• Journal of Powder Materials
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• v.19 no.1
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• pp.13-18
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• 2012

This study has been performed on the full density sintering of Fe nanopowder and the surface hardening by plasma ion nitriding. The Fe sintered part was fabricated by pressureless sintering of the Fe nanopowder at $700^{\circ}C$ in which the nanopowder agglomerates were controlled to have 0.5-5 ${\mu}m$ sized agglomerates with 150 nm Fe nanopowders. The green compact with 46% theoretical density(T.D.) showed a homogeneous microstructure with fine pores below 1 ${\mu}m$. After sintering, the powder compact underwent full densification process with above 98%T.D. and uniform nanoscale microstructure. This enhanced sintering is thought to be basically due to the homogeneous microstructure in the green compact in which the large pores are removed by wet-milling. Plasma ion nitriding of the sintered part resulted in the formation of ${\gamma}$'-$Fe_4N$ equilibrium phase with about 12 ${\mu}m$ thickness, leading to the surface hardening of the sintered Fe part. The surface hardness was remarkably increased from 176 $H_v$ for the matrix to 365 $H_v$.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2012.10a
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• pp.127-128
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• 2012

• Journal of the Korean Geotechnical Society
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• v.18 no.4
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• pp.33-43
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• 2002

Recently, as large constructions on the coast increase, an application of a surface layer stabilization method which is one of the improvement methods for dredged soft clay has increased. However, there are few studies about this. The purpose of this study is clarifying characteristics of ultra-soft marine clay and hardening agent. Also, it is verifying an optimal mixture ratio of hardening agent through the laboratory tests according to designed experiments and proving by statistical analysis and pilot tests. Laboratory tests were performed with proper hardening agent and test soil in accordance with the design of experiments. Regression equations between hardening agents materials and unconfined compressive strength were derived from the tests. The applicability of regression equations were also verified by pilot tests. From the test results, it was found that hardening agent materials(cement, slag, fly-ash, inorganic salts, arwin, gypsum etc.) have some effect upon compressive strength. The optimal mixture ratio which satisfies the required compressive strength was derived from the statistical analysis. The effect of ground improvement by cements and hardening agents was confirmed through the pilot tests. This study will suggest data for design or construction criteria of stabilization of surface layer on ultra-soft marine clay.

• Journal of Welding and Joining
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• v.19 no.2
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• pp.228-234
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• 2001

A methodology is developed and used to evaluate the response sensitivity of the thermal systems to variations in their design parameters. Technique for computing the sensitivity of temperature distributions to changes in processing parameters needed to decide the more effective laser input parameters for laser surface hardening treatment is considered. In this study, a state equation governing the heat flow in laser surface treatment is analyzed using a three-dimensional finite element method and sensitivity data of the processing parameter obtained using a direct differentiation method is applied to the sensitivity analysis. The interesting processing parameters are taken as the laser scan velocity and laser beam radius ( $r_{ b}$), and the sensitivities of the temperature T versus v and $r_{b}$ are analyzed. These sensitivity results are obtained with another parameters fixed. To verify the numerical analysis results, hardened layer dimensions (width and depth) of the numerical analysis are compared with the experimental ones.nes.

• Laser Solutions
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• v.2 no.2
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• pp.42-51
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• 1999

This study has been performed to investigate into some effects of the output power and traverse speed of laser beam on the microstructures, hardness and fatigue resistance of the ductile iron surface-hardened by $CO_2$ laser defocussed beam. Optical micrographs have shown that with increasing the output power and decreasing the traverse speed, the martensite was coarsened and some retained austenite were appeared in ductile iron. The microstructures of hardening zone were composed of bull's eye and some nodular graphite dissolved structures by the effect of self quenching. Fatigue fracture characteristics of ductile iron have appeared in the high stress and low stress ranges. The fracture initiated at nodular graphites in the surface hardened layer due to the stress concentration caused by a notch effect. The interior graphite nodules were broken away or popped out during crack propagation. Fatigue test has shown that values of fatigue strength considerably increased with increasing output power at a given traverse speed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.78-83
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• 2009

In general, Light-hardening polymer was used UV nanoimprint technology. A light-hardening polymer was had the problem of poor hardness, durability. In order to overcome the problem of polymer, inter change optical glass. However glass is very manufacture and a lowering of standars transmittance. In order to glass recover was necessary polishing process. The process is magnetorheological fluids polishing. MR polishing has been developed as a new precision finishing technique to obtain a fine surface. Hence, Magnetorheological fluids has been used for micro polishing to get micro parts. This polishing process guarantees high polishing quality by controlling the fluid density electrically. The applied material in experiments is fused silica glass. Fused silica glass is widely used in the optical field because of high degree of purity. For MR polishing experiments, MR fluid was composed with DI-water, carbonyl iron and nano slurry ceria. The wheel speed and electric current were chosen as the variables for analyzing the characteristics of MR polishing process. Outstanding surface roughness of Ra=1.58nm was obtained on the fused silica glass specimen. And originally glass transmittance was recover on the fused silica glass.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.10 no.1
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• pp.31-37
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• 2011

Recently, the technology of surface treatment is being more important which affects the material cost reduction and substitution to the expensive material. The material used for the mechanical processing should have not only high intensity, but also strength toughness, wear resistance and corrosion resistance. In order to increase the durability and have better quality of the parts using such kind of tooling material, various kinds of research of the surface hardening through many kinds of heat resources is being done and practically applied. In this study, the characteristics of hardening surface zone for high strength of the press die material through laser beam irradiation are researched. In this study, it is experimentally observed by the status of the surface morphology, tensile strength, the hardness distribution of the base metal and wear condition by the surface hardness pattern by the laser beam based on the process parameters of $CO_2$ laser by using SM45C and STD11 used for press tool. Through this research, the characteristics of surface hardened zone for high strength of the thin metal by laser beam irradiation is done.

• 제어로봇시스템학회:학술대회논문집
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• 1991.10a
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• pp.252-257
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• 1991

This paper proposed that the eddy-current measurement method can be used a means of in-process measuring the hardening depth in Laser surface treatment process. Also, this paper deal with the numerical analysis of magnetic flux distribution and experimental result of measurement. In Laser heat treatment process of steels, a thin layer of the substrate is rapidly heated to austenitizing temperature and subsequently cooled at a very fast rate due to the self-quenching by heat conduction into the bulk body, to produce a martensite structure which have low magnetic permeability. The eddy-current measurement method depends on the properties of material to be measured such as electric conductivity, magnetic permeability and geometry. In this paper, the hardening depth was measured by detecting relevant magnetic permeability changes caused by heat treatment of steels.

• Proceedings of the KWS Conference
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• 2006.05a
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• pp.248-250
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• 2006

The study on a surface transformation hardening of a rod-shaped SM45C carbon steel is carried out by using CW Nd:YAG laser. Conventionally, $CO_2$ laser has been usually used as a laser source for a transformation hardening. however, it is needed to an additional absorbent coating like a colloidal graphite owing to a lower absorbtion rate. On the other hand, no cost and post-removal process of coating is required to Nd:YAG laser, due to a higher absorbtion rate relatively. Moreover, there is a merit which is capable of building up the more flexible processing system resulted from a beam delivery through a optical fiber. In this study, we were going to recognize characteristics of a transformation hardening using a optic head with a gaussian beam distribution.

• Proceedings of the KSR Conference
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• 2001.05a
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• pp.408-415
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• 2001

Hardening agent has been the traditional material for surface soil stabilization of soft ground. The aim of this study if to determine optimal mixture ratio of hardening agent in accordance with the required design specifications. Hardening agent consists of fly ash, gypsum, slag and cement for the ettringite hydrates and if effective for early stabilization of unconsolidated soil. The raw ground material is the clay that is widely found here and there in Korea. In this study, preliminary tests were performed to get optimal mixture ratio of stabilizer ingredient and marine clay in Jinhae was used to get physical and chemical properties. Laboratory tests of 50 stabilized soils were performed to get optimal mixture ratio for 16-stabilizer materials of 6 types, and mixture ratio of stabilizer ingredient and marine clay was determined.