• 제목/요약/키워드: temperature standards

검색결과 885건 처리시간 0.028초

543 nm 헬륨네온 레이저의 주파수 안정화를 위한 I2 포화흡수분광 (I2-Saturated Absorption Spectroscopy for Frequency-Stabilization of He-Ne Laser at 543 nm)

  • 김경찬;엄년식;홍주현;서호성
    • 한국산학기술학회논문지
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    • 제11권3호
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    • pp.859-865
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    • 2010
  • 본 연구는 543 nm 헬륨네온 레이저의 주파수 안정화를 위한 $^{127}I_2$ 포화흡수분광 장치의 설계와 제작에 관한 것이다. 온도와 PZT 변화에 의한 레이저관 길이 가변을 이용하여 543 nm 헬륨네온 레이저의 주파수를 주사시켰다. 3차 고조파 신호을 얻기 위해 PZT 변조 가능한 레이저 출력경을 이용하여 주파수 변조를 하였다. 그 결과, $^{127}I_2$용 B-X 시스템의 R(12) 26-0에서 R(106) 28-0의 천이를 가지는 초미세구조 분광은 포화흡수분광기를 사용한 3차 미분신호에서 관찰되었다. 또한, 전형적인 초미세구조 분광 신호의 신호대 잡음비는 약 30:1 로 얻어졌다.

자동차 시트용 폐폴리우레탄의 해중합 (Depolymerization of Waste Polyurethane from Automotive Seats)

  • 민성진;공승대;윤철훈;강안수;엄재열;신판우;이석우
    • 한국응용과학기술학회지
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    • 제18권2호
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    • pp.103-110
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    • 2001
  • Resource recovery and recycling of materials and products, including polyurethanes is viewed as a necessity in today's society. Most urethane polymers are made from a polyol and a diisocyanate. these and be chemicals such as water, diamines or diols that react with isocyanate groups and add to the polymer backbone. The problems of recycling polyurethane wastes has major technological, economic and ecological significance because polyurethane itself is relatively expensive and its disposal whether by burning is also costly. In general, the recycling methods for polyurethane could be classified as mechanical, chemical and feedstock. In the chemical recycling method, there are hydrolysis, glycolysis, pyrolysis and aminolysis. This study, the work was carried out glycolysis using sonication ant catalyzed reaction. Different kinds of recycled polyols were produced by current method(glycolysis), catalyzed reaction and sonication as decomposers and the chemical properties were analyzed. The reaction results in the formation of polyester urethane diols, the OH value which is determined by the quantity of diol used for the glycolysis conditions. The glycolysis rates by sonication for the various glycols, increased as fallows: PPG

포장재에 따른 멸균품의 유효기간에 관한 연구 (Study on the Shelf Life of Sterilized Products according to Packaging Materials)

  • 장송자;정정희;최경미;김미영;박주희;정나연
    • 임상간호연구
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    • 제25권3호
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    • pp.333-341
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    • 2019
  • Purpose: The purpose of this study was to determine the most appropriate shelf life for sterilized products according to their packaging material. Methods: Samples were prepared to target six nursing units in one general hospital in Seoul. After steam and E.O gas sterilization, sterilized product, samples were supplied to wards. Data collection was conducted for 3 months, after the expiration date of 3 months had passed for samples packaged with crepe paper and nonwoven wraps. For samples packaged with paper-plastic pouches, data collection conducted for 3 months when the expiration date of 9 months had passed. The sterilized products were collected and tested for microbial contamination. Identification of the storage environment was done as samples were collected. Results: This study confirmed that the storage environment met international standards such as CDC, except for temperature. For steam sterilized crepe paper packaging samples and steam and E.O gas sterilized for nonwoven packaging samples no contamination in all products was found for 3 months past the expiration date. However, in the E.O gas sterilized paper-plastic pouch packaging sterile samples, Gram-positive bacilli were detected in one sample from a surgical intensive care unit at 45 weeks and another sample from an operating room at 47 weeks. Furthermore, the results did not show any microorganisms for up to 52 weeks in all products. Conclusion: According to the results of this study, sterilized product packaging made with crepe paper and nonwoven wraps is better able an extended shelf life from 3 months to 6 months, reducing unnecessary costs.

저온 열처리 목재 표면의 분광학적 특성 (Spectroscopic Characterization of Wood Surface Treated by Low-Temperature Heating)

  • 김강재;나기백;류지애;엄태진
    • Journal of the Korean Wood Science and Technology
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    • 제46권3호
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    • pp.285-296
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    • 2018
  • ISPM No. 15에 의거한 열처리 목재의 검증을 위한 연구로서 열처리 목재 표면의 분광학적 특성을 분석하였다. IR 스펙트럼 상에서는 다양한 작용기들이 확인되지만 수종간, 열처리 시간 및 보관 기간에 따른 특별한 차이를 발견하기 어려웠다. HBI(hydrogen-bonding intensity)는 보관 기간에 따른 열처리 목재의 변화는 관찰할 수 있지만 열처리 시간에 따른 변화는 관찰하기 어려웠다. 하지만 PCA score plot 상에서 수종 내에서 60분 혹은 90분의 열처리 시간에 따라 목재의 분류가 가능하였다. PCA에서 열처리 목재의 분류의 기준은 목재 내 리그닌의 방향족 환과 셀룰로오스의 C-H bending이었으며 이들 성분에 의해 ISPM No. 15로 열처리된 목재를 분류할 수 있었다.

급·배기 일체형 디퓨저의 환기 및 온열환경 유지성능에 대한 연구 (A Study on The Performance of Ventilation and Maintaining Thermal Environment for a Combined Type Diffuser)

  • 임석영;장현재
    • 설비공학논문집
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    • 제28권6호
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    • pp.232-241
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    • 2016
  • Installing a ventilator for an apartment house composed of over 100 dwelling units was mandated in 2006 to improve indoor air quality. In the case of mechanical ventilators, the air change rate is kept stable, however 68% of dwellers do not operate their ventilator because of an increased electrical bill and noise. In the case of natural ventilators, the former problems are settled, but there are concerns about cold draught and an increase of heating/cooling cost. Authors are developing a heat recovery type natural ventilator which is a natural ventilator equipped with total heat recovery element, and it is expected that those problems of mechanical ventilator and natural ventilator are resolved by this. The combined type diffuser of this study is an under developed fit to the heat recovery type natural ventilator above. There are no standards to evaluate the performance for this type of diffuser. Due to this issue this study investigated the performance of the ventilation and maintained a thermal environment for the combined type diffuser by comparing it with existing diffusers. The results revealed that the performances of the combined type of diffusers showed different features from the existing ones, and was estimated to be high enough in the performances above.

Multicomponent assessment and ginsenoside conversions of Panax quinquefolium L. roots before and after steaming by HPLC-MSn

  • Huang, Xin;Liu, Yan;Zhang, Yong;Li, Shuai-Ping;Yue, Hao;Chen, Chang-Bao;Liu, Shu-Ying
    • Journal of Ginseng Research
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    • 제43권1호
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    • pp.27-37
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    • 2019
  • Background: The structural conversions in ginsenosides induced by steaming or heating or acidic condition could improve red ginseng bioactivities significantly. In this paper, the chemical transformations of red American ginseng from fresh Panax quinquefolium L. under steaming were investigated, and the possible mechanisms were discussed. Methods: A method with reversed-phase high-performance liquid chromatography coupled with linear ion trap mass spectrometry ($HPLC-MS^n$)-equipped electrospray ionization ion source was developed for structural analysis and quantitation of ginsenosides in dried and red American ginseng. Results: In total, 59 ginsenosides of protopanaxadiol, protopanaxatriol, oleanane, and ocotillol types were identified in American ginseng before and after steaming process by matching the molecular weight and/or comparing $MS^n$ fragmentation with that of standards and/or known published compounds, and some of them were determined to be disappeared or newly generated under different steaming time and temperature. The specific fragments of each aglycone-type ginsenosides were determined as well as aglycone hydrated and dehydrated ones. The mechanisms were deduced as hydrolysis, hydration, dehydration, and isomerization of neutral and acidic ginsenosides. Furthermore, the relative peak areas of detected compounds were calculated based on peak areas ratio. Conclusion: The multicomponent assessment of American ginseng was conducted by $HPLC-MS^n$. The result is expected to provide possibility for holistic evaluation of the processing procedures of red American ginseng and a scientific basis for the usage of American ginseng in prescription.

치매요양시설에서의 치료를 위한 빛·색채의 시설적 적용 특성에 관한 고찰 - 정성적 및 정량적 적용 특성을 중심으로 (A Study on the Characteristics of Application for Therapeutic Light and Color in Dementia Care Facilities - Focused on Qualitative and Quantitative Application Characteristics)

  • 지수인
    • 의료ㆍ복지 건축 : 한국의료복지건축학회 논문집
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    • 제24권4호
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    • pp.69-87
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    • 2018
  • Purpose: This study has been started with the awareness that light and color are the main visual sensors of the multi-sensory stimulation environment to achieve the therapeutic environment for demented elderly. The purpose of this study therefore is for clarifying the application characteristics of therapeutic light and color for dementia care facilities. Methods: Internal and external literature reviews have been conducted for the investigation into a)disorders and visual system in demented elderly, b)therapeutic effects of light and color, c)heliotherapy, light therapy and color therapy to deduce the therapeutic characteristics of light and color for demented elderly, and finally into d)the application characteristics of it for dementia care facilities. Results: The application characteristics of the therapeutic light and color for dementia care facilities are classified into both qualitative and quantitative characteristics. Qualitative application characteristics of light represented using of daylight, using of lighting approximate to daylight, expansion of iluminance level, equality in iluminance Level, reduction of shadow, and as well as exclusion of blare. Quantitative application characteristics of it represented iluminance level, color temperature and color rendering index prescribed in international lighting standards. Qualitative application characteristics of color represented non-monochromatic color, color contrast, long wavelength of yellow-red colors, exclusion of short wavelength of blue colors and patterns, and as well as different colors for idenfication. Quantitative application characteristics of it represented kontrast(K) prescribed in DIN32975:2009 and light reflectance value(LRV) prescribed in BS8300:2009. Implications: To form dementia care facilities as therapeutic environment both qualitative and quantitative application characteristics of therapeutic light and color in dementia care facilities are needed.

Development of Highly Sensitive Analytical Method for Evaluation of Evening Primrose Oil's Enhancing Effect in Prostaglandin E1(OP 1206) Biosynthesis

  • Lee, Sung-Hoon
    • 인간식물환경학회지
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    • 제21권6호
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    • pp.485-492
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    • 2018
  • This study aimed to develop and validate highly sensitive determination method of a prostaglandin ($PGE_1$, OP 1206) in human plasma by LC-MS/MS using column switching. Plasma stored at $-30^{\circ}C$ and treated with methanol effectively inhibited interferences synthesized post-sampling. Samples were added with internal standard and were separated by reversed-phase HPLC with a cycle time of 30min. The method was selective for OP 1206 and the regression models, based on internal standard, were linear across the concentration range 0.5-50 pg/mL with the limit of quantification of 0.5 pg/mL (limit of quantitation, LOQ) for OP 1206. The calibration curve of OP 1206 standards spiked in five individual plasma samples was linear ($r^2=0.9999$). Accuracy and precision at the concentrations of 0.5, 1.5, 5.0 and 40 pg/mL, and at the lower LOQ of 0.5 pg/mL were excellent at 20%. OP120 < 6 was stable in plasma samples for at least 24 hours at room temperature, 24 hours frozen at $-70^{\circ}C$, 24 hours in an auto sampler at $6^{\circ}C$, and for two freeze/unfreezing cycles. The validated determination method successfully quantified the concentrations of OP 1206 in plasma samples from simulated administrating a single $5{\mu}g$ OP 1206 formulation. Thus, this novel LC-MS/MS technique for drug separation, detection and quantitation is expected to become the standard highly-sensitive detection method in bioanalysis and to be applied to many low dose pharmaceutical products.

레미콘 슬러지를 활용한 콘크리트블록 활용에 대한 기초 연구 (A Study on the Possibility of Using Concrete Blocks with Ready Mixed Concrete Sludge)

  • 정재호
    • 한국건축시공학회지
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    • 제19권4호
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    • pp.307-312
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    • 2019
  • 레미콘 제조 시 발생되는 슬러지는 폐기물로 분류되어 높은 비용을 지불하며 처리를 하고 있다. 특히 중소레미콘 업체에서는 이 비용이 큰 부담으로 작용되며, 일부 업체에서는 불법적인 처리가 발생되고 있는 실정이다. 따라서 본 연구에서는 레미콘슬러지를 콘크리트블록용 조성물로 재활용하는 방법을 제시 하는데 그 목적이 있다. 레미콘슬러지를 단순 건조하여 사용 하였을 때에는 슬러지에 포함된 잔류화학혼화제와 에트린가이트가 존재하여 콘크리트블록의 압축강도, 동결융해 후 압축강도 물리적성능이 크게 떨어져 콘크리트호안 및 옹벽블록의 품질기준을 만족하지 못하는 것으로 나타났다. 물리적 성능을 만족시키기 위한 방법으로 레미콘슬러지를 $900^{\circ}C$정도의 고온에서 소성시켜 에트린가이트와 잔류 화학혼화제 등을 분해시킨 후 사용하는 것이 우수한 것으로 나타났다.

Effect of pumice powder and artificial lightweight fine aggregate on self-compacting mortar

  • Etli, Serkan;Cemalgil, Selim;Onat, Onur
    • Computers and Concrete
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    • 제27권3호
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    • pp.241-252
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    • 2021
  • An experimental program was conducted to investigate the fresh properties, mechanical properties and durability characteristics of the self-compacting mortars (SCM) produced with pumice powder and Artificial Lightweight Fine Aggregate (aLWFA). aLWFA was produced by using fly ash. A total of 16 different mixtures were designed with a constant water-binder ratio of 0.37, in which natural sands were partially replaced with aLWFA and pumice powder at different volume fractions of 5%, 10% and 15%. The artificial lightweight aggregates used in this study were manufactured through cold bonding pelletisation of 90% of class-F fly ash and 10% of Portland cement in a tilted pan with an ambient temperature and moisture content. Flowability tests were conducted on the fresh mortar mixtures beforehand, to determine the self-compacting characteristics on the basis of EFNARC. To determine the conformity of the fresh mortar characteristics with the standards, mini-slump and mini-V-funnel tests were carried out. Hardened state tests were conducted after 7, 28 and 56 days to determine the flexural strength and axial compressive strength respectively. Durability, sorptivity, permeability and density tests were conducted at the end of 28 days of curing time. The test results showed that the pumice powder replacement improved both the fresh state and the hardened state characteristics of the mortar and the optimum mixture ratio was determined as 15%, considering other studies in the literature. In the aLWFA mixtures used, the mechanical and durability characteristics of the modified compositions were very close to the control mixture. It is concluded in this study that mixtures with pumice powder replacement eliminated the negative effects of the aLWFA in the mortars and made a positive contribution.