• 한국전기전자재료학회논문지
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• 제17권1호
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• pp.59-64
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• 2004

We have fabricated the polymer dispersed liquid crystal (PDLC) cell where a control of phase separation is very important. The factors to influence the phase separation are mixing ratio of LC and polymer, curing temperature and UV intensity. In this paper, we inspected the change of a phase separation as a function of curing temperature for the mixture of E7 and. NOA65 with different ratios. When the LC concentration is less than polymer such as LC:NOA65 = 40:60wt％, the PDLC cell is influenced strongly by the curing temperature. However, when the LC concentration is much less than polymer such as LC:NOA65 = 80:20wt％, it is influenced slightly by the curing temperature. The reason is because the mixture shows upper critical solution temperature behavior and therefore it is important to know the behavior of phase separation as a function of curing temperature of the mixture.

• Fibers and Polymers
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• 제2권2호
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• pp.98-107
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• 2001

The phase transition behavior isothermal micro-phase separation kinetics of polyester-based thermoplastic elastomer were studied using the synchrotron X-ray scattering(SAXS) method. The structural changes occurring during heating period were investigated by determining the changes of the one-dimensional correlation function, interfacial thickness and Porod constant. Based on the abrupt increases of the domain spacing and interfacial thickness, a major structural change occurring well below the melting transition temperature is suggested. Those changes are explained in terms of melting of the thermodynamically unstable hard domains or/and the interdiffusion of the hard and soft segments in the interfacial regions. SAXS profile changes during the micro-phase separation process were also clearly observed at various temperatures and the separation rate was found to be sensitively affected by the temperature. The peak position of maximum scattering intensity stayed constant during the entire course of the phase separation process. The scattering data during the isothermal phase separation process was interpreted with the Cahn-Hilliard diffusion equation. The experimental data obtained during the early stage of the phase separation seems to satisfy the Cahn-Hilliard spinodal mechanism. The transition temperature obtained from the extrapolation of the diffusion coefficient to zero value turned out to be about 147$\pm$$2^{\circ}$, which is close to the order-disorder transition temperature obtained from the Porod analysis. The transition temperature was also estimated from the inveriant growth rate. By extrapolating the inveriant growth rate to zero, a transition temperature of about 145$\pm$$\pm$$2^{\circ}$ was obtained.

• Nuclear Engineering and Technology
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• 제51권7호
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• pp.1866-1870
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• 2019

Residual salt separation is an essential step in pyroprocessing because its reaction products, as prepared by electrochemical unit processes, contain frozen residual electrolyte species, which are generally composed of alkali-metal chloride salts (e.g., LiCl, KCl). In this study, a simple technique that utilizes high-temperature gas flux as a driving force to melt and push out the residual salt in the reaction products was developed. This technique is simple as it only requires the use of a heating gun in combination with a gas injection system. Consequently, $LiNO_3-ZrO_2$ and $LiCl-ZrO_2$ mixtures were successfully separated by the high-temperature gas injection (separation efficiency > 93%), thereby demonstrating the viability of this simple technique for residual salt separation.

• Tribology and Lubricants
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• 제32권5호
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• pp.166-171
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• 2016

Electric vehicle ownership is expanding for two reasons: its technology features have enhanced fuel economy, and the number of vehicle emissions regulations is increasing. Battery performance has a large influence on the capability of electric vehicles, and even though battery thermal management has been actively researched, specific technological improvements to battery performance are not being presented. For instance, many industrial applications utilize vortex tubes as components for refrigeration machines because of their numerous intrinsic benefits. If electric vehicles incorporate vortex tubes for battery cooling, performance and efficiency advancements are possible. This study uses a counter-flow vortex tube to investigate its temperature separation characteristics, based on the back pressure of the cold air exit and the difference between the inlet and back pressures. The experiment uses a vortex tube with the following parameters: six nozzle holes, a 20 mm inner vortex diameter (D), a 14D tube length, a 0.7D cold exit orifice diameter, and a nozzle area ratio of 0.142. The measurements prove that the temperature difference between the hot air and cold air decreased because of the flow resistance of the hot air and the backflow phenomenon at the cold air exit. The flow resistance causes the temperature difference to decrease, and the back pressure of the cold air exit influences the flow resistance. The results show that the back pressure significantly influences the efficiency of temperature separation.

• 대한기계학회논문집B
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• 제30권2호
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• pp.177-185
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• 2006

This study aims deriving analysis the flow characteristic of kitchen hood system with using 3-D numerical analysis method and improving the system to expel pollutes more efficiently. To understand the flow characteristics of four models, this study only focuses on velocity field, temperature field, and concentration field varying with followings whether separation plate is set or not and the shapes of separation plates. The quantity of air, speed of exhaust fan and temperature and concentration of heating source are concerned as constant values. The three models having different shapes have one exhaust port and the model which has the vent at the closest position to where pollutes are generated is discovered to be the most efficient model. Compare to the initial model (having no separation plate), it was $1.4-1.9\%$ more efficient at temperature distribution and $9.4-11.9\%$ more at $CO_2$ concentration distribution.

• 한국자동차공학회논문집
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• 제18권1호
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• pp.93-98
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• 2010

An object of this study is to confirm the opening amount of the throttle valve that is begun the temperature separation of vortex tube for various engine speed and load condition in a common rail diesel engine. The vortex tube located at downstream of the exhaust manifold is a device separating the incoming exhaust gas to hot and cold stream. To find optimum separation efficiency of vortex tube, the opening amount of throttle valve has been investigated for various engine speed and load conditions. Engine speed was found that the influence of engine speed was dominant compared with that of engine load. As engine speed was increased, the throttle opening amount starting temperature separation was reduced.

• 한국자동차공학회논문집
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• 제10권4호
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• pp.69-76
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• 2002

The aim of this study is to provide fundamental informations that make it possible to use a cool stream and a hot stream simultaneously. We changed the pressure of compressed air that flows into a tube, the inner diameter of orifice that a cold stream exits, and the mass flow rate ratio. And in each case, we measured the temperature of a cold stream and a hot stream in each exit of a tube. Also we measured the axial and the radial temperature distribution in internal spare of a tube. From the study, fellowing conclusive remarks 7an be made. First, As the number of nozzles increase, separation point move into the hot exit. Second, When we use guide vane type nozzle, the axial temperature distribution constant over the 0.75 of air mass flow rate radio. Third, When we use Spiral type nozzle, axial and radial temperature distribution in the inner space is higher than another nozzle. Fourth, Axial and radial temperature distribution in the inner space vortex-tube is determined by separation point. And separation point is moved by changing of air mass flow rate ratio. At last, A heating apparatus is possible far vortex-tube to use.

• 한국해양공학회지
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• 제9권2호
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• pp.123-132
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• 1995

During compression molding of fiber-reinforced polymeric composites, microstructural changes such as the fiber-matrix separation and the fiber orientation are occurred by the flow of composite materials. Since the nonhomogeneity and anisotropy of composites are caused by the separation and orientation of fibers. On the other hand, the separation and the orientation of fibers are inseparably related to each other. In this paper the degree of nonhomogeneity which is a measure of the separation is obtained using one-dimensional rectangular shaped part compression molding. And the orientation function is measured by the image processing using soft X-rayed photograph and image scanner. We study effects of the mold temperature on the degree of nonhomogeneity and the orientation function.

• 한국환경과학회지
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• 제10권5호
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• pp.381-386
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• 2001

The characteristics of precipitation separation and solvent extraction separation of magnesium from the waste bittern were studied experimentally In the result of precipitation separation, the size of magnesium hydroxide precipitated was not affected on pH, but decreased with increasing the precipitation temperature. The purity of magnesium oxide precipitated was increased with pH beyond pH 11. From the solvent extraction separation, the equilibrium extraction ratio of magnesium was increased with pH and temperature of extraction phase, the concentration of stripping phase, and with decreasing pH of stripping phase. The extractant of Aliquat 336 and Acid 810 mixture was more effective than that of DCH18C6 and $D_2EHPA$ mixture in the extraction separation of magnesium.

• Biotechnology and Bioprocess Engineering:BBE
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• 제5권1호
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• pp.17-22
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• 2000

The separation of tryptophan enantiomers was carried out with medium-pressure liquid chromatography using BSA (bovine serum albumin)-bonded silica as a chiral stationary phase. The influence of various experimental factors such as pH and ionic strength of mobile phase, separation temperature, and the presence of organic additives on the resolution was studied. In order to expand this system to preparative scale, the loadability of sample and the stability of stationary phase for repeated use were also examined. The separation of tryptophan enantiomers was successful with this system. The data indicated that a higher separation factor (a) was obtained at a higher pH and lower temperature and ionic strength in mobile phase. Addition of organic additives (acetonitrile and 2-propanol) in mobile phase contributed to reduce the retention time of L-tryptophan. About $30\%$ of the separation factor was reduced after 80 days of repeated use.