• 제목/요약/키워드: surface roughness measurement

검색결과 456건 처리시간 0.029초

아연전기도금의 존착성에 미치는 폴리에탈렌글리콜의 영향 (The Effect of polyethlenglycol on Electrocrystallization of zine Coat)

  • 김현태;정원섭;조남웅
    • 한국표면공학회지
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    • 제30권2호
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    • pp.128-135
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    • 1997
  • The effect of the polyethyledglycol(PEG) on the surface morphology and crystal orientation of electrodeposited zinc from a chloride (1.5M Zinc+7.0M chloriode) have been studied by means of electrochemical methodes, scanning electron microscopy, surface appearance measurement and X-ray diffraction patterns. The resistance of electrodeposit increased, whereas the evolution of hydrogen decreased with incrasing of molecular weight of the PEG. Large grains of electrodeposit were obtained from bath in the absence of organid additive. When the PEG was added, fine grained crystals were observed and the surface roughness was relatively small, but surface appearance deteriorated. The preferred orientation with a(101) plane parallel to the surface was obtained from the PEG addited bath.

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초청정한 Si 기판 위에서 Ti의 초기 반응 (Initial Reactions of Ti on the Atomically Clean Si Substrates)

  • 전형탁
    • 분석과학
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    • 제5권3호
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    • pp.303-308
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    • 1992
  • Ti과 Si의 초기 반응이 Titanium Silicide의 표면 거칠기 (Surface roughness)를 고찰하기 위해 연구하였다. 형성기구는 In-situ AES와 LEED의 측정장비로 연구하였다. Ti의 하나나 두 원자층이 초고진공에서 원자적으로 깨끗한 Si 기판 위에 증착되었다. Reconstruction이 된 $7{\times}7$ Si(111) 표면이 초 고진공하에서 얻어졌으며 박막의 증착은 Quartz Crystal Oscillator로 측정되었다. In-situ 측정 결과 Ti과 Si의 초기 반응이 실온에서 일어났으며 Disorder막을 형성하였다. 낮은 온도($200^{\circ}C{\sim}300^{\circ}C$)에서 Ti과 Si의 Intermixing이 고찰되었고 $400^{\circ}C$ 근처에서 $1{\times}1$ Si(111) LEED 패턴이 관찰되었다. 이것은 Disorder막이 Order막으로 변화가 생긴 것을 나타낸다. 더 높은 온도에서 $7{\times}7$ Si(111) LEED 패턴이 재관찰되었는데 이것은 3차원적인 $TiSi_2$의 형성을 증명하는 것이다.

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RF 마그네트론 스퍼터링 공정 조건에 따른 AlN 박막의 배향성, 표면 거칠기 및 압전 특성에 관한 연구 (Orientation, Surface Roughness and Piezoelectric Characteristics of AlN Thin Films with RF Magnetron Sputtering Conditions)

  • 방정호;장동훈;강성준;김동국;윤영섭
    • 대한전자공학회논문지SD
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    • 제43권4호
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    • pp.1-7
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    • 2006
  • RF 마그네트론 스퍼터링 방법을 이용하여 $Ar/N_2$ 가스비와 기판 온도 변화에 따른 AlN 박막의 배향성과 표면 거칠기 그리고 압전 특성의 변화를 조사하였다. 특히, $Ar/N_2$=10/10 (sccm), 기판 온도 $400^{\circ}C$ 일 때 가장 우수한 (002) 배향성을 얻을 수 있었다. AFM 을 이용하여 표면 거칠기를 분석한 결과, 기판 온도 $400^{\circ}C$ 인 경우 $Ar/N_2$ 가스비의 변화에 대해서는 $N_2$의 분압비가 증가할수록 표면 거칠기 특성이 좋아지는 것으로 나타났으며 $Ar/N_2$=0/20 (sccm) 일 때 2.1 nm 로 가장 작은 값을 나타내었다. $Ar/N_2$=10/10 (sccm) 인 조건에서 기판 온도 변화에 대한 표면 거칠기 특성은 기판 온도가 상온에서 $300^{\circ}C$ 로 증가함에 따라 향상되는 경향을 보였으며, $300^{\circ}C$ 에서 3.036 nm 로 최소값을 나타낸 후, 기판 온도가 $300^{\circ}C$ 이상으로 상승하면 표면 거칠기는 다시 열악해지는 것을 확인할 수 있었다. Pneumatic probe 방법을 이용하여 압전 특성을 측정한 결과, $Ar/N_2$=10/10 (sccm), 기판 온도 $400^{\circ}C$ 일 때 Piezoelectric constant ($d_{33}$)=6.01 pC/N 이라는 가장 우수한 값을 나타내었으며, 이는 AlN 박막이 가장 좋은 (002) 배향성을 갖는 조건과 일치하는 것이다.

SEM 측정법에 의한 초정밀 표면가공 특성연구 (A Study on the Surfaces Machining Characteristics of Ultra-precision through SEM Measurement)

  • 강순준;오상록;이갑조;김종관
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2004년도 춘계학술대회 논문집
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    • pp.34-41
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    • 2004
  • The purpose of this paper is to look at the characteristics of surface finishing which is one of the form accuracies and to obtain the fundamental technical data from the process of machining with diamond tool through experiment and theoretical analysis. The experiments were conducted with domestic made ultra-precision machine and MCD.PCD tool, with aluminum alloyed material and brass being used for the work pieces. The goal of the size accuracy was set to 100nm. The most suitable tool nose radius and machining conditions were selected, and the variations of the surface roughness were observed using SEM method while machining the distance of up to 500km. These data were evaluated and they examined the variation of the machined surfaces while cutting up to 500km of machining distance. At the same time, the state for the wear of diamond tool nose was analyzed and carefully examined through the newest measuring device. Additionally, the characteristics of ultra-precision machining technology were studied through visual analysis.

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순 티타늄 판재의 변형 특성 및 성형성 평가 (A Study on Plastic Deformation Characteristics and Formability for Pure Titanium Sheet)

  • 인정훈;정기조;이현석;김정한;김진재;김영석
    • 소성∙가공
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    • 제27권5호
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    • pp.301-313
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    • 2018
  • In this paper, tensile test was performed on pure titanium sheet (CP Ti sheet) with HCP structure in each direction to evaluate mechanical and surface properties and analyze microstructural changes during plastic deformation. We also evaluated forming limits of Ti direction in dome-type punch stretching test using a non-contact three-dimensional optical measurement system. As a result, it was revealed the pure titanium sheet has strong anisotropic property in yield stress, stress-strain curve and anisotropy coefficient according to direction. It was revealed that twinning occurred when the pure titanium sheet was plastic deformed, and tendency depends differently on direction and deformation mode. Moreover, this seems to affect the physical properties and deformation of the material. In addition, it was revealed the pure titanium sheet had different surface roughness changes in 0 degree direction and 90 degree direction due to large difference of anisotropy, and this affects the forming limit. It was revealed the forming limit of each direction obtained through the punch stretching test gave higher value in 90 degree direction compared with forming limit in 0 degree direction.

델타스폿용접을 이용한 이종소재 웰드본딩공정 시 표면 거칠기 부여 가공방법의 영향 (Effect of Surface Roughness on Weld-bonding Process using Heterogeneous Materials)

  • 김영현;김재웅;김지선;김영곤;표창민
    • 한국기계가공학회지
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    • 제19권11호
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    • pp.102-108
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    • 2020
  • The demand for lightweight materials and high-strength steel has rapidly increased to help reduce the weight of a vehicle body; it improves the fuel efficiency of automobiles and provides passenger safety. Additionally, as the material becomes thinner, the demand for its resistance against corrosion becomes higher. Hence, the application of the surface-treated steel sheet has surged rapidly. In this study, a weld bonding experiment using a delta spot welding machine is performed on a thin sheet of a different material (Al6061-T6/GA440). The thickness of the material was kept at 1 mm to reduce the weight of the automobile body parts. Additionally, the purpose of this study is to control the heat input by applying the welding conditions of a multi-stage pressure pattern to improve corrosion resistance shear strength. The analysis of nugget diameter measurement, shear tensile test, and salt spray test was performed to achieve the aim.

거제 내만해역에서의 고주파 양상태 해수면 음파산란 채널 측정 및 모의 (Measurement and simulation of high-frequency bistatic sea surface scattering channel in shallow water of Geoje bay)

  • 최강훈;김용빈;김시문;최지웅
    • 한국음향학회지
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    • 제40권1호
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    • pp.1-9
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    • 2021
  • 해수면 상태에 따른 고주파 양상태 해수면 음파산란 채널 측정 실험은 2020년 4월 거제 내만해역에서 수행되었으며 산란이론을 기반으로 한 모의결과와 비교하였다. 신호는 중심주파수 128 kHz, 대역폭 32 kHz의 선형 주파수 변조 신호를 이용하였다. 파고부이를 통해 측정된 해수면 거칠기로부터 해수면 파수 스펙트럼을 계산하였고 산란이론인 Small Slope Approximation(SSA)에 적용하여 해수면 거칠기에 의한 산란강도를 추정하였다. 또한 실험 당시 풍속을 이용하여 해수면 부근 공기방울층 음파산란을 고려하여 산란강도를 계산하였다. 모의된 산란강도를 이용하여 해수면 산란 채널 세기 임펄스 응답을 모의하였고, 해수면 파수 스펙트럼과 공기방울층 산란에 따른 모의결과를 측정치와 비교, 분석하였다.

공구마모보정을 위한 전기접점식 자동공구 보정시스템 개발 (A Study on Measurement for Endmill Dia. using Electric Contact Method)

  • 정상화;신형성;나윤철
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2001년도 춘계학술대회 논문집
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    • pp.445-449
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    • 2001
  • The tool wear that is developed by long-term machining in mold manufacturing with machining center makes a severe influence to the accuracy and the surface roughness. In this reason, tool-wear supervising system which has guaranteed high accuracy and high speed is needed to improve the measurement quality. Touching probe and touch sensor are widely used to measure the tool profile at on-machine measurement. In this paper, using the newly developed electric touch point measuring system, the Automatic Tool Compensation System is developed to correct the error of tool diameter resulted from the wear, and the operating method of this system is also provided.

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High-Frequency Bistatic Scattering from a Corrugated Sediment Surface

  • Cho, Hong-Sang;La, Hyoung-Sul;Yoon, Kwan-Seob;Na, Jung-Yul;Kim, Bong-Chae
    • The Journal of the Acoustical Society of Korea
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    • 제25권2E호
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    • pp.60-68
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    • 2006
  • High-frequency bistatic scattering measurements from a corrugated surface were made in an acoustic water tank. First the azimuthal scattering pattern was measured from an artificially corrugated surface which has varying impedance. The corrugated surface was installed both transverse to the direction of incident wave and longitudinal to the direction of incident wave. The angle between the corrugated surface and the direction of the incident wave was about $45^{\circ}$. Second, the scattering strengths were measured from the flat sediment and the corrugated sediment. A critical angle of about $37^{\circ}$ was calculated in the acoustic water tank. The measurements were made at three fixed grazing angles: $33^{\circ}$ (lower than critical angle), $37^{\circ}$ (critical angle), and $41^{\circ}$ (higher than critical angle). The scattering angle and the grazing angle are equal in each measurement. Frequencies were from 50 kHz to 100 kHz with an increment of 1 kHz. The corrugated sediment was made transverse to the direction of the incident wave. The first measurement indicates that the scattering patterns depend on the relations between the corrugated surface and the direction of the incident wave. In the second measurement, the data measured from the flat sediment were compared to the APL-UW model and to the NRL model. The NRL model's output shows more favorable comparisons than the APL-UW model. In case of the corrugated sediment, the model and the measured data are different because the models used an isotropic wave spectrum of sediment roughness in the scattering calculations. The isotropic wave spectrum consists of $w_2$ and ${\gamma}_2$. These constants derived from sediment names or bulk size. The model which used the constants didn't consider the effect of a corrugated surface. In order to consider a corrugated surface, the constants were varied in the APL-UW model.

저온 플라즈마 처리를 이용한 파라 아라미드 섬유의 표면 개질 효과 및 역학적 특성(2) (Surface Modification Effect and Mechanical Property of para-aramid Fiber by Low-temperature Plasma Treatment)

  • 박성민;손현식;심지현;김주용;김태경;배진석
    • 한국염색가공학회지
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    • 제27권1호
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    • pp.18-26
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    • 2015
  • para-aramid fibers were treated by atmosphere air plasma to improve the interfacial adhesion. The wettability of plasma-treated aramid fiber was observed by means of dynamic contact angle surface free energy measurement. Surface roughness were investigated with the help of scanning electron microscopy and atomic force microscopy. The tensile test of aramid fiber roving was carried out to determine the effect of plasma surface treatments on the mechanical properties of the fibers. A pull-out force test was carried out to observe the interfacial adhesion effect with matrix material. It was found that surface modification and a chemical component ratio of the aramid fibers improved wettability and adhesion characterization. After oxygen plasma, it was indicated that modified the surface roughness of aramid fiber increased mechanical interlocking between the fiber surface and vinylester resin. Consequently the oxygen plasma treatment is able to improve fiber-matrix adhesion through excited functional group and etching effect on fiber surface.