• 제목/요약/키워드: temperature cycles

검색결과 881건 처리시간 0.025초

Mechanical Properties of Cf/SiC Composite Using a Combined Process of Chemical Vapor Infiltration and Precursor Infiltration Pyrolysis

  • Kim, Kyung-Mi;Hahn, Yoonsoo;Lee, Sung-Min;Choi, Kyoon;Lee, Jong-Heun
    • 한국세라믹학회지
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    • 제55권4호
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    • pp.392-399
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    • 2018
  • $C_f/SiC$ composites were prepared via a process combining chemical vapor infiltration (CVI) and precursor infiltration pyrolysis (PIP), wherein silicon carbide matrices were infiltrated into 2.5D carbon preforms. The obtained composites exhibited porosities of 20 vol % and achieved strengths of 244 MPa in air at room temperature and 423 MPa at $1300^{\circ}C$ under an Ar atmosphere. Carbon fiber pull-out was rarely observed in the fractured surfaces, although intermediate layers of pyrolytic carbon of 150 nm thickness were deposited between the fiber and matrix. Fatigue fracture was observed after 1380 cycles under 45 MPa stress at $1000^{\circ}C$. The fractured samples were analyzed by transmission electron microscopy to observe the distributed phases.

정극재료용 $Li_{2}O-P_{2}O_{5}-V_{2}O_{5}$계 결정화 유리의 전기화학적 특성 (Electrochemical Properties of $Li_{2}O-P_{2}O_{5}-V_{2}O_{5}$ Glass-ceramics for cathode Material)

  • 손명모;이헌수;김종욱;김윤선;구할본
    • 한국전기전자재료학회논문지
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    • 제14권8호
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    • pp.652-657
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    • 2001
  • Vanadate glasses containing 10~20mol% glass former, P$_2$O$_{5}$ were prepared by melting the batch in platinum crucible and quenching on the copper plate. Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ glass-ceramics having LiV$_3$O$_{8}$ were obtained by heat-treatment of this glass in crystallization temperature. The glass-ceramics showed singnificantly good capacity and long cycles life according to heating condition. In this paper, we described electrochemical properties during crystallization process and found the best crystallizaton condition of Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ glass as cathode material. Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ glass-ceramics heat-treated at 233$^{\circ}C$ for 3 hors showed good rechargeable capacity of 220mAh/g in the cycling range between 2.0 and 3.9V.en 2.0 and 3.9V.

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Si 첨가에 따른 리튬 이차 박막 전지용 주석 산화물 박막의 음극 특성 (Anode Characteristics of Tin Oxide Thin Films According to Various Si Additions for Lithium Secondary Microbattery)

  • 박건태;박철호;손영국
    • 한국세라믹학회지
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    • 제40권1호
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    • pp.69-76
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    • 2003
  • 리튬이차 박막전지로서, 실리콘 첨가(0, 2, 6, 10, 20㏖%)에 따른 주석 산화물 박막을 기판온도 30$0^{\circ}C$, Ar:O$_2$=7:3으로 R.F. magnetron sputtering법으로 제조하였다. 실리콘의 함량이 증가함에 따라, Si-O 결합량이 증가하고 Sn-O 결합량은 감소하였다. 적정량의 실리콘 첨가는 주석의 산화상태를 감소시켜 비가역성을 줄이고 충방전 동안 주석의 부피변화를 막아 사이클 특성이 향상되는 결과를 보여주었다. 6㏖% Si를 첨가한 주석 산화물 박막은 100사이클동안 700mAh/g의 용량을 가지는 가장 좋은 사이클 특성을 나타내었다.

산소동위원소 분석을 이용한 신석기시대 연대도 패총의 굴 (Crassostrea gigas) 채집 계절성 연구 (Seasonality of shellfish gathering using oxygen isotope analysis of Crassostrea gigas from the Neolithic Yeondae-do shell midden site, Tongyeong, Korea)

  • 안덕임;이인성
    • 한국패류학회지
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    • 제31권1호
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    • pp.43-48
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    • 2015
  • Oxygen isotope ratios (${\delta}^{18}O$) of three Pacific oyster (Crassostrea gigas) specimens from the Neolithic Yeondae-do shell midden site, Tongyeong, Korea, were analyzed to determine the seasonality of shellfish gathering and site occupation. Oxygen isotope samples were taken from the left valve hinge sections of the specimens. Oxygen isotope values ranged between -0.1 ‰ and -2.4 ‰, between -0.2 ‰ and -2.9 ‰, and between 0.3 ‰ and -2.8 ‰ in oyster specimen #one, #two and #three, respectively. The isotope profiles showed seasonal temperature cycles, providing information related to the seasonality of shellfish gathering and site occupation. Hinge-edge oxygen isotope values of the specimens showed decreasing trends after passing through maximum values (winter), indicating that they formed during spring. Thus it can be assumed that during spring season, oysters were gathered and the site was occupied.

An Experimental Study on the Performance of Inverter Heat Pump with a Variation of Frequency and Capillary Size

  • Choi, Jong-Min;Kim, Yong-Chan;Kim, Jong-Yup
    • International Journal of Air-Conditioning and Refrigeration
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    • 제6권
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    • pp.27-35
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    • 1998
  • An experimental study was performed to investigate the optimum cycle of an inverter heat pump as a function of frequency. The performance of the inverter heat pump with the rated cooling capacity of 4,141 W(3,550kcal/h) was measured with a variation of frequency, indoor and outdoor temperature, and length of capillary tube in the psychrometric test room. As a base case, the inverter heat pump with the standard capillary length of l,000mm(optimum size for the frequency of 60Hz) and ASHRAE Test condition "A" was tested by varying frequency from 30Hz to 80Hz. Then, the optimum cycles were investigated by varying the length of capillary tube at each frequency level of 30, 60 and 80Hz. Based on the experimental data, the change of system characteristics between the optimum and the base case were analyzed for each selected frequency level. Generally, for low frequency level(30Hz), the longer length of the capillary tube compared with the standard size showed the higher energy efficiency ratio(EER), while for high frequency level(80Hz) the shorter length of the capillary tube showed the higher EER.

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The Performance Evaluation of R407C and R410B in a Residential Window Air-Conditioner

  • Kim, Man-Hoe;Shin, Jeong-Seob;Kim, Kwon-Jin
    • International Journal of Air-Conditioning and Refrigeration
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    • 제6권
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    • pp.148-157
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    • 1998
  • This study presents test results of a residential window air-conditioner using R22 and two potential alternative refrigerants, R407C and R410B. A series of performance tests has been carried out for the basic and liquid-suction heat exchange cycles in a psychometric calorimeter test facility. For R407C, the same rotary compressor was used as in the R22 system. However, compressor for the R410B system was modified to provide the similar cooling capacity. The evaporator circuit was changed to get a counter-cross flow heat exchanger to take advantage of zeotropic mixture's temperature glide, and liquid-suction heat exchange cycle was also considered to improve the system performance. Test results were compared with those for the basic R22 system. The modified system with a liquid-suction heat exchanger increased cooling capacity and energy efficiency by up to 5%.

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소형 암모니아 흡수식 냉난방기의 난방성능 특성 (The Characteristics of Heating Performance on Small Sized Ammonia Absorption System)

  • 진병주;오승택;윤정인;황준현;진심원
    • 대한설비공학회:학술대회논문집
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    • 대한설비공학회 2008년도 하계학술발표대회 논문집
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    • pp.120-123
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    • 2008
  • Refrigeration plants using absorption principles have been around for many years with initial development taking place over 100 years ago. Although the majority of absorption cycles are based on water-LiBr cycle, many applications exist where ammonia-water can be used, especially where lower temperatures are desirable. In both systems water is used as working fluid, but in quite different ways: as a solvent for the ammonia system, and as refrigerant for the lithium bromide system. This explains that the lithium bromide absorption system is strictly limited to evaporation temperatures above $0^{\circ}C$. The main industrial applications for refrigeration are in the temperature range below $0^{\circ}C$, the field for the binary system ammonia-water.

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초음파 검사법을 이용한 STS304 배관재 내부 균열 측정 방법에 대한 연구 (A study on the detection method of inner's crack of STS304 pipe using Ultrasonic Testing)

  • 황웅기;이경민;우영관;서덕희;이보영
    • 한국전산구조공학회:학술대회논문집
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    • 한국전산구조공학회 2011년도 정기 학술대회
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    • pp.415-418
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    • 2011
  • Thermal fatigue is one of the life-limiting damage mechanisms in the nuclear power plant conditions. The turbulent mixing of fluids of different temperatures induces rapid temperature changes to the pipe wall. The successive thermal transients cause varying cyclic thermal stresses. These cyclic thermal stresses cause fatigue crack nucleation and growth similar to the cyclic mechanical stresses. The aim of this study was to fulfil the need by developing an real crack manufacturing method, which would produce realistic cracks. The test material was austenitic STS 304, which is used as pipelines in the reactor coolant system of a nuclear power plants. In order to fabricate thermal fatigue crack similar to realistic crack, successive thermal transients were applied to the specimen. Thermal transient cycles were combined with heating (60sec) and cooling cycle (30sec). And, In order to identify ultrasonic characteristic, it was performed the ultrasonic reflection measuring method for the fabricated specimen. From the results of ultrasonic reflection measuring testing, it was conformed that A-scan results(average 83% of real crack depth) for the TFC reference specimen was more enhanced NDT reliability than results(average 38% of real crack depth) for the EDM notch reference specimen.

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Immobilization and Characterization of Tannase from a Metagenomic Library and Its Use for Removal of Tannins from Green Tea Infusion

  • Yao, Jian;Chen, Qinglong;Zhong, Guoxiang;Cao, Wen;Yu, An;Liu, Yuhuan
    • Journal of Microbiology and Biotechnology
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    • 제24권1호
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    • pp.80-86
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    • 2014
  • Tannase (Tan410) from a soil metagenomic library was immobilized on different supports, including mesoporous silica SBA-15, chitosan, calcium alginate, and amberlite IRC 50. Entrapment in calcium alginate beads was comparatively found to be the best method and was further characterized. The optimum pH of the immobilized Tan410 was shifted toward neutrality compared with the free enzyme (from pH 6.4 to pH 7.0). The optimum temperature was determined to be $45^{\circ}C$ for the immobilized enzyme and $30^{\circ}C$ for the free enzyme, respectively. The immobilized enzyme had no loss of activity after 10 cycles, and retained more than 90% of its original activity after storage for 30 days. After immobilization, the enzyme activity was only slightly affected by $Hg^{2+}$, which completely inhibited the activity of the free enzyme. The immobilized tannase was used to remove 80% of tannins from a green tea infusion on the first treatment. The beads were used for six successive runs resulting in overall hydrolysis of 56% of the tannins.

미립캡슐잠열재 제조 및 축열식 냉방기 적용실험 (An Experimental Study for Manufacturing MPCM Slurry and Its Application to a Cooling System)

  • 이효진;최준규;이재구
    • 설비공학논문집
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    • 제15권5호
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    • pp.352-359
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    • 2003
  • The present study has been conducted for manufacturing MPCM (microencapsulated phase change material) slurry with in-situ polymerization and proving their applicabilities for tooling system. The surface of MPCM is composed of melamine, while tetradecane, paraffin wax, is centered in the MPCM. The produced capsules are observed by the optical microscope and SEM for superficial shapes. Their thermal properties are measured by DSC. Their size distributions are observed by FA particle analyzer. A narrow size distribution from 1 to 10 ${\mu}{\textrm}{m}$ with 5 ${\mu}{\textrm}{m}$ of average diameter was observed. Melting temperature was 6.7$^{\circ}C$. The durability of MPCM was tested with various types of pump such as centrifugal, peristaltic, and mono pumps. During 10000 cycles the fraction of broken capsules was smaller than 6% for the centrifugal and peristaltic pumps, while bigger value of 8% for the mono pump. A cooling system, which adopted MPCM slurry as a media for transporting cold thermal energy, was designed to investigate the performance of the MPCM. The discharging times of 10 and 20 wt% MPCM slurry were lasted up to 105 and 285 minutes longer, respectively, than the water cooling system.