• 제목/요약/키워드: temperature-time curve

Search Result 391, Processing Time 0.026 seconds

Time-Temperature-Transition Diagrams with Liquid Crystalline Phase Changes of Liquid Crystalline Epoxy (열경화성 액정 에폭시 수지의 액정상 변화를 포함한 시간-온도-전이 다이어그램)

  • Seung Hyun Cho
    • Composites Research
    • /
    • v.37 no.3
    • /
    • pp.215-218
    • /
    • 2024
  • Liquid crystalline thermosetting epoxy oligomer DD-A was synthesized with Diglycidyl ether of 4,4'-dihydroxy-α-methylstilbene (DGE-DHMS) and aniline in a ratio of 2:1 and cured with a catalytic curing agent, 1-Methyl Imidazole. The gelation times and vitrification times were measured to create Time-Temperature-Transition Diagrams with liquid crystalline phase changes. It was found that the gelation and vitrification times were decreased as the concentration of curing agent increased, and the vitrification curve showing a typical S-shape was confirmed.

HOMOGENEOUS SOLUTION FOR SW LACERTAE

  • Kim, Kyung-Joo;Kang, Young-Woon
    • Journal of Astronomy and Space Sciences
    • /
    • v.13 no.1
    • /
    • pp.19-31
    • /
    • 1996
  • We have analyzed collected photoelectric light curves for light variations of SW Lac. The method of Fourier analysis was adopted to quantify the light variation from season to season. We found the linear relation between the Fourier coefficient, B1 and the magnitude difference between two maxima. The total light of the system has been decreased as much as 0m.04 during approxiamately 20 years time interval. Photoelectric parameters including spot parameters for all light curves were obtained by the method of the Wilson and Devinney differential correction in order to secure the variations of parameters from season to season. SW Lac, not like RS CVn type stars, required to adjust all parameters as well as spot parameters for a reasonable fit to the observations of each epoch. A surface temperature of cooler star is one of the most sensitive parameters to affect a shape of light curve of SW Lac. We conclude that the shape of light curve of SW Lac varies even during one season as well as season to season. The light curve is mainly caused by inhomogeneous surface temperature due to strong chromospheric activity of the system.

  • PDF

Structural and ferroelectric characteristics of sol-gel $Pb(Zr_{1-x}Ti_x)O_3$ thin films according to the sintering conditions and Zr/Ti mol% (소성 조건과 Zr/Ti 몰비에 따른 졸겔 $Pb(Zr_{1-x}Ti_x)O_3$ 박막의 구조 및 강유전 특성)

  • 김준한;윤현상;박정흠;장낙원;박창엽
    • Electrical & Electronic Materials
    • /
    • v.9 no.8
    • /
    • pp.836-850
    • /
    • 1996
  • In this study, we have analyzed structural analysis and measured ferroelectric characteristics of PZT thin films prepared by sol gel process with different sintering conditions and different Zr/Ti mot%. When the Zr mot% of PZT thin film was increased, it was found that the remanent. polarization and coercive field were decreased and increased, respectively. Also, the maxium dielectric constant of PZT(50/50) thin film was 786.8. We got double hysteresis(anti-fcrroelectric) curve from PbZrO$_{3}$ thin film. As heating rate goes up, pyrochlore phase of PZT thin film was decreased and dielectric and ferroelectric characteristics were improved. As a result of variation of sintering temperature and time 500.deg. C-800.deg. C and 5 sec.-8 hours, respectively, we got optimal sintering temperature and time. The optimium sintering temperature and time of conventional furnace method and rapid thermal processing method were 650.deg. C-700.deg. C for 30-60 minutes and 700.deg. C/20 seconds-2 minutes, respectively.

  • PDF

Adsorption Characteristics of Water Vapor on Zeolite (Zeolite의 수증기 흡착특성)

  • Lee, Song-Woo;Na, Young-Soo;An, Chang-Doeuk;Lee, Min-Gyu
    • Journal of Environmental Science International
    • /
    • v.20 no.5
    • /
    • pp.667-672
    • /
    • 2011
  • The purpose of this work is to present the experiment results by a dynamic adsorption of water vapor on pelletized zeolites (ADZ300, ADZ400, and ADZ500) in fixed bed. The breakthrough curves of water vapor with several different concentrations and temperature in the range of 25~45 $^{\circ}C$ on zeolite bed were investigated. In the same conditions, the breakthrough time on ADZ400 and ADZ500 were little longer than ADZ300, and the equilibrium adsorption capacity on ADZ500 was highest. The higher the concentration of water vapor was, the faster the breakthrough time was, and the slope of breakthrough curves showed a tendency to increase. The faster the flow rate of water vapor was, the faster the breakthrough time was relatively, but variations between flow rate and breakthrough time did not have a proportional relationship. The breakthrough curve maintained constant gradient in spite of variation of flow rate in the same concentration. The temperature rise in zeolite bed by adsorption heat was occurred in the early stage of adsorption. After water molecule layers were formed on the surface of zeolite, the temperature was slowly cooled by water vapors continuously flowed in as constant temperature. The greater the concentration of water vapor and adsorption temperature were, the temperature difference in zeolite bed was increased.

A Study on the loading test for of slab by Fire damaged (화재피해를 입은 RC 슬래브의 재하실험에 관한 연구)

  • Lee, Kyu Min;Kang, Seung Goo;Kim, Dong Jun;Kwon, Young Jin
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2013.11a
    • /
    • pp.50-51
    • /
    • 2013
  • In case of Korea, it goes frequently that underground parks has been burned. Based on standard temperature time curve(ISO-834), gerber, walls, slab of structures are constructed. However, Standard temperature time Curve is not considered that buildings are affected by vehicle fire. that is why it has the hazard that makes building reinforcement feeble. Based on the result that got from vehicle experiment before, we made four RC slab in this experiment and set the fire severity. according to the loading experiment after heating, we measured the effects that makes reinforcement and shape changes. Furthermore, we examined the safty of the structure by comparing before and after heating.

  • PDF

A Study on The Fabrication of The Sintering Process and The Thermoluminescence Properties of UV Dose about The Mg2SiO4 Thermoluminescent Phosphors (Mg2SiO4 열형광체의 소결공정과 자외선 선량에 대한 TL 특성에 관한 연구)

  • Kim, Young-KooK;Shon, In-Ho;Kim, Il-Hong;Song, Jae-Heung;Doh, Sih-Hong;Kang, Hee-Dong
    • Korean Journal of Materials Research
    • /
    • v.12 no.11
    • /
    • pp.870-874
    • /
    • 2002
  • $Mg_2$$SiO_4$: Dy, Tb pellets were made by using a sintering process, including pressing and heat treatment. In the present study, the optimum parameters of the sintering for the $Mg_2$$SiO_4$: Dy, Tb pellets obtained such as the pressing pressure, the sintering temperature and the sintering time were in terms of thermoluminescence. Experimental results showed that the main peak of the glow curve for $Mg_2$$SiO_4$: Dy, Tb thermoluminescence dosimeter was clearly correlated with the energy of the UV and with the grain size. The intensity of the TL glow curve increased and its main peak position shifted to lower temperature with increasing UV irradiation time.

Fluctuation of Solid-Liquid Interface of Faceted Phase and Nonfaceted Phase by Periodic Temperature Variation

  • Oh, Sung-Tag;Kim, Young Do;Song, Young-Jun;Suk, Myung-Jin
    • Korean Journal of Materials Research
    • /
    • v.26 no.11
    • /
    • pp.644-648
    • /
    • 2016
  • In order to examine how the solid-liquid interface responds to temperature variation depending on the materials characteristics, i.e. faceted phase or nonfaceted phase, the moving solid-liquid interface of transparent organic material, as a model substance for metallic materials (pivalic acid, camphene, salol, and camphor-50wt% naphthalene) was observed in-situ. Plots of the interface movement distance against time were obtained. The solid-liquid interface of the nonfaceted phase is atomically rough; it migrates in continuous mode, giving smooth curves of the distance-time plot. This is the case for pivalic acid and camphene. It was expected that the faceted phases would show different types of curves of the distance-time plot because of the atomically smooth solid-liquid interface. However, salol (faceted phase) shows a curve of the distance-time plot as smooth as that of the nonfaceted phases. This indicates that the solid-liquid interface of salol migrates as continuously as that of the nonfaceted phases. This is in contrast with the case of naphthalene, one of the faceted phases, for which the solid-liquid interface migrates in "stop and go" mode, giving a stepwise curve of the distance-time plot.

Thermal stress of concrete structure at high temperature considering inelastic thermal strain change (고온에서의 비선형 변형도를 고려한 콘크리트 구조물에서의 열응력 분포)

  • 강석원;홍성걸;신영수
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2000.10b
    • /
    • pp.1145-1150
    • /
    • 2000
  • Concrete behaves as ductile material at high temperature. The existing stress-strain relationship is not valid at high temperature condition. Thus, stress-strain curve of concrete at high temperature is re-established by modifying Saenz's suggestion in this study. A constitutive model of concrete subjected to elevated temperature is also suggested. The model consists of three components; free thermal stain, mechanical strain and thermal creep strain. As the temperature increase, the thermal creep becomes more critical to the failure of concrete. The thermal creep strain of concrete is derived from the modified power-law relation for the steady state creep. The proposed equation for thermal creep employs a Dorn's temperature compensated time theorem

  • PDF

A Study about Pb-ferrite & effect of Annex (Pb-ferrite와 첨가물의 효과)

  • 배진호;사공건
    • 전기의세계
    • /
    • v.23 no.5
    • /
    • pp.61-65
    • /
    • 1974
  • Ba-ferrite and Sr-ferrite are mostly used for permanent magnetic materials. In this work, we investigated Pb-ferrite which is studying now at abroad. We studied the most appropriate mole percent of PbO to Fe$_{2}$O$_{3}$, calcinating temperature and time, sintering temperature and time, and further investigated effects of the annex(NaBiO$_{3}$) The method of appraisment is the microscope for meta and B-H curve by flaxmeter.

  • PDF

A Study on the Integrated Computer Program for the Multi Analysis of In-Situ Aquifer and Geothermal Response Test (현장 열응답시험과 현장 대수성시험결과를 동시 분석 가능한 통합전산 Program에 관한 연구)

  • Hahn, Jeong-Sang;Han, Hyuk-Sang;Yonn, Yun-Sang
    • Journal of the Korean Society for Geothermal and Hydrothermal Energy
    • /
    • v.4 no.1
    • /
    • pp.11-19
    • /
    • 2008
  • Groundwater flow in confined aquifer and heat transport in underground geologic media are using same governing equation(line source) like well fuction. Therefore the conventional slope method using only later data obtained from in-situ thermal response test to determine the thermal conductivity of vertical geothermal heat exchanger(GHEX) is basically identical with one of Theis straight line method of aquifer test under artesian condition. In case that the pumping rate(Q, $m^3$/d) and drawdown(s,m) which are used for input data of existing hydrogeologic computer programs for aquifer test are replaced and converted to supplying heat energy per unit length of bore hole(Q/L,w/m or Kcal/h.m) and temperatures (T,$^{\circ}C$)measured at in and out-let of GHEX as in put data respectively, thermal conductivity around geothermal heat exchanger can be easily estimated without any special modification of the existing hydrogeologic computer program. Two numbers of time series temperature variation data obtained from in situ geothermal response test are analized using Theismethods(standard curve and straight line method) by using existing aquifer test program and conventional Slope method proposed by ASHRAE. The results show that thermal conductivity values estimated by two straight methods are identical and the difference of estimated values between standard curve methods and Slope method are also within acceptable ranges. In general,the thermal conductivity estimated from Theis straight linemethod gives more accurate value than the one of Slope method due to that Slope method uses only visual matching otherwise Theis method uses automatic curve matching estimation with reducing RSS.

  • PDF