• Title/Summary/Keyword: surface hardening

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Surface Modification for Improving Adhesion between Etching Resist and Copper Substrate (Etching resist와 Copper substrate 간의 Adhesion 향상을 위한 표면개질)

  • Park, Sung-Jun;Seo, Shang-Hoon;Kim, Yong-Sik;Kim, Tae-Gu;Lee, Sang-Gyun;Joung, Jae-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.129-129
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    • 2006
  • 인쇄회로를 제작하기 위하여 기판상에 에칭 레지스트, 도금막, 절연재료, 솔더 마스크 등을 패터닝 하게 되는데, 일반적으로 이러한 유기체 막들은 대부분 액상이나 고형의 필름 형태로 패턴을 형성하게 된다. 형성된 패턴과 동박과의 접착력 향상이 가장 주요한 문제점 중의 하나이다. 상대적으로 편평한 동박면과 유기체 막과의 접착력을 향상시키기 위해 일반적으로 접촉 면적을 증가시키기 위한 표면개질을 하게 된다. 기계적 브러싱이나 스크러빙에 의해서도 기판상의 동박의 surface topography 를 개선하기 위한 노력이 시도 되고 있지만, 본 연구에서는 microetching 방법에 의해서 화학적으로 동박 표면상에 최대한 요철을 많이 형성하여 에칭 레지스트와 동박 간의 접착력을 증대시키기 위한 연구를 수행하였다.

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Mechanical behavior and chloride resistance of cementitious composites with PE and steel fiber

  • Liao, Qiao;Guo, Zhen-wen;Duan, Xin-zhi;Yu, Jiang-tao;Liu, Ke-ke;Dong, Fang-yuan
    • Advances in concrete construction
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    • v.12 no.6
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    • pp.451-459
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    • 2021
  • The mechanical behaviors and chloride resistance performance of fiber reinforced cementitious composites (FRCC) with hybrid polyethylene (PE) and steel fiber (in total 2% by volume) were investigated. Based on micro-mechanics and fracture mechanics, the reason why the tensile strain capacity of FRCC changed obviously was obtained. Besides, the effects of the total surface area of fiber in FRCC on compressive strength and chloride content were clarified. It is found that the improvement of the tensile strain capacity of FRCC with hybrid fiber is attributed to the growth of strain-hardening performance index (the ratio of complementary energy to crack tip toughness). As the total surface area of fiber related with the interfacial transition zone (ITZ) between fiber and matrix increases, compressive strength decreases obviously. Since the total surface area of fiber is small, the chloride resistance performance of FRCC with hybrid PE and steel fiber is better than that of FRCC containing only PE fiber.

Characterization of Residual Stress in Shot Peened Al 7075 Alloy Using Surface Acoustic Wave (표면파를 이용한 쇼트피닝된 Al 7075 합금의 잔류응력 평가)

  • Kim, Chung-Seok;Kim, Yong-Kwon;Park, Ik-Keun;Kwun, Sook-In
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.5
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    • pp.291-296
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    • 2006
  • The residual stress in shot-peened Al 7075 alloy was evaluated using surface acoustic wave (SAW). Shot peening was conducted to produce a variation in the residual stress with the depth below the surface under a shot velocity of 30 m/s. The SAW velocity was measured from the V(z) curve using a scanning acoustic microscopy (SAM). The Vickers hardness profile from the surface showed a significant work hardening near the surface layer with a thickness of about 0.25 mm. As the residual stress became more compressive, the SAW velocity increased, whereas as the residual stress became more tensile, the SAW velocity decreased. The variation in the SAW velocity through the shot peened surface layer was in good agreement with the distribution of the residual stress measured by X-ray diffraction technique.

Rolling Contact Fatigue and Residual Stress Properties of SAE52100 Steel by Ultrasonic Nano-Crystalline Surface Modification (UNSM) (초음파 나노표면 개질처리를 통한 베어링강의 회전접촉피로 및 잔류응력 특성에 대한 연구)

  • Lee, Changsoon;Park, Ingyu;Cho, Insik;Hong, Junghwa;Jhee, Taegu;Pyoun, Youngsik
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.1
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    • pp.10-19
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    • 2008
  • To investigate the effect of ultrasonic nano-crystalline surface modification (UNSM) treatment on rolling contact fatigue and residual stress properties of bearing steels, this paper carried out a rolling contact fatigue test, measured residual stress and retained austenite, performed a wear test, observed microstructure, measured micro hardness, and analyzed surface topology. After the UNSM treatment, it was found that the surface became minute by over $100{\mu}m$. The micro surface hardness was changed from Hv730~740 of base material to Hv850~880 with about 20% improvement, and hardening depth was about 1.3 mm. The compressive residual stress was measured as high as -700~-900 MPa, and the quantity of retained austenite was reduced to 27% from 34%. The polymet RCF-6 ball type rolling contact fatigue test showed over 4 times longer fatigue lifetime after the UNSM treatment under 551 kgf load and 8,000 rpm. In addition, this paper observed the samples, which went through the rolling contact fatigue test, with OM and SEM, and it was found that the samples had a spalling phenomenon (the race way is decentralized) after the UNSM treatment. However, before the treatment, the samples had excessive spalling and complete exploration. Comparison of the test samples before and after the UNSM treatment showed a big difference in the fatigue lifetime, which seems to result from the complicated effects of micro particles, compressive residual stress, retained austenite, and surface topology.

Surface Roughness and Formation of Compound Layer in the Controlled Gaseous Nitriding Process on Cast Iron GC250D (GC250D의 가스분위기 제어질화 공정에서 화합물층의 형성에 따른 표면조도의 변화)

  • Minjae Jeong;Seokwon Son;Jae-Lyoung Wi;Yong-Kook Lee;Won-Beom Lee
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.2
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    • pp.49-57
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    • 2024
  • We investigated the changes in microstructure and surface roughness of the compound layer of GC250D gray cast iron, commonly used in brake discs, during gas nitriding. The gas atmosphere of the nitriding process was controlled with a hydrogen partial pressure of 49.5%, and the process was conducted at a nitriding temperature of 520℃ with various process times. As the nitriding process time of the GC250D material increased, both the depth of hardening and the thickness of the compound layer increased, with a maximum surface hardness of approximately 1265 HV0.1 was measured. Additionally, the surface roughness increased with the process time. Phase analysis of the compound layer revealed an increase in the proportion of the γ' phase as the nitriding process time increased. Changes in the formation of the compound layer were observed depending on the orientation of graphite within the material, leading to the formation of wedges. Therefore, the increase in surface roughness appears to be attributed to the uneven compounds, the expansion of the compound layer and wedges formed on the surface during the nitriding process.

Electro-deposition and Crystallization Behaviors of Cr-C and Cr-C-P Alloy Deposits Prepared by Trivalent Chromium Sulfate Bath (황화물계 3가 크롬도금욕에서 크롬-탄소 및 크롬-탄소-인 합금도금의 전착과 결정화거동)

  • Kim, Man;Kim, Dae-Young;Park, Sang-Eon;Kwon, Sik-Chul;Choi, Yong
    • Journal of the Korean institute of surface engineering
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    • v.37 no.2
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    • pp.80-85
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    • 2004
  • Chromium-carbon (Cr-C) and chromium-carbon-phosphorus (Cr-C-P) alloy deposits using trivalent chromium sulfate baths containing potassium formate were prepared to study their current efficiency, hardness change and phase transformations behavior with heat treatment, respectively. The current efficiencies of Cr-C and Cr-C-P alloy deposits increase with increasing current density in the range of 15-35 A/dm$^2$. Carbon content of Cr-C and phosphorous of Cr-C-P layers decreases with increasing current density, whereas, the carbon content of Cr-C-P layer is almost constant with the current density. Cr-C deposit shows crystallization at $400^{\circ}C$ and has (Cr+Cr$_{ 23}$$C_{6}$) phases at $800^{\circ}C$. Cr-C-P deposit shows crystallization at $600^{\circ}C$ and has (Cr+Cr$_{23}$ $C_{6}$$+Cr_3$P) phases at $800^{\circ}C$. The hardness of Cr-C and Cr-C-P deposits after heating treatment for one hour increase up to Hv 1640 and Hv 1540 and decrease about Hv 820 and Hv 1270 with increasing annealing temperature in the range of $400~^{\circ}C$, respectively. The hardness change with annealing is due to the order of occurring of chromium crystallization, precipitation hardening effect, softening and grain growth with temperature. Less decrease of hardness of Cr-C-P deposit after annealing above $700^{\circ}C$ is related to continuous precipitation of $Cr_{23}$ $C_{6}$ and $Cr_3$P phases which retard grain growth at the temperature.

Microstructure and Tensile Properties of 700 MPa-Grade High-Strength and Seismic Resistant Reinforced Steel Bars (700 MPa급 고강도 및 내진 철근의 미세조직과 인장 특성)

  • Hong, Tae-Woon;Lee, Sang-In;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.28 no.7
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    • pp.391-397
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    • 2018
  • This study deals with the microstructure and tensile properties of 700 MPa-grade high-strength and seismic reinforced steel bars. The high-strength reinforced steel bars (600 D13, 600 D16 and 700 D13 specimens) are fabricated by a TempCore process, while the seismic reinforced steel bar (600S D16 specimen) is fabricated by air cooling after hot rolling. For specimens fabricated by the TempCore process, the 600 D13 and 600 D16 specimens have a microstructure of tempered martensite in the surface region and ferrite-pearlite in the center region, while the 700 D13 specimen has a microstructure of tempered martensite in the surface region and bainite in the center region. Therefore, their hardness is the highest in the surface region and shows a tendency to decrease from the surface region to the center region because tempered martensite has a higher hardness than ferrite-pearlite or bainite. However, the hardness of the 600S D16 specimen, which is composed of fully ferrite-pearlite, increases from the surface region to the center region because the pearlite volume fraction increases from the surface region to the center region. On the other hand, the tensile test results indicate that only the 700 D13 specimen with a higher carbon content exhibits continuous yielding behavior due to the formation of bainite in the center region. The 600S D16 specimen has the highest tensile-to-yield ratio because the presence of ferrite-pearlite and precipitates caused by vanadium addition largely enhances work hardening.

Microstructure and Properties of Ni-SiC Composite Coating Layers Formed using Nano-sized SiC Particles (SiC 나노입자를 이용하여 형성한 Ni-SiC 복합도금막의 미세구조 및 특성)

  • Lee, Hong-Kee;Son, Seong-Ho;Lee, Ho-Young;Jeon, Jun-Mi
    • Journal of the Korean institute of surface engineering
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    • v.40 no.2
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    • pp.63-69
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    • 2007
  • Ni-SiC composite coating layers were formed using two kinds of SiC nano-particles by DC electrodeposition in a nickel sulfamate bath containing SiC particles. The effect of stirring rate and SiC particle type on the microstructure and properties of Ni-SiC composite coating layers were investigated. Results revealed that the trend of deposition rate is closely related to the codeposition of SiC and the deposition rate. or nickel, and the codeposition behavior of SiC can be explained by using hydrodynamic effect due to stirring. The average roughness and friction coefficient are closely related to the codeposition of SiC and SiC particle size. It was found that the Victors microhardness of the composite coating layers increased with increasing codeposition of SiC. The composite coating layers containing smaller SiC particle showed higher hardness. This can be explained by using the strengthening mechanism resulting from dispersion hardening. Anti-wear property of the composite coating layers formed using 130 nm-sized SiC nano-particles has been improved by 2,300% compared with pure electroplated-nickel layer.

A Study on the Optimum Mix and Exposing Method of the Fine-Size Exposed Aggregate PCC Pavements (소입경 골재노출콘크리트포장의 최적 배합 및 노출기법에 관한 연구)

  • Kim, Young-Kyu;Lee, Seung-Woo;Yoo, Tae-Seok;Kim, Hyung-Bae
    • International Journal of Highway Engineering
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    • v.11 no.2
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    • pp.1-15
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    • 2009
  • Surface of exposed aggregate concrete pavements is consists of exposed coarse aggregate by removing upper 2$\sim$3mm mortar of concrete slab. Exposed aggregate concrete pavements have advantages of maintaining low-noise and adequate skid-resistance level during the performance period. In order to provide the successful exposed concrete aggregate pavement, uniform distribution of the coarse aggregate on pavement surface through adequate the mix design and exposing method. The mix design in concrete pavement is generally designed on the basis of strength, but mix design of exposed aggregate pavement employed in this study includes the consideration of noise and skid resistance, as well as strength. Smaller of maximum coarse aggregate is known to be effective for reduce noise level. Optimum mix design and exposing method of fine-size exposed aggregate portland cement concrete pavement that can reducing the noise and maintain the adequate level of skid resistance are proposed in this study. To consider the variation of optimum exposing time due to the hardening speed of mortar by climatic condition, quantitative is also suggested measurement of hardening state.

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Compression Strength Behavior of Mixed Soil Recycling Bottom Ash for Surface Layer Hardening (매립석탄회를 재활용한 표층연약지반 개량용 혼합토의 압축강도 특성 연구)

  • Oh, Gi-dae;Kim, Kyoung Yul
    • KEPCO Journal on Electric Power and Energy
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    • v.5 no.4
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    • pp.287-293
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    • 2019
  • Domestic thermal power plant fly ash is at a situation which emissions are increasing every year. Comparing to Fly Ash, Bottom Ash is only 15 %, but it's recycling rate is low, so most of them is being buried in the ground. However, landfill site of every power plant is full, and the construction of a new landfill is difficult. To solve this problem, the best solution is to use Bottom Ash as a landfill of large-scale civil engineering projects. The purpose of this study was to investigate the compression strength behavior characteristics of weak clay and uniaxial compression test to examine the applicability of surface soil solidification method of mixed soils mixed with industrial waste coal ash and weak clay which is buried in bulk. As a result of the test, the fluidity of the Mixed soil with clay + bottom ash + cement was improved to 200 mm at the water content of 91-92 %. The uniaxial compressive strength was also good for the mixed soils (clay + bottom ash + cement) meeting the required strength of 159 kN/㎡ at 28 days. However, the other samples did not meet the required strength. In this study, the prediction equations for the compression strength behavior by cement and curing period were presented.