• 제목/요약/키워드: tensile modulus

검색결과 1,191건 처리시간 0.027초

Measurement of Degree of Hydrolysis of a PA66/GF Composite using a py-GC/MS analysis

  • Lee, Jong-Young;Kim, Kwang-Jea
    • Elastomers and Composites
    • /
    • 제52권1호
    • /
    • pp.59-68
    • /
    • 2017
  • The effect on the hydrolysis resistance properties by the addition of maleic anhydride grafted EMDM (MA-g-EPDM) and PP (MA-g-PP) to a PA66/GF composite was investigated with respect to the mechanical properties, thermal properties, and morphology. The degree of hydrolysis of the PA66/GF composite was measured using py-GC/MS analysis. When compared to the PA66/GFcomposite in MEG/water solution, the composites where MA-g-EPDM and MA-g-PP were added to PA66/GF showed a higher degree of hydrolysis resistance, impact strength, and thermal properties, whereas their tensile strength, tensile modulus, flexural strength and flexural modulus decreased. As immersion time in the solution increases, the rate of tensile strength drop of the MA-g-PP added composite appeared lower than that of the PA66/MA-g-EPDM/GF and PA66/GF composites. The py-GC/MS analysis confirmed the formation of PA66 hydrolysis reaction by products such as carboxylic acid and alkylamine with increasing immersion time.

고온가황에 의한 탄성체의 물성변화에 관한 연구 (A study on the change of physical properties of elastomer in high temperature curing)

  • 이정호
    • Elastomers and Composites
    • /
    • 제19권3호
    • /
    • pp.163-177
    • /
    • 1984
  • The effect of curing temperature increase and sulfur amount added were studied with natural and synthetic rubbers. Also, the effects of TMTD, MBTS and mixture of zinc soaps of high molecular fatty acids added to natural rubber were investigated respectively. The experimental results showed that, in the case of the conventional curing ($145^{\circ}C$), natural rubber, compared with synthetic rubber, gave higher values in elongation, tensile strength, cure rate, and lower values in modulus change. But, at high temperature curing ($180^{\circ}C$), natural rubber showed faster reversion rate, and higher heat build-up compared to synthetic rubber, than in the conventional curing. Also, natural rubber produced at high temperature showed severe degradation in hardness and tensile strength before heat-aging as well as in hardness, modulus and tensile strength after heat-aging. Improved reversion effect was obtained with natural rubber either by blending mixture of zinc soaps of high molecular acids or by applying semi-efficient vulcanization system.

  • PDF

Tensile, Thermal and Morphological Properties of Ballmilled Clay/Wood Flour Filled Polypropylene Nanocomposites

  • Lee, Sun-Young;Kang, In-Aeh;Chun, Sang-Jin
    • 한국응용과학기술학회지
    • /
    • 제25권2호
    • /
    • pp.160-167
    • /
    • 2008
  • Nanocomposites with polypropylene/clay/wood flour were prepared by melt blending and injection molding. Thermal, mechanical and morphological properties were characterized. The addition of ballmilled clay, compatibilizer and wood flour significantly improved the thermal stability of the hybrids. The tensile modulus and strength of most hybrids was highly increased with the increased loading of clay, maleated polypropylene (MAPP) and wood flour (WF), compared to the PP/WF hybrids. The tensile modulus and strength of most hybrids were highly increased with the increased loading of ballmilled clay, MAPP and wood flour, compared to the hybrids with PP/WF. The transmission electron microscopy (TEM) photomicrographs illustrated the intercalated and partially exfoliated structures of the hybrids with ballmilled clay, MAPP and wood flour.

단축 인장에 의한 SU-8박막의 기계적 물성 측정 (Measurement of mechanical properties of SU-8 thin film by tensile testing)

  • 백동천;박태상;이순복;이낙규
    • 반도체디스플레이기술학회지
    • /
    • 제3권2호
    • /
    • pp.23-26
    • /
    • 2004
  • Thin film is one of the most general structures used in micro-electro-mechanical systems (MEMS). To measure the mechanical properties of SU-8 film, tensile testing was adopted which offers not only elastic modulus but also yield strength and plastic deformation by load-displacement curve. Tensile testing system was constructed with linear guided servo motor for actuation, load cell for force measurement and dual microscope for strain measurement.

  • PDF

암석의 강도 및 변형거동의 온도의존성에 관한 연구 (A Study on Temperature Dependency of Strength and Deformation Behavior of Rocks)

  • 이형원;이정인
    • 터널과지하공간
    • /
    • 제6권2호
    • /
    • pp.101-121
    • /
    • 1996
  • The thermomechanical characteristics of rocks such as temperature dependency of strength and deformation were experimentally investigated using Iksan granite, Cheonan tonalite and Chung-ju dolomite for proper design and stability analysis of underground structures subjected to temperature changes. For the temperature below critical threshold temperature $T_c$, the variation of uniaxial compressive strength, Young's modulus, Brazilian tensile strength and cohesion with temperature were slightly different for each rock type, but these mechanical properties decreased at the temperatures above $T_c$ by the effect of thermal cracking. Tensile strength was most affected by $T_c$, and uniaxial compressive strength was least affected by $T_c$. To the temperature of 20$0^{\circ}C$ with the confining prressure to 150 kg/$\textrm{cm}^2$, failure limit on principal stress plane and failure envelope on $\sigma$-$\tau$ plane of Iksan granite were continuously lowered with increasing temperature but those of Cheonan tonalite and Chung-ju dolomite showed different characteristics depending on minor principal stress on principal stress plane and normal stress on $\sigma$-$\tau$ plane. The reason for this appeared to be the effect of rock characteristics and confining pressure. Young's modulus was also temperature and pressure dependent, but the variation of Young's modulus was about 10%, which was small compared to the variation of compressive strength. In general, Young's modulus increased with increasing confining pressure and increased or decreased with increasing temperature to 20$0^{\circ}C$ depending on the rock type.

  • PDF

Tensile strength of unidirectional CFRP laminate under high strain rate

  • Taniguchi, Norihiko;Nishiwaki, Tsuyoshi;Kawada, Hiroyuki
    • Advanced Composite Materials
    • /
    • 제16권2호
    • /
    • pp.167-180
    • /
    • 2007
  • The tensile strength of unidirectional carbon fiber reinforced plastics under a high strain rate was experimentally investigated. A high-strain-rate test was performed using the tension-type split Hopkinson bar technique. In order to obtain the tensile stress-strain relations, a special fixture was used for the impact tensile specimen. The experimental results demonstrated that the tensile modulus and strength in the longitudinal direction are independent of the strain rate. In contrast, the tensile properties in the transverse direction and the shear properties increase with the strain rate. Moreover, it was observed that the strain-rate dependence of the shear strength is much stronger than that of the transverse strength. The tensile strength of off-axis specimens was measured using an oblique tab, and the experimental results were compared with the tensile strength predicted based on the Tsai-Hill failure criterion. It was concluded that the tensile strength can be characterized quite well using the above failure criterion under dynamic loading conditions.

레이저 적층제조기술로 제작한 폴리아미드 12 시편의 인장특성 연구 (Study on Tensile Properties of Polyamide 12 produced by Laser-based Additive Manufacturing Process)

  • 김무선
    • 한국산학기술학회논문지
    • /
    • 제20권11호
    • /
    • pp.217-223
    • /
    • 2019
  • 복합 형상 부품 제작 및 제작 공정의 일체화 장점으로 3D 프린팅 기술의 적용 분야가 확대되고 있으며, 지속적인 연구 개발에 의해 다양한 기술방안들이 등장하고 있다. 대표적인 기술로는 파우더 형태의 소재 위에 레이저를 조사함으로써 원하는 영역을 소결 및 적층 제작하는 방식의 SLS 기술이 있으며, 고성능의 엔지니어링 플라스틱을 활용하여 실제 사용할 수 있는 부품을 제작하는 사례가 늘어나고 있다. 본 연구에서는 활용도가 높은 고분자 소재인 폴리아미드 12 소재 및 글라스 비드가 보강된 폴리아미드 12 소재를 대상으로 인장시편을 제작하여 시편 제작 방향 및 인장 시험 온도에 따른 특성 결과를 비교 분석하였다. 시편 제작방향은 작업 평면 기준으로 0°, 45°, 90° 로 구분하였으며, 인장시험온도는 -25℃, 25℃, 60℃로 조건을 구분하였다. 시험 결과로부터 제작 방향이 90°에 가까울수록 두 소재 모두 탄성률의 미세한 감소를 보였으며, 인장강도는 PA12보다 글라스 비드 보강 PA12가 제작방향에 대한 의존성을 명확하게 보였다. 또한 시험 온도 증가에 따라 탄성률 및 인장강도의 저하를 확인할 수 있었다.

수중 보관이 접착용 레진의 물리적 성질에 미치는 영향 (The Influence of Water Storage on Mechanical Properties of Adhesive Resin)

  • 김원찬;이광원;이정;유미경;김정희
    • 구강회복응용과학지
    • /
    • 제22권2호
    • /
    • pp.193-202
    • /
    • 2006
  • Objective To evaluate the influence of water storage on the mechanical properties of dental adhesives over 1 and 3 months. Materials and Methods Adhesive resin sheets were prepared by pouring either All-bond 2(AB), Clearfil SE Bond(SE) into a mold measuring $15{\times}15{\times}0.9mm$. After solvent in primer evaporation, the adhesives were light-cured and removed from the mold and divided in two pieces, trimmed to hourglass shape that were used to determine the micro-tensile strength(MTS). Another hourglass shaped metal mold measuring $2.0{\times}1.5mm$ in cross-section area was made to determine the Young's modulus(E). Adhesive specimens for Young's modulus(E) were prepared in the same method. Specimens were stored at $37^{\circ}C$ in distilled water and tested after 1 and 3 months. The data were analyzed by one-way ANOVA and Tukey's test. Results Water storage significantly decreased the micro-tensile strength(MTS) of AB and SE specimens after 1 and 3 months(P<0.05). The Young's modulus(E) were also decreased after water storage for 1 and 3 months, but statistically not significant in each group of AB and SE group respectively. Conclusions Long-term exposure of adhesive resin to water can cause reduction of mechanical properties. It may compromise resin/dentin bonds and affect longevity of restorations.