• 한국재료학회지
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• 제19권11호
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• pp.601-606
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• 2009

$BiFeO_3$ (BFO) thin films were prepared on $Pt/TiO_2/Si$ substrate by r.f. magnetron sputtering. The effects of deposition pressure on electrical properties were investigated using measurement of dielectric properties, leakage current and polarization. When BFO targets were prepared, Fe atoms were substituted with Mn 0.05% to increase electrical resistivity of films. (Fe+Mn)/Bi ratio of BFO thin films increases with increasing partial pressure of $O_2$ gas. The deposited films showed the only BFO phase at 10 mTorr, the coexistence of BFO and $Bi_2O_3$ phase at 30-50 mTorr, and the only $Bi_2O_3$ phase at 70 mTorr. The crystallinity of BFO films was reduced due to the higher Bi contents and the decrease of surface mobility of atoms at high temperature. The porosity and surface roughness of films increased with the increase of the deposition pressure. The films deposited at high pressure showed low dielectric constant and high leakage current. The dielectric constant of films deposited at various deposition pressures was 84${\sim}$153 at 1 kHz. The leakage current density of the films deposited at 10${\sim}$70 mTorr was about $7{\times}10.6{\sim}1.5{\times}10.2A/cm^2$ at 100 kV/cm. The leakage current was found to be closely related to the morphology and composition of the BFO films. BFO films showed poor P-E hysteresis loops due to high leakage current.

• Advances in aircraft and spacecraft science
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• 제6권3호
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• pp.239-256
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• 2019

This study develops a dual purpose: i) evaluating the effects of two different Mars atmosphere models (NASA Glenn and GRAM-2001) on aerodynamics of a capsule (Pathfinder) entering the Mars atmosphere, ii) verifying the feasibility of evaluating the ambient density and pressure by means of the methods by McLaughlin and Cassanto, respectively and therefore to re-build the values provided by the models. The method by McLaughlin relies on the evaluation of the capsule drag coefficient, the method by Cassanto relies on the measurement of pressure at a point on the capsule surface in aerodynamic shadow. The study has been carried out computationally by means of: i) a code integrating the equations of dynamics of the capsule for the computation of the entry trajectory, ii) a DSMC code for the solution of the flow field around the capsule in the altitude interval 50-100 km. The models show consistent differences at altitudes higher than about 40 km. It seems that the GRAM-2001 model is more reliable than the NASA Glenn model. In fact, the NASA Glenn model produces, at high altitude, temperatures that seem to be too low compared with those from the GRAM-2001 model and correspondingly very different aerodynamic conditions in terms of Mach, Reynolds and Knudsen numbers. This produces pretty different capsule drag coefficients by the two models as well as pressure on its surface, making not feasible neither the method by McLaughlin nor that by Cassanto, until a single, reliable model of the Mars atmosphere is not established. The present study verified that the implementation of the Cassanto method in Mars atmosphere should rely (such as it is currently) on pressure obtained experimentally in ground facilities.

• 한국응용과학기술학회지
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• 제32권3호
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• pp.522-527
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• 2015

변위전류 측정법을 L-${\alpha}$-dilauryl phosphatidylcholine(DLPC) 단분자 막의 연구에 적용하였다. 변위전류는 물 표면에서 DLPC 단분자 층에서 압축과 확장에 의해 발생되었다. 맥스웰 변위전류(MDC) 발생은 분자 당 점유면적 $200{\AA}^2$ 에서 $40{\AA}^2$에 대하여 관찰하였다. 맥스웰 변위전류는 단분자 층의 압축 사이클에 대해 조사하였으며, MDC의 최대 값은 압축 사이클의 표면 압력이 처음 상승하기 바로 직전의 분자당 점유면적에서 나타나는 것을 알 수 있었다. LB막의 단분자층 표면 형태는 원자힘 현미경(AFM)으로 측정하였다. 결과적으로, AFM 이미지에 나타난 LB막의 특성은 단분자 층의 배향이 좋았으며 단분자 층의 두께는 약 5~10 nm였다.

• 한국해양공학회지
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• 제13권3호통권33호
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• pp.92-99
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• 1999

High temperature and pressure materials in power plant are degraded by creep damage, if they are exposed to constant loads for long times, which occurs in load bearing structures of pressurized components operationg at elevated temperatures. Many conventional measurement techniques such as replica method, electric resistance method, and hardness test method for measuring creep damgage have been used. So far, the replica method is mainly used for the inspection of high temperature and pressure components. This technique is, however, restricted to applications at the surface of the testpieces and cannot be used to material inside. In this paper, ultrasonic evaluation for the detection of creep damage in the form of cavaties on grain boundaries or intergranular microcracks were carried out. And the absolute measuring method of quantitative ultrasonic velocity technique for Cr-Mo material degradation was analyzed. As a result of ultrasonic tests for crept for specimens, we founded that the sound velocity was decreased as increase of creep life fraction(${phi}c$) and also, confirmed that hardness was decreased as increase of creep life fraction(${phi}c$).

• 한국항공우주학회지
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• 제50권11호
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• pp.747-754
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• 2022

유체진동기에서 분출되는 초음속 진동제트를 이용하여 충격파에 의한 경계층 박리유동을 제어하는 실험적 연구가 이루어졌다. 유체진동기의 위치와 제어압력의 변화가 경사충격파에 의하여 발생되는 경계층 박리유동의 특성에 미치는 영향이 관찰되었고, 이를 위하여 고속 슐리렌, 표면유동가시화, 벽압력 측정, 그리고 정밀 피토관 측정 기법이 적용되었다. 본 연구의 초음속 진동제트의 박리유동 제어 특성은 공기제트 와류를 이용한 기존 제어기법과 정량적으로 비교 분석되었다.

• 소성∙가공
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• 제13권1호
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• pp.9-14
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• 2004

Recently, various bulk metallic glasses (BMG's) having good mechanical and chemical properties were developed. BMG's can easily be deformed in the supercooled liquid region, via viscous flow mechanism. By using the viscous flow, the very low pressure is needed to deform the materials. In this study, we investigated the structural transition and deformation behavior of Vitreloy 1 (Zr/sub 41.2/Ti/sub 13.8/Cu/sub 12.5/Ni/sub 10/Be/sub 22.5/) using TMA and DSC. We applied the results to the micro forming process. The forming condition was chosen based on the viscosity data from TMA, and Si wafer with micro patterns on the surface was used as a forming die. The deformed surface was analyzed by SEM and 3D Surface Profiling System. The alloy showed good replication of the patterns. Quantitative measurement of roughness was useful to evaluate the replication. Surface condition of the deformed surface was determined by the initial surface condition.

• 한국터널지하공간학회 논문집
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• 제9권1호
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• pp.49-62
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• 2007

본 연구에서는 사질토 지반에 설치된 수직갱에 작용하는 토압에 대한 기존 제안식을 수정하였다. 이를 검증하기 위하여 깊이에 관계없이 동일한 반경방향 변위를 일으킬 수 있는 실내 모형시험장치를 개발하였으며, 벽면마찰각과 상대 밀도를 변수로 시험하였다. 실내 모형시험 결과는 수정식에서 접선방향 토압계수(수직응력에 대한 접선방향 응력 비)인 $\lambda$값을 $\lambda=1-sin\phi$와$\lambda=1$을 사용하였을 경우의 토압 사이에 분포하였다. 다층지반에 설치된 원형수직갱 배면지반의 파괴면을 가정하고 수정식을 적용하여 다층지반에 설치된 원형수직갱에 작용하는 토압 산정방법을 제안하였다. 시공현장의 3개의 수직갱으로부터 계측 데이터를 획득하였으며 이를 토압으로 환산하여 제안된 방법을 검증하였다. 계측 데이터로부터 환산된 대부분의 환산 토압은 제안된 방법의 토압과 잘 일치하였다.

• 대한의용생체공학회:의공학회지
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• 제35권6호
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• pp.203-210
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• 2014

Wearable medical device has been a resurgence of interest thanks to the development of technology and propagation of smart phone in recent years. Various types of wearable devices have been introduced and available in market. Capacitive coupled electrode which measures electrocardiogram over cloth is able to be applied wearable device. In previous approaches of capacitive electrode, they need proper pressure for stable contact of the electrode to body surface. However, wearable device that gives pressure on body surface is not suitable for long-term monitoring. In this study, we proposed adhesive polyurethane-based capacitive electrode for patch-type wearable electrocardiogram (ECG) monitoring device. Self-adhesive polyurethane make the electrode and whole system be adhered to the surface of skin without any pressure. The patch-type system is consisted of analog filter, analog-to-digital converter and wireless transmission module and designed to be attached on the body as a patch. To validate the feasibility of the developed system, we measured ECG signal in stable and active state and extracted heart rate. Therefore, we observed skin response after long-term attachment for biocompatibility of the adhesive polyurethane and adhesive strength of it. The result shows the possibility of applying the developed system for ECG monitoring in real-life.

• Membrane and Water Treatment
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• 제10권4호
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• pp.287-298
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• 2019

Lotus leaf has a special dual micro and nano surface structure which gives its highly hydrophobic surface characteristics and so-called self cleaning effect. In order to endow PVDF hollow fiber membrane with this special structure and improve the hydrophobicity of membrane surface, PVDF hollow fiber composite membranes was obtained through the immersion coating of poly(vinylidene fluoride-co-hexafluoropropylene) (PVDF-HFP) dilute solution on the outside surface of PVDF support membrane. The prepared PVDF composite membranes were used in the vacuum membrane distillation (VMD) for the desalination. The effects of PVDF-HFP dilute solution concentration in the dope solution and coating time on VMD separation performance was studied. Membranes were characterized by SEM, WCA measurement, porosity, and liquid entry pressure of water. VMD test was carried out using $35g{\cdot}L^{-1}$ NaCl aqueous solution as the feed solution at feed temperature of $30^{\circ}C$ and the permeate pressure of 31.3 kPa. The vapour flux reached a maximum when PVDF-HFP concentration in the dilute solution was 5 wt% and the coating time was kept in the range of 10-60 s. This was attributed to the well configuration of micro-nano rods which was similar with the dual micro-nano structure on the lotus leaf. Compared with the original PVDF membrane, the salt rejection can be well maintained which was greater than 99.99 % meanwhile permeation water conductivity was kept at a low value of $7-9{\mu}S{\cdot}cm^{-1}$ during the continuous testing for 360 h.

• 공업화학
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• 제34권1호
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• pp.9-14
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• 2023

본 논문에서는 용액의 이온 농도 측정이 가능한 나피온 폴리머(Nafion polymer) 코팅 기반 2상 금 전극의 임피던스(Impedance) 센서를 개발하였다. 스퍼터링(Sputtering) 공정을 통해서 제작된 금 전극의 표면을 나피온 폴리머를 사용하여 표면 개질 하였다. 상기 제작된 전극은 분극 현상 제어가 가능하여 전기화학적 신호를 안정적으로 측정할 수 있도록 하였다. 분광학과 전자주사현미경 관찰을 통하여 박막의 나피온 폴리머 코팅을 확인하였다. 나피온 코팅이 된 전극은 기존 금 전극에 비해 안정적인 임피던스 신호를 보여 주었으며, 표준 염화나트륨(NaCl) 용액 사용 시 임피던스 센서의 신뢰성 높은 검정 곡선(R² = 0.983)을 나타내었다. 또한, 임피던스 센서는 상용화 전도도 장치와 인공 눈물의 이온 농도 측정 비교 실험을 진행하였으며, 유사한 결과값을 확인하였다.