• Title/Summary/Keyword: temperature stable characteristics

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Synthesis and Formation Mechanism of Cobalt Doped Willemite Blue Pigments (Co-Doped Willemite 파란색 안료의 합성과 생성기구)

  • Hwang, Dong-Ha;Han, Kyong-Sop;Lee, Byung-Ha
    • Journal of the Korean Ceramic Society
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    • v.47 no.6
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    • pp.603-607
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    • 2010
  • Turquoise blue pigment of Vanadium-zircon blue (DCMA number 14-42-2), which was already commercialized, was stable to be reproduced but insufficient to give strong blue. However, it possible to obtain more intense blue by partially substituting cobalt ions into the willemite($Zn_2SiO_4$) lattice classified into DCMA number 7-10-2 for blue ceramic pigment. By the composition of willemite $Co_xZn_{2-x}SiO_4$(X=0.01, 0.03, 0.05, 0.07, 0.09 mole), this study used reagent grade zinc oxide, cobalt oxide and silicon dioxide as starting materials, carrying out the synthesis with solid reaction method by adding $H_3BO_3$ as a mineralizer. The firing temperature was between $1200^{\circ}C$ and $1400^{\circ}C$. The characteristics of synthesized pigment were analyzed by X-ray diffraction, Raman spectroscopy and SEM and the characteristics of color tones were analyzed by UV-Vis spectroscopy and CIE-$L^*a^*b^*$ measurement. As a result, the optimal composition was $Zn_{1.95}Co_{0.05}$ with 1wt% of $H_3BO_3$ as a mineralizer and firing condition was $1350^{\circ}C$/3 h. $L^*a^*b^*$ value was 29.25, 41.03, -59.93 for on glaze pigment and 37.03, 36.41, -60.03 for under glaze pigment.

Characteristics of α-Tocopherol-loaded Nanostructured Lipid Carriers and their Stabilization Effect (α-Tocopherol을 함유한 Nanostructured Lipid Carriers의 특성과 안정화 효과)

  • Jun, Yoon Kyung;Lim, Yoon Mi;Jin, Byung Suk
    • Applied Chemistry for Engineering
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    • v.26 no.6
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    • pp.659-665
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    • 2015
  • Loading of hydrophobic ${\alpha}$-tocopherol into nanostructured lipid carrier (NLC) was performed for improving its oxidative stability. First, various NLCs with different constituents and mixing ratios were prepared and their characteristics were investigated. While the stable NLCs were made when cetyl palmitate (CP) or glyceryl monosterate (GMS) was used as a solid lipid, the phase separation occurred in the NLCs consisting of stearic acid. Particle sizes of the NLCs were several hundreds of nanometers and the size decreased with increasing the ratio of solvent to lipid. It was examined from DSC thermogram and anisotropy test that the degree of crystallinity of the lipid phase decreased and the lipid matrix became less ordered when octyldodecanol, a long chain fatty alcohol, was added into the solid lipid. The oxidative stability of ${\alpha}$-tocopherol in NLC was remarkably improved compared to that in solution or emulsion under high temperature ($45^{\circ}C$) and UV radiation, which was verified through DPPH test and peroxide value measurement.

Characteristics of the Algal Growth inhibition Substances Produced by Alteromonas sp. SR-14 (Alteromonas sp. SR-14가 생산하는 조류증식 저해 물질의 특성)

  • 김지회;이희정;이태식;김형락;이명숙;장독석
    • Journal of Food Hygiene and Safety
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    • v.14 no.3
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    • pp.270-276
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    • 1999
  • In previous reports, the authors isolated the algicidal marine bacterium, Alteromonas sp. SR-14 and demonstrated its growth inhibition of diatom, Chaetoceros calcitrans (C. calcitrans). In this paper, we studied the effects of cell free culture filtrate of Alteromonas sp. SR-14 on the growth of C. calcitrans, and the characteristics of the algal growth inhibition substance. The culture filtrate of Alteromonas sp. SR-14 grown in peptone broth showed growth inhibition activity against C. calcitrans. The reasonable culture conditions of the bacterium for producing of algal growth inhibition substances were $15~20^{\circ}$ in temperature, 7.0-9.0 in pH and $23~30{\textperthousand}$ in salinity, respectively. The algal growth inhibition activity of culture filtrate was increased from stationary phase in growth curve of Alteromonas sp. SR-14. The molecular weights of algal growth inhibition substances produced by Alteromonas sp. SR-14 were ranged about from 3 KDa to 12 KDa. Among the substances, less than 10 KDa fraction were stable by heating at $100^{\circ}$ for 10 minutes, while more than 10 KDa fraction were heat labile. According to the experimental results, the algal growth inhibition substance produced by the bacterium was not a single compound.

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Design of Phase Locked Dielectric Resonator Oscillator with Low Phase Noise for X-band (저위상잡음을 갖는 X-band용 위상고정 유전체 공진 발진기의 설계 및 제작)

  • 류근관
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.8 no.1
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    • pp.34-40
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    • 2004
  • The PLDRO(Phase-Locked Dielectric Resonator Oscillator) with low phase noise is designed for X-band. The phase of VCDRO(Voltage Controlled Dielectric Resonator Oscillator) is locked to that of a high stable reference oscillator by using a SPD(Sampling Phase Detector) to improve phase noise performance in the loop bandwidth. And, the VCDRO is implemented using a high impedance inverter coupled with dielectric resonator to improve the phase noise performance out of the loop bandwidth. This PLDRO exhibits the harmonic rejection characteristics of 51.67㏈c and requires below 1.95W. The phase noise characteristics are performed as -107.17㏈c/Hz at 10KHz offset frequency and -113.0㏈c/Hz at 100KHz offset frequency, respectively, at ambient. And the output power of 13.0㏈m${\pm}$0.33㏈ is measured over the temperature range of $-20 ∼ +70^{\circ}C$ .

A Study on Structural Characteristics of SM490A TMC Thick Steel Plates (SM490A TMC 후판강재의 소재 및 용접부 특성에 관한 연구)

  • Kim, Jong Rak;Park, Yang Hee
    • Journal of Korean Society of Steel Construction
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    • v.15 no.3
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    • pp.331-339
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    • 2003
  • The study discussed in this paper investigated the material characteristics for the Thermo-Mechanical Control Process(TMCP) plates, which are controlled by several factors such as rolling, cold-stripping, cooling rate, and fixed carbon quantity. The suitability of thick TMCP steel plates as structural steel was also estimated through several experiments and with the us of a statistical method to analyze mill certificate sheets provided by the manufacturer. The results of this study are as follows: the TMCP steel plates showed stable values of the composition parameter ($P_cm$) and the carbon equivalents ($C_eq$ ) with satisfied yield strength, ultimate strength, and low-yield ratio.

Morphological and Cytogenetic Analysis of Colchicine-induced Tetraploids of Fallopia multiflolra Haraldson (Colchicine 처리에 의해 유기된 4배체 하수오의 형태 및 세포유전학적 특성)

  • Kim, Ki Hyun;Youn, Cheol Ku;Kim, In Jae;Lee, Kyung Ja;Kim, Young Ho;Hong, Seong Tack;Woo, Sun Hee
    • Korean Journal of Medicinal Crop Science
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    • v.26 no.5
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    • pp.362-369
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    • 2018
  • Background: For stable induction of tetraploidy in Fallopia multiflora Haraldson, colchicine was treated to establish the condition of induction and investigated the morphological and cytogenetic traits of the tetraploid plants obtained compared to those of diploid ones. Methods and Results: For the induction of tetraploidy, F. multiflora plants were soaked in aqueous solutions of colchicine at various concentration (0.1, 0.5, and 1.0%). After this, 2% dimethyl sulfoxide (DMSO) was added at room temperature on a shaker set at 150 rpm for periods of 12, 24, and 48 h. The induction rate of tetraploids appeared to be the highest in plants treated with 0.5% colchicine for 24 h. As the colchicine concentration and soaking time increased above these levels, the growing tip of the roots did not develop and they began to rot. When compared to diploid plants, tetraploids differed greatly in various characteristics, including the sizes and shapes of the leaves, fruits, flowers and roots. The induced tetraploid F. multiflora had larger guard cells, and chloroplasts, increased number of chloroplast in the guard cells and decreased stomatal densities. Conclusions: When colchicine induced plants for tetraploid, it can be distinguished from diploids, in various characteristics such as morphological changes as stomatal size, number of chloroplasts per guard cell, number of chromosomes and flow cytometry. Therefore, it proved that these methods are suitable, quick and easy methods for the identification of the ploidy level of F. multiflora.

An implementation of NDIR type $CO_2$ gas sample chamber and measuring hardware for capnograph system in consideration of the time response characteristics (시간응답특성을 고려한 2광원 1센서 방식의 capnograph 시스템용 NDIR식 $CO_2$ 가스 챔버 설계 및 측정 회로의 구현)

  • Park, I.Y.;Lee, I.K.;Lee, S.K.;Kang, K.M.;Kang, S.W.;Cho, J.H.
    • Journal of Sensor Science and Technology
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    • v.10 no.5
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    • pp.279-285
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    • 2001
  • The capnograph system for determining the partial pressure of carbon dioxide in the blood of a patient was developed based on the NDIR(non-dispersive infrared) absorption technology. NDIR gas analyzing method requires an optical absorption chamber and signal processing hardware. In this paper, we have designed and implemented NDIR type $CO_2$ gas chamber in consideration of the time response characteristics and lamp chopping frequency. And we have implemented signal processing hardware using two infrared sources to reduce the thermal background effect. The implemented gas chamber and signal processing hardware were tested in the temperature variation experiment and human expiratory experiment. The results showed that the system could produce a stable output signal and a good $CO_2$ gas concentration curve like a typical capnogram.

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Nutritional Characteristics and Physiological Functionality of Lipase Inhibitor-Containing Desmodium oxyphyllum DC. Extracts (지질분해효소 저해물질 함유 도둑놈의 갈고리 추출물의 영양특성 및 생리기능성)

  • Lee, Jong-Kug;Kang, Min-Gu;Lee, Jong-Soo
    • The Korean Journal of Food And Nutrition
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    • v.24 no.2
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    • pp.153-158
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    • 2011
  • This study was performed to develop new anti-obesity agents from medicinal plants for functional food industry. We prepared lipase inhibitor-containing ethanol extracts from Desmodium oxyphyllu DC. and its nutritional characteristics, stability of temperature and pH and physiological functionalities were investigated. Crude lipid content and curde protein content of ethanol extract from Desmodium oxyphyllum DC. were 26.5% and 5.7%, respectively and its asparagine content was 4,860 mg/100 g, dry basis. The ethanol extracts were also stable from pH 3.0 to pH 9.0 and below $80^{\circ}C$. The ethanol extract were showed high lipase inhibitory activity of 74.2% and acetylcholinesterase inhibitory activity of 68.4%.

Design of Local Oscillator with Low Phase Noise for Ka-band Satellite Transponder (Ka-band 위성 중계기용 저위상잡음 국부발진기의 설계 및 제작)

  • 류근관;이문규;염인복;이성팔
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.13 no.6
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    • pp.552-559
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    • 2002
  • The EM(Engineering Model) LO(Local Oscillator) is designed for Ka-band satellite transponder. The VCO(Voltage Controlled Oscillator) is implemented using a high impedance inverter coupled with dielectric resonator to improve the phase noise performance out of the loop bandwidth. The phase of VCO is locked to that of a stable OCXO(Oven Controlled Crystal Oscillator) by using a SPD(Sampling Phase detector) to improve phase noise performance in the loop bandwidth. This LO exhibits the harmonic rejection characteristics above 43.83 dBc and requires 15 V and 160 mA. The phase noise characteristics are performed as -102.5 dBc/Hz at 10 KHz offset frequency and -104.0 dBc/Hz at 100 KHz offset frequency, respectively, with the output power of 13.50 dBm$\pm$0.33 dB over the temperature range of -20~+7$0^{\circ}C$.

Effects of Alloying Elements on the High Pressure Wear Characteristics of Ductile Cast Iron II - Silicon and Molybdenum (구상흑연주철의 고압하 마멸특성에 미치는 합금원소의 영향 II-Si, Mo)

  • Bang, Woong-Ho;Kang, Choon-Sik;Park, Jae-Hyun;Kweon, Young-Gak
    • Journal of Korea Foundry Society
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    • v.20 no.4
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    • pp.240-246
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    • 2000
  • Surface layer properties such as composition, phase, hardness, and oxide layer condition are very important if the main failure mechanism of metals is wear. Generally, stable and dense oxide layers are known to decrease the wear rate of metals by prohibition of metallic junction occurred between bare metals. Addition of Si above 4 wt% to DCI(Ductile Cast Iron) is reported to enhance the significant oxidation resistance by forming the silicon-rich surface layer which inhibits further oxidation. And addition of up to 2 wt% Mo to high Si ductile iron produces significant increases in high temperature tensile strength, creep strength, thermal fatigue resistance and oxidation resistance. High pressure wear characteristics of unalloyed DCI(Ductile cast Iron), 4.46 wt% Si ductile iron, 4.3 wt% Si-0.52 wt% Mo ductile iron were investigated through unlubricated pin-on-disc wear test. Wear test was carried out at speed of 23m/min, under pressure of 3 MPa and 3.3 MPa. Wear surfaces of each specimen were observed by SEM to determine the wear mechanism under high pressure wear condition. Addition of Si 4.46 wt% severely deteriorated wear property of ductile iron compared to unalloyed DCI. But combined addition of Si 4.3 wt%andMo0.52wt%decreasedthefrictioncoefficient(${\mu}$)ofductileironsandremarkablydelayedthemild-severeweartransition.

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