• 분석과학
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• 제20권4호
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• pp.261-267
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• 2007

건축자재에서 방출되는 오염물질을 평가하는 20 L 시험챔버법은 챔버 내부에 노출되는 시료의 표면방출만을 측정한다. 일정한 크기로 절단한 시편을 알루미늄 호일로 감싼 후 시편홀더에 고정시켜 20 L 시험챔버 내에 위치시킨 후 방출시험을 실시한다. 이때 시편홀더의 기밀성이 보장되지 못한다면 시료절단면에서 방출되는 오염물질로 인하여 정확한 평가가 이루어질 수 없다. 이러한 절단면의 영향은 표면처리를 하여 표면에서 보다 절단면에서 더 많은 오염물질이 방출되는 판상재(합판, 장판) 시료의 경우 더 크다. 이 연구에서는 바닥재로 사용되는 장판을 대상으로 20 L 시험챔버와 1 L 시험챔버의 방출시험결과를 비교하여 시편홀더의 기밀성을 확인하였다. 또한 가구재로 사용되는 LPM 양면처리한 MDF를 대상으로 현행의 시험방법과 시료절단면을 VOC 저방출 tape으로 밀봉한 방법을 비교하여 시편홀더의 부족한 기밀성의 개선이 가능하지 확인하였다. LPM 양면처리한 MDF의 7일 경과 후 방출강도는 TVOC의 경우 Tape 사용 유무에 따라 각각 $0.009mg/m^2h$, $0.003mg/m^2h$로 기밀성을 보완할 수 있었다. 또한 n=3에서 상대표준편차가 현행의 방법은 $0.004mg/m^2h$, tape을 사용했을 경우 $0.002mg/m^2h$로 현행 방법의 시험편홀더 기밀성 부족으로 인한 절단면의 불균일한 영향을 VOC 저방출테이프 사용으로 배제할 수 있었다.

• 분석과학
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• 제34권6호
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• pp.251-258
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• 2021

현재까지 강력 사건에서 범인들은 칼을 흉기로 가장 많이 사용하였으며 범죄 현장에 범인이 직접 종이와 테이프로 제작한 간이 칼집이 남아있는 경우가 있다. 다공성 표면에 테이프가 붙어있는 검체는 지문을 현출하기 어려우므로 간이 칼집과 같은 증거물이 발견되었을 때 각 표면에서 지문을 현출하는 적절한 기법과 지문의 분포 위치를 확인하는 실험이 필요하다. 본 연구는 이를 확인하기 위해 간이 칼집 50개를 만들어 테이프 비접착면에 cyanoacrylate fuming (CA fuming)을 사용하여 지문을 현출하고 이중목적 1,2-indanedione/Zn (1,2-IND/Zn) 시약으로 종이와 테이프를 박리함과 동시에 종이에 있는 지문을 현출하였다. 테이프 접착면은 Wet Powder Black^®을 사용하여 지문을 현출하였다. R program을 이용하여 heatmap으로 각 표면에서 지문이 현출된 위치를 표시한 결과, 테이프 접착면의 중간 부분보다 양끝에 지문이 많이 분포되어 있는 것을 확인할 수 있었으며 비접착면과 종이는 뚜렷한 분포 패턴이 나타나는 것은 아니나 개인식별에 이용할 수 있을 정도의 선명도를 가진 지문이 다수 현출된 것을 확인하였다. 범죄 현장에서 간이 칼집이 발견되었을 때 이러한 연구 결과를 참고하여 증거물을 처리할 수 있을 것이다.

• 수산해양기술연구
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• 제27권2호
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• pp.125-131
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• 1991

Electrolyte matrix fabrication process can be classifed as hot pressing, tape casting, callendering, electrophoretic deposition. however, these have limits in practice. Hot pressing is cumbersome method, because of careful heating and cooling. Furthermore, the perfected tile is so fragile that it is difficult to fit in a cell. Therefore this method is not adequate for mass production of the electrolyte matrix. Using electrophoretic deposition method, a very thin matrix can be made, but many attempts of the electrolyte embeding were found to be failure. Tape casting and callendering methods are employed in most of the matrix fabrication for the present. But these methods require lots of water as a solvent, so that coating of the LiAlO sub(2) with electrolyte is difficult. Recently, hot roll milling method has been developed and the perfected matrix was proved to be free from crack. The method, however, needs a roller to make a matrix and a perfected matrix is carefully striped off from the cooled roller. Therefore, this method requires a long time due to the cooling process. The author proposes a cold rolling process. On this method, heated slurry of the LiAlO sub(2) mixed with binder, is rolled with a cold roller. The heated slurry dose not adhere to the roller, since contacted hot slurry is rapidly solidified. Therefore fabrication speed is increased, without getting rid of merits of the hot rolling process.

• Current Optics and Photonics
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• 제1권1호
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• pp.7-11
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• 2017

In this study, multilayered graphene was easily transferred to the target substrate in one step using thermal release tape. The transmittance of the transferred graphene according to the number of layers was measured using a spectrophotometer. The sheet resistance was measured using a four-point probe system. Graphene formed using this transfer method showed almost the same electrical and optical properties as that formed using the conventional poly (methyl methacrylate) transfer method. This method is suitable for the mass production of graphene because of the short process time and easy large-area transfer. In addition, multilayered graphene can be transferred on various substrates without wetting problem using the one-step dry transfer method. In this work, this easy transfer method was used for dielectric substrates such as glass, paper and polyethylene terephthalate, and a sheet resistance of ~240 ohm/sq was obtained with three-layer graphene. By fabricating organic solar cells, we verified the feasibility of using this method for optoelectronic devices.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 2002년도 학술대회 논문집
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• pp.149-152
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• 2002

SrZrO3 resistive oxide barriers on Ag sheathed Bi2223 tapes prepared by the sol-gel and dip coating method were evaluated with an aid of Taguchi method and orthogonal arrays to elucidate the effects of experimental parameters, such as ratio of starting solution, amount of additives, and heat treatment temperature and time on the properties of the thin films. Six experimental parameters were selected and then Ll8(21x37) orthogonal arrays were constructed. Finally, SEM and XRD results were related to signal to noise (S/N) ratio to evaluate the optimized experimental condition.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 2002년도 학술대회 논문집
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• pp.315-317
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• 2002

The value of I$_{c}$(critical current) in HTS (High Temperature Superconducting) tape has a great influence on B(equation omitted) (magnetic field amplitude applied perpendicular to the tape surface). Therefore, I$_{c}$ of HTS magnet is determined by not only operating temperature but also the B(equation omitted). In shape design of field coil for the HTS motor, a method to reduce the B(equation omitted) and to determine operating current should be considered in order to optimal design. On the basis of the magnetic field analysis, this paper deals with various field coil shape to obtain operating current of HTS motor by using analytical method. And also this paper discusses the operating current of 100hp class HTS motor by using I$_{c}$-B(equation omitted) curve.curve.

• Progress in Superconductivity
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• 제5권1호
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• pp.65-69
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• 2003

Many researches on fabrication process for BSCCO precursor powders have been developed for high J$_{c}$ BSCCO-2223 tape. Spray pyrolysis method for fabrication of precursor powder has many advantages, such as high purity, fine particle size and low carbon content of BSCCO precursor powder. Fine, spherical powders were prepared by ultrasonic spray pyrolysis from the aqueous solution of metal nitrates. BSCCO precursor powders were synthesized with various solutes concentration and heat treatment conditions. Average particle size for spray pyrolysis powders was $1.5∼3\mu\textrm{m}$. Bi-2223/Ag tape was prepared by PIT method and followed by various sintering conditions. BSCCO precursor powders were characterized by XRD, SEM, EDS, Carbon content and particle size analysis.s.

• Progress in Superconductivity
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• 제3권2호
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• pp.193-197
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• 2002

There are many problems in wire fabrication of long length Bi-2223 superconductor by using conventional extrusion method. They are mainly due to high surface resistance and inhomogeneous distribution of inner stress. Hydrostatic extrusion process will not only decrease the extrusion pressure but also enhance homogeneous deformation of material by reducing friction force between billet and container Hydrostatic extrusion method is considered to be useful fur fabrication of the homogeneous wire with high density. In this paper, hydrostatic extrusion process is introduced to fabricate Bi-2223 superconducting tape, and also discussed are the interface homogeneity and microstructural aspects of extruded BSCCO/Ag billet.

• KIEE International Transactions on Electrophysics and Applications
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• 제5C권5호
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• pp.204-210
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• 2005

Alternating current (AC) losses of two Bi-2223 ([Bi, Pb]: Sr: Ca: Cu: O = 2:2:2:3) tapes [(Tape I, un-twist-pitch) and the other with a twist-pitch of 10 mm (Tape II)] were measured and compared. These samples, produced by the powder-in-(Ag) tube (PIT) method, are multi-filamentary. Also, it's produced by non-twist and different twist pitch (8, 10, 13, 30, 50 and 70 mm). The critical current measurement was carried out under the environment in liquid Nitrogen and in zero-field by 4-probe method. Susceptibility measurements were conducted while cooling in a magnetic field. Flux loss measurements were conducted as a function of ramping rate, frequency and field direction. The AC flux loss increases as the twist-pitch of the tapes decreased, in agreement with the Norris Equation. Neutron-diffraction measurements have been carried out investigate the crystal structure, magnetic structures, and magnetic phase transitions in Bi-2223([Bi, Pb]:Sr:Ca:Cu:O)

• 한국초전도ㆍ저온공학회논문지
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• 제21권4호
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• pp.34-38
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• 2019

Multilayered high-temperature superconductor coated conductor (CC) tapes are used in an extensive range of applications and are exposed to many stresses such as hoop stress, radial/transverse tensile stress under large Lorentz forces, and thermal stress while cooling if thermal expansion properties differ. Loads induced transversely at the tape surface inevitably create delamination phenomena in the multilayered CC tapes. Thus, delamination behaviors of CC tapes along the c-axis under transverse loading conditions, which can vary based on manufacturing process and constituent layers, must be characterized for applications. The anvil test method was used to mechanically investigate the delamination characteristics of various commercially available Ag-stabilized CC tapes at room temperature and 77 K, finding superior strength at the latter. The wide variations found depended on tape structure and fabrication technique. Fractographic morphologies of delaminated tapes supported the findings under transverse loading conditions.