• Journal of Pharmaceutical Investigation
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• 제29권4호
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• pp.315-321
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• 1999

Poly (lactide-co-glycolide) (PLGA) microspheres containing ovalbumin (OVA) as a model protein drug were prepared by double emulsification method, and various conditions such as mixing rate, volume of outer phase and isopropyl alcohol concentration in outer phase during secondary emulsification were observed to control the size of microspheres. In addition, entrapment efficiency of OVA and protein denaturation were also evaluated. As the rate of stirring was increased, the size of particles was decreased. But excessive stirring increased the particle size of microspheres. In a preparation condition of small volume of outer phase, the particle size was decreased but the entrapment efficiency was increased. Adding isopropyl alcohol to outer phase decreased the size of particles, but increased the entrapment efficiency. Microparticles should have smaller size than $10\;{\mu}m$ to be uptaked by Peyer's patch in small intestine. High speed of mixing and relatively small volume of outer phase are needed to reduce the size. In addition, appropriate amount of isopropyl alcohol in outer phase also plays an important role in size reduction of PLGA microspheres.

• 전력전자학회논문지
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• 제9권6호
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• pp.560-567
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• 2004

이 논문에서는 Planar transformer를 적용한 30W급 포워드 컨버터에 대한 설계와 실험결과를 소개한다. 컨버터의 전체적인 크기와 체적은 일반적인 권선형 변압기 대신 Planar transformer를 적용함으로써 감소하였고 크기와 체적의 감소로 포워드 컨버터의 전력밀도가 증가하였다. 또한, Single Switch 포워드 컨버터 와 Active Clamp ZVS 포워드 컨버터를 비교연구 하였다.

• 한국의류학회지
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• 제20권3호
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• pp.438-451
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• 1996

This study was performed to provide basic data for design of maternity brassiere. In order to find out transformation of breast size, shape and volume properties during the period of pregnancy, direct measurements of 306 subjects using Martin's anthropometer and indirect measurements using photography were conducted. And also breast surface area, volume and assumed weight using the molding of adhisive sheet are calculated. The results are as follows; 1) Size (breast widths, depths, girths and lengths) of the breast of pregnant woman are gradually increased during pregnancy. But underbust girth is decreased after delivery. 2) Front view of the breast is gradully dropped and widened. 3) Surface area, volume were measured for each stage of pregnancy, and weights of breasts were estimated. The surface area of breast of latter stage of prgnancy was increased 1.7 times comparing with the early stage. 4) Changes of bust girth, breast depth, underbust girth, volume and estimated breast weight during pregnancy should be considered for cup size, cup shape, width and strain of strap, and width of the wings.

• Composites Research
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• 제26권4호
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• pp.218-222
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• 2013

본 연구에서는 제강 과정의 부산물로 발생하는 슬래그의 구조용 충전제로써의 사용 가능성을 검토하였다. 고분자 기지 슬래그 복합재료를 제작하여 슬래그 입자의 크기(8~12 ${\mu}m$ and 12~16 ${\mu}m$), 체적 비(0-30 vol.%)에 따른 슬래그 복합재료의 기계적 특성에 대한 실험적 연구를 수행하였다. 복합재료 물성에 영향을 주는 요인인 입자 분산 도와 계면상태를 고찰하기 위해 각각 시편에 대하여 조직사진을 촬영하였다. 인장 시험 결과 슬래그 복합재료의 재료강성은 슬래그 체적비가 증가할수록 증가하였고 인장 강도는 체적비가 증가할수록 감소하였다. 슬래그 복합재료의 재료강성은 슬래그 입자의 크기의 변화에 따른 뚜렷한 경향성을 띄지 않았고 인장강도는 입자의 크기가 작을수록 높은 값을 가졌다. 조직 사진 촬영 결과 슬래그 복합재료가 양호한 계면상태를 보였고, 낮은 체적 비에서는 좋은 분산 도를 나타냈지만 체적비가 높아지면 입자들의 뭉침 현상이 발생하는 것을 알 수 있었다.

• 한국산업융합학회 논문집
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• 제26권1호
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• pp.79-86
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• 2023

This study was investigated the effect of carbon on the micro-structure and hardness of ductile cast iron roll with internal curing capacity. Spheroidal graphite existed at roll body with rapid cooling, but granular graphite existed at roll neck with slow cooling. The volume fraction of graphite increased at roll body with rapid cooling, That of roll neck with slow cooling decreased, but graphite size increased. The volume fraction of cementite decreased, but volume fraction increased. The cementite size was larger at roll neck than roll body. The hardness was decreased at roll body and roll neck due to volume fraction of cementite. The hardness of roll body was higher than roll neck.

• 열처리공학회지
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• 제30권3호
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• pp.99-105
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• 2017

This study was carried out to investigate the effect of heat treatment on the microstructure and mechanical properties in 90% hot forged Incoloy 825 alloy. With increasing solution treatment temperature, the grain size increased and the volume fraction of total precipitates decreased, and the precipitates disappeared at $1,000^{\circ}C$. With increasing aging time at $700^{\circ}C$, the volume fraction of precipitate increased and the precipitates size increased. Most of the precipitates consist $Cr_{23}C_6$ carbide, and a small amount of TiC carbide was also observed. With decreasing solution treatment temperature and increasing aging time, tensile strength and hardness increased, and the elongation and impact value decreased. With increasing aging time, the impact value decreased sharply by the increased of the precipitate size.

• Korean Chemical Engineering Research
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• 제51권5호
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• pp.622-627
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• 2013

콜로이달 실리카는 실리콘과 사파이어 웨이퍼의 정밀연마슬러리, 유-무기 하이브리드 코팅제, 정밀주조의 바인더 등 다양한 제품으로 사용되는 물질이다. 이러한 실리카 졸의 입자크기 및 분산 안정성은 웨이퍼의 표면, 코팅 막 혹은 벌크의 기계적, 화학적, 광학적 특성에 영향을 주기 때문에 정확한 측정값이 요구된다. 본 연구에서는 제조사에서 제시한 입자 크기 및 표면 특성이 다른 8종류 실리카 졸의 부피 분율에 따라 입자 크기, 졸 점도 및 입자 전기영동이동도의 측정결과에 미치는 영향을 논의하였다. 높은 표면활성을 지닌 실리카 입자의 특성 및 실리카 졸의 희석에 의한 안정화 이온 농도의 변화로 인해 실리카의 측정 입자 크기와 이동도는 졸의 부피 분율 혹은 입자 크기에 따라 변한다. 60 nm 보다 작은 입자는 부피 분율이 증가함에 따라 측정된 입자 크기가 증가한 반면에, 그 보다 큰 입자에서는 측정된 입자 크기가 감소하였다. 12 nm와 같이 작은 입자는 부피 분율이 증가함에 따라 점도가 상승하면서 측정 입자의 이동도가 감소한 반면에 100 nm의 큰 입자는 0.048의 낮은 부피 분율까지 이동도가 증가하다가 그보다 높은 부피 분율부터 감소하였다.

• 환경위생공학
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• 제13권3호
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• pp.19-29
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• 1998

The calcination reactivity of limestone and physical property changes of calcined lime were investigated with a temperature($720~1000^{\circ}C$ under atmospheric gas($N_2$, $CO_2$) conditions. The mechanisms of mass transport in a lime matrix were represented by the evaporation and condensation (${\gamma}=1.7$) at $1000^{\circ}C$ and the volume diffusion (${\gamma}=2.7$) at $800^{\circ}C$, which was obtained by the specific surface area of calcined lime with sintering conditions. Also, the effect of physical property on the reactivity of sulfation reaction was determined by the changes of pore size with $lime-SO_2$ reaction in this work. The initial sulfation rate of calcined lime increased with increasing temperature, whereas the capture capacity of $SO_2$ exhibited a maximum value at $900^{\circ}C$. The pore volume of sulfated lime was decreased with increasing sulfation time, but the major pores shifted to the distribution of larger size at a temperature of $850{\;}~{\;}1000^{\circ}C$. The mean pore size of sulfated lime based on pore volume decreased gradually at $1000^{\circ}C$; however, it increased with sulfation time up to 40 min and rapidly decreased thereafter.

• 동력기계공학회지
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• 제9권4호
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• pp.130-136
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• 2005

The effects of additional Mg content, the size and volume fraction of reinforcement phase on the mechanical properties of ceramic particle reinforced aluminium matrix composites fabricated by pressureless metal infiltration process were investigated. The hardness of $SiC_p/AC8A$ composites increased gradually with an increase in the additive Mg content, while the bending strength of $SiC_p/AC8A$ composites increased with an increase in additive Mg content up to 5%. However, this decreased when the level of additive Mg content was greater than 5% due to the formation of coarse precipitates by excessive Mg reaction and an increase in the porosity level. The hardness and strength of the composites increased with decreasing the size of SiC particle. It was found that the composites with smaller particles enhanced the interfacial bonding than those with bigger particles from fractography of the composites. The hardness of $Al_2O_{3p}/AC8A$ composites increased gradually with an increase in the volume fraction, however, the bending strength of $Al_2O_{3p}/AC8A$ composites decreased when the volume fraction of alumina particle was greater than 40% owing to the high porosity level.

• 한국세라믹학회지
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• 제37권7호
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• pp.638-644
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• 2000

The sintering behaviors of the glass-alumina composites for low firing temperature were investigated as functiions of the volume fraction of alumina powder and the particle size with respect to porosity and pore shape. As the volume fraction of alumina powder was increased or the particle size of it was decreased, the sintering temperature of open pore-closing was raised. When the volume fractions of alumina which had 2.19$\mu\textrm{m}$ median diameter were increased with 20, 30, 40, and 50%, the sintering temperatures of open pore-closing were 425, 450, 475, and 500$^{\circ}C$. And when the median particle size of alumina was diminished from 2.19$\mu\textrm{m}$ to 0.38$\mu\textrm{m}$, the sintering temperature of open pore-closing was increased from 450$^{\circ}C$ to 475$^{\circ}C$. Especially, the sintering temperature, which showed maximum density, was corresponded with the stage of open pore-closing and after achieving maximum density over heating resulted in dedensification of specimen, so called, over-firing behavior.