, 영구 소구치 48개를 대상으로 베이스의 유지 형태가 다른 3종의 세라믹 브라켓을 광중합과 화학 중합을 포함한 3종의 교정용 접착제를 사용하여 접착하고 전단 결합 강도와 파절 양상을 관찰한 결과, 화학 중합형 레진으로 접착한 경우 광중합형으로 접착한 경우보다 결합강도가 높았으며, 화학적 결합을 하는 Starfire 브라켓이, 기계적 결합을 하는 Transcend나, 복합형 결합인 Fascination 보다 전단 결합 강도가 낮았다. Trascend는 주로 법랑질과 레진(E/R)에서, Fascination은 법랑질, 레진, 브라켓 베이스에 혼합(COMB)되어 파절되며, Starfire는 레진과 브라켓 베이스(R/B)에서 파절이 나타났다.

• 대한치과기공학회지
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• 제30권2호
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• pp.23-29
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• 2008

The purpose of this study is to evaluate possibility of using indirect composite resin instead of porcelain through the measurement of shear bond strength between zirconia core and indirect composite resin under treatment of $Rocatec^{TM}$ system for improving the adhesion of indirect composite resin. 20 cylindrical zirconia core specimens were divided into 2 groups, according to zirconia surface treatment and attached materials: 1) treated with sandblast and attached with indirect composite resin, 2) treated with sandblast + $Rocatec^{TM}$ system and attached with indirect composite resin. The shear bond strength of each experimental group was measured by MTS and the changes of zirconia core surface according to surface treatments were obtained by SEM observation and measurements of surface roughness. The mean shear bond strength values are $0.55\;{\pm}\;0.11MPa$(Group SC) and $1.16\;{\pm}\;0.46MPa$(Group SRC). The mean Ra values for the surface treatments were follows: $0.39\;{\pm}\;0.13$($100{\beta}_{{\mu}m}$ sandblast) and $0.50\;{\pm}\;0.03$($100{\beta}_{{\mu}m}$ sandblast + $Rocatec^{TM}$ system). In the analysis of EDS, Si element was detected in the Group SC. The shear bond strength between zirconia core and indirect composite resin was improved significantly by using $Rocatec^{TM}$ system.

• Restorative Dentistry and Endodontics
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• 제43권4호
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• pp.45.1-45.11
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• 2018

Objectives: This study was conducted to evaluate fluoride release and the micro-shear bond strength of resin-modified glass ionomer cement (RMGIC) in casein phosphopeptide-amorphous calcium phosphate (CPP-ACP)-remineralized caries-affected dentin (CAD). Materials and Methods: Exposed dentin surfaces of 30 human third molar teeth were divided into 2 equal groups for evaluating fluoride release and the micro-shear bond strength of RMGIC to CAD. Each group was subdivided into 3 equal subgroups: 1) control (sound dentin); 2) artificially demineralized dentin (CAD); 3) CPP-ACP remineralized dentin (remineralized CAD). To measure fluoride release, 15 disc-shaped specimens of RMGIC (4 mm in diameter and 2 mm in thickness) were bonded on one flat surface of the dentin discs of each group. Fluoride release was tested using ion chromatography at different intervals; 24 hours, 3, 5, 7 days. RMGIC micro-cylinders were built on the flat dentin surface of the 15 discs, which were prepared according to the assigned group. Micro-shear bond strength was measured after 24 hours water storage. Data were analyzed using 1- and 2-way analysis of variance and the post hoc least significant difference test (${\alpha}=0.05$). Results: Fluoride detected in solutions (at all intervals) and the micro-shear bond strength of RMGIC bonded to CPP-ACP-remineralized dentin were significantly higher than those bonded to artificial CAD (p < 0.05). Conclusions: Demineralized CAD consumes more fluoride released from RMGIC into the solution for remineralization than CPP-ACP mineralized dentin does. CPP-ACP increases the micro-shear bond strength of RMGIC to CAD.

• 대한치과보철학회지
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• 제40권4호
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• pp.365-373
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• 2002

The purpose of this study was to investigate the effects of desensitizer on shear bond strength of adhesive resin cements for all ceramic crown. For this study, Gluma $desensitizer^{(R)}$(Heraeus Kulzer, Germany) and MS $Coat^{(R)}$(Sun medical, Japan) were used as desensitizer, and Bistite $II^{(R)}$ resin cement(Tokuyama, Japan) and Variolink $II^{(R)}$ resin cement (Ivoclar, Liechtenstein) were used. IPS Empress ceramics were bonded to dentin surfaces after application of desensitizer and shear bond strength of specimens were measured using UTM(Zwick 1456 41. Zwick, Germany) at a crosshead speed of 1mm/min. The obtained results were as follows : 1. The shear bond strength of both resin cements were not affected by Gluma $desensitizer^{(R)}$ containing HEMA 2. The shear bond strength of Bistite $II^{(R)}$ resin cement was significantly decreased by MS $Coat^{(R)}$. 3. The failure mode in MS $Coat^{(R)}-Bistite \;II^{(R)}$ group was mainly adhesive type between dentin and resin cement. but that of Gluma $desensitizer^{(R)}$-Variolink $II^{(R)}$ group was mainly mixed type, combined adhesive failures between dentin and resin cement or porcelain and resin cement.

• 한국방재학회 논문집
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• 제9권1호
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• pp.27-32
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• 2009

본 연구의 주목적은 아스팔트 포장층간의 접착전단강도를 측정하는 실험법과 평가 방법을 개발하고 배수성 포장에 사용되는 택코트 재료의 특성과 적정 살포량을 평가하고자 하였다. 실험에는 두 종류(RSC-4, 개질유화)의 유화아스팔트와 가열 아스팔트바인더 타입(HM-1) 한 종류로 실시하였으며, HM-1은 배수성 포장에 사용하기 위해 새로 개발된 제품이다. 접착전단강도를 측정하기 위해 직접전단실험을 다양한 실험 조건에서 수행하였다. 실험을 통해 얻은 접착전단강도 값은 결과의 변별력이 떨어 졌으며 하중-변위 곡선의 면적인 터프니스가 접착전단강도를 평가하는데 보다 유용한 것을 확인 할 수 있었다. 배수성 포장의 경우 RSC-4의 경우는 $0.8l/m^2$ 이상, 개질유화아스팔트의 경우는 $0.5{\sim}0.6l/m^2$의 살포량이 적당한 것으로 나타났다. Trackless 성능이 우수한 HM-1은 유화 아스팔트 택코트에 비해 월등히 좋은 접착전단성능을 발휘하는 것으로 나타났다.

• The Journal of Advanced Prosthodontics
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• 제10권5호
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• pp.361-366
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• 2018

PURPOSE. The aim of this study was to evaluate the effects of relining materials on the flexural strength of relined thermoplastic denture base resins (TDBRs). MATERIALS AND METHODS. For shear bond strength testing, 120 specimens were fabricated using four TDBRs (EstheShot-Bright, Acrytone, Valplast, Weldenz) that were bonded with three autopolymerizing denture relining resins (ADRRs: Vertex Self-Curing, Tokuyama Rebase, Ufi Gel Hard) with a bond area of 6.0 mm in diameter and were assigned to each group (n=10). For flexural strength testing, 120 specimens measuring $64.0{\times}10.0{\times}3.3mm$ (ISO-1567:1999) were fabricated using four TDBRs and three ADRRs and were assigned to each group (n=10). The thickness of the specimens measured 2.0 mm of TDBR and 1.3 mm of ADRR. Forty specimens using four TDBRs and 30 specimens using ADRRs served as the control. All specimens were tested on a universal testing machine. For statistical analysis, Analysis of variance (ANOVA) with Tukey's test as post hoc and Spearman's correlation coefficient analysis (P=.05) were performed. RESULTS. Acry-Tone showed the highest shear bond strength, while Weldenz demonstrated the lowest bond strength between TDBR and ADRRs compared to other groups. EstheShot-Bright exhibited the highest flexural strength, while Weldenz showed the lowest flexural strength. Relined EstheShot-Bright demonstrated the highest flexural strength and relined Weldenz exhibited the lowest flexural strength (P<.05). Flexural strength of TDBRs (P=.001) and shear bond strength (P=.013) exhibited a positive correlation with the flexural strength of relined TDBRs. CONCLUSION. The flexural strength of relined TDBRs was affected by the flexural strength of the original denture base resins and bond strength between denture base resins and relining materials.

• 대한치과보철학회지
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• 제40권2호
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• pp.201-212
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• 2002

This study investigated the shear bond strengths between abrasion-resistant denture teeth and composite resins according to surface treatments. Denture teeth for this study were Trubyte IPN teeth(Dentsply Inc., USA) with interpenetrating polymer network and Endura Posterio (Shofu Inc. Japan) of composite resin teeth, and restorative composite resins were Clearfil FII (Kuraray, Japan) of the self-cured composite resin and Z100(3M Dental Product, USA) of the light-cured composite resin. Five different surface treatments were evaluated: (1) $50{\mu}m\;A1_2O_3$ sandblasting: (2) #100 carbide paper; (3) chloroform; (4) retentive holes; and (5) no treatment. After surface treatments, denture teeth were examined by scanning electron microscopy(SEM), and the maximum shear bond strengths between abrasion-resistant denture teeth and composite resins were measured using Instron. The results were as follows; 1. IPN teeth treated with sandblasting had the highest shear bond strength, and Endura treated with sandblasting and carbide paper had significantly greater shear bond strength than with any other surface treatment. 2. Regardless or composite resins, the shear bond strength on Endura was greater than on IPN teeth. 3. Regardless of denture teeth, the shear bond strength of Clearfil FII was greater han of Z100. 4. In appearance of SEM, IPN teeth treated with sandblasting showed generalized roughness on the all of surface, however, carbide paper treatment resulted in partly rough. Endura treated with sandblasting and carbide paper showed similar surface characteristics. Wetting denture teeth surface with chloroform removed the debris and created a particle-free and smooth surface.

• 대한치과기공학회지
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• 제33권4호
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• pp.349-357
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• 2011

Purpose: In this study, for the reasons of observing the changes when using bonding agent with Ni-Cr alloy and Co-Cr alloy and using VM13 and Vintage MP ceramic which have the disparity in coefficient of thermal expansion, it is carried out to evaluate the characteristics of the bonding agent through the analysis of the interface between metal and ceramic and the analysis of bond strength by variable. Methods: The surface treatment was performed on the two kinds of alloy(Ni-Cr alloy and Co-Cr alloy) specimens, which were sandblasted and were treated with bonder application. The metal-ceramic interfaces were analyzed with EPMA in order to ionic diffusion, and the shear test was performed. Results: As a result of observation of metal-ceramic interfacial properties, it was observed that Cr atoms were spread from the alloy body to the ceramic floor in the specimen of Group B. It was also seen that Cr, W atoms were spread from the alloy body to the ceramic floor in the specimen of Group S. In consequence of observing Shear bond strength, it was calculated that the specimen of BSV was 27.75(${\pm}11.21$)MPa, BSM was 27.02(${\pm}5.23$)MPa, BCV was 30.20(${\pm}5.99$)MPa, BCM was 27.94(${\pm}10.76$)MPa, SSV was 20.83(${\pm}2.58$)MPa, SSM was 23.98(${\pm}3.94$)MPa, SCV was 32.32(${\pm}4.68$)MPa, and SCM was 34.54(${\pm}10.63$)MPa. Conclusion: In the metal-ceramic interface of Bellabond plus sample group, diffusion of Cr atoms was incurred and diffusion of C Cr atoms and W atoms in the sample group of $Starloy{(R)}\;C$ was observed. Using bonding agent showed the higher bond strength than using the sand blasting treatment. In the Bellabond plus alloys, the specimen group with the use of binding materials showed higher shear bond strength, but didn't show statistically significant differences (p>0.05). In the $Starloy{(R)}\;C$ alloys, the specimen group with the use of binding materials showed higher shear bond strength and statistically significant differences(p<0.05). In terms of VM13 ceramic, it was in the Bellabond plus alloys that the high shear bond strength was showed, but there's no statistically significant differences(p>0.05). In terms of Vintage MP ceramic, it was in the $Starloy{(R)}\;C$ alloys that the high shear bond strength was showed and statistically significant differences(p<0.05). Metal-ceramic to fracture of the shear strength measurements and an analysis of all aspects of military usage fracture of the composite, respectively.

• The Journal of Advanced Prosthodontics
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• 제5권2호
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• pp.98-103
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• 2013

PURPOSE. To evaluate the effects of hydrofluoric acid etching and Er,Cr:YSGG laser irradiation on the shear bond strength of resin cement to lithium disilicate ceramic. MATERIALS AND METHODS. Fifty-five ceramic blocks ($5mm{\times}5mm{\times}2mm$) were fabricated and embedded in acrylic resin. Their surfaces were finished with 1000-grit silicon carbide paper. The blocks were assigned to five groups: 1) 9.5% hydrofluoric-acid etching for 60 s; 2-4), 1.5-, 2.5-, and 6-W Er,Cr:YSGG laser applications for 60 seconds, respectively; and 5) no treatment (control). One specimen from each group was examined using scanning electron microscopy. Ceramic primer (Rely X ceramic primer) and adhesive (Adper Single Bond) were applied to the ceramic surfaces, followed by resin cement to bond the composite cylinders, and light curing. Bonded specimens were stored in distilled water at $37^{\circ}C$ for 24 hours. Shear bond strengths were determined by a universal testing machine at 1 mm/min crosshead speed. Data were analyzed using Kruskal-Wallis and Mann-Whitney U-tests (${\alpha}$=0.05). RESULTS. Adhesion was significantly stronger in Group 2 ($3.88{\pm}1.94$ MPa) and Group 3 ($3.65{\pm}1.87$ MPa) than in Control group ($1.95{\pm}1.06$ MPa), in which bonding values were lowest (P<.01). No significant difference was observed between Group 4 ($3.59{\pm}1.19$ MPa) and Control group. Shear bond strength was highest in Group 1 ($8.42{\pm}1.86$ MPa; P<.01). CONCLUSION. Er,Cr:YSGG laser irradiation at 1.5 and 2.5 W increased shear bond strengths between ceramic and resin cement compared with untreated ceramic surfaces. Irradiation at 6 W may not be an efficient ceramic surface treatment technique.