• 한국정밀공학회지
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• 제23권10호
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• pp.68-73
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• 2006

In this study, the graphite/epoxy prepregs were surface-treated using oxygen plasma, and optimal treatment time was determined measuring the contact angle on the prepreg surface. Interlaminar fracture behavior of surface-treated graphite/epoxy composites was compared with that of regular (untreated) graphite/epoxy composites. The results showed that the contact angle was a minimum when treated for 30 minutes. The interlaminar fracture toughness of surface-treated specimen was improved about 15% compared with that of regular specimen.

• 한국산업융합학회 논문집
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• 제24권4_2호
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• pp.435-441
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• 2021

This research was performed to study the effect of the Ni + Mo addition on the fatigue properties in 12Cr steel. After heat treatment of 12Cr steel and 12Cr-Ni-Mo steel, tensile tests, impact tests, hardness tests, and rotary bending fatigue tests were performed, respectively. The fatigue fracture surface was observed and analyzed using SEM and EDS. The fatigue limit of 12Cr steel was 554 MPa, which was 49 MPa higher than 505 MPa of 12Cr-Ni-Mo steel. Striations, which are the shape of the typical fatigue fracture surface, were observed at the fracture surface near the starting point of fatigue fracture in the 12Cr steel and 12Cr-Ni-Mo steel. However, unlike the case of 12Cr steel, 12Cr-Ni-Mo steel also had a mixed fracture surface with the fatigue and the ductile fracture surface. When brittle non-metallic inclusions exist near the starting point of fatigue failure, the crack propagation was further promoted and the fatigue life was drastically reduced.

• 대한치과기공학회지
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• 제41권4호
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• pp.279-285
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• 2019

Purpose: The dental CAD / CAM system has been popular with the development of the digital dental industry. Zirconia is a typical material in dental CAD / CAM systems. Zirconia crowns are classified into single layer and double layer. This study is about the double layer crown of zirconia. The surface roughness, bond strength and fracture patterns of the zirconia surface were observed. Methods: Zirconia blocks were cut using a low speed cutter. Sintered to form a plate shape (6mm × 6mm × 3mm). The prepared specimens were surface treated in four ways. Surface roughness and bond strength were measured. And the fracture pattern was observed. Results: Result of surface treatment of zirconia. The surface roughness test results were as ET 2.87 ㎛, ST 2.67 ㎛, LT 2.44 ㎛, AT 2.41 ㎛, CN 2.08 ㎛ order. Bond Strength results were as LT 25.09 MPa, AT 23.27 MPa, ST 21.27 MPa, ET 21.09 MPa, CN 16.12 MPa order. Fracture patterns showed cohesive failure of 25-50% of the bond area. Conclusion: Surface roughness, bond strength and fracture pattern of the zirconia surface were observed. Etching the surface treatment of zirconia materials has been shown to affect the surface roughness. Zirconia special binder treatment has been shown to affect the bond strength improvement.

• The Journal of Advanced Prosthodontics
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• 제14권3호
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• pp.173-181
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• 2022

PURPOSE. This analysis aimed to evaluate the intaglio surface trueness, antagonist's wear volume loss, and fracture resistance of full-contour crowns of (Y, Nb)-stabilized fully-sintered zirconia (FSZ), 4 mol% or 5 mol% yttria-stabilized partially sintered zirconia (4YZ or 5YZ) with high-speed sintering. MATERIALS AND METHODS. A total of 42 zirconia crowns were separated into three groups: FSZ, 4YZ, and 5YZ (n = 14). The intaglio surface trueness of the crowns was evaluated at the inner surface, occlusal, margin, and axial areas and reported as root-mean-square, positive and negative average deviation. Half of the specimens were aged for 120,000 cycles in the chewing simulator, and the wear volume loss of antagonist was measured. Before and after chewing, the fracture load was measured for each group. The trueness values were analyzed with Welch's ANOVA, and the wear volume loss with the Kruskal-Wallis tests. Effect of the zirconia type and aging on fracture resistance of crowns was tested using two-way ANOVA. RESULTS. The intaglio surface trueness measured at four different areas of the crown was less than 50 ㎛, regardless of the type of zirconia. No significant P in wear volume loss of antagonists were detected among the groups (P > .05). Both the type of zirconia and aging showed statistically significant effects on fracture resistance (P < .05). CONCLUSION. The full-contour crowns of FSZ as well as 4YZ or 5YZ with high-speed sintering were clinically acceptable, in terms of intaglio surface trueness, antagonist's wear volume loss, and fracture resistance after simulated mastication.

• 한국정밀공학회지
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• 제13권3호
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• pp.94-101
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• 1996

This paper presents an investigation of the ability of the scheme to simultaneously accomplish both prediction of fracture initiation and analysis of deformation in cold forged products. The Cockcroft-Latham criterion which is successfully applied to a variety of loading situations is used in the present investigation to estimate if and where surface and internal fracture occur during the deformation process. The numerical predictions and experimental results of two types of fundamental cold metal forming process taken into account are compared. Finite element simulation combined with fracture criterion has successfully predicted the site of surface or internal fracture initiation and corresponding to level of deformation observed experimentally.

• 대한금속재료학회지
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• 제46권10호
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• pp.634-645
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• 2008

In this study, surface composites were fabricated with Fe-based amorphous alloy powders and VC powders by high-energy electron beam irradiation, and the correlation of their microstructure with hardness and fracture toughness was investigated. Mixture of Fe-based metamorphic powders and VC powders were deposited on a plain carbon steel substrate, and then electron beam was irradiated on these powders without flux to fabricate surface composites. The composite layers of 1.3~1.8 mm in thickness were homogeneously formed without defects and contained a large amount (up to 47 vol.%) of hard $Cr_2B$ and $V_8C_7$ crystalline particles precipitated in the solidification cell region and austenite matrix, respectively. The hardness of the surface composites was directly influenced by hard $Cr_2B$ and $V_8C_7$ particles, and thus was about 2 to 4 times greater than that of the steel substrate. Observation of the microfracture process and measurement of fracture toughness of the surface composites indicated that the fracture toughness increased with increasing additional volume fraction of $V_8C_7$ particles because $V_8C_7$ particles effectively played a role in blocking the crack propagation along the solidification cell region heavily populated with $Cr_2B$ particles. Particularly in the surface composite fabricated with Fe-based metamorphic powders and 30 % of VC powders, the hardness and fracture toughness were twice higher than those of the surface composite fabricated without mixing of VC powders.

• 한국해양공학회지
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• 제5권1호
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• pp.71-80
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• 1991

This paper reveals the effect of the effective case depth(ECD) on the fatigue behavior of a high-frequency induction hardened SM45C in rotated bending fatigue test. In addition, the effects of fracture modes(surface origin type, inner origin type) on it are discussed. The fatigue limit of the induction hardened steel is remarkably increased compared with that of base metal. In addition, the fatigue limit is linearly increased as the effective casedepth grows deep in the region of this experiment (ECD/R;0.23-0.49). The S-N curve and fracture mode in the induction case hardened steel are classified into two kinds, as a result : N$_{f}$<10$^{5}$ ;surface origin type fracture(at high stress), N$_{f}$>10$^{5}$ ; in ner origin type fracture(at low stress). In case of inner origin type fracture; as the effective case depth(ECD) gets deep, the fatigue limit is increased by the reason that the fracture origin moves toward center; in reverse, is decreased by reason that the compressive residual stress gets low. As a result, the increasing effect of the former is much bigger than the decreasing effect of the latter, and the fatigue limit is increased as the ECD gets deep.eep.

• The Journal of Advanced Prosthodontics
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• 제14권2호
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• pp.122-132
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• 2022

PURPOSE. This in-vitro analysis aimed to compare the intaglio trueness, the antagonist's wear volume loss, and fracture load of various single-unit zirconia prostheses fabricated by different manufacturing techniques. MATERIALS AND METHODS. Zirconia crowns were prepared into four different groups (n = 14 per group) according to the manufacturing techniques and generations of the materials. The intaglio surface trueness (root-mean-square estimates, RMS) of the crown was measured at the marginal, axial, occlusal, and inner surface areas. Half of the specimens were artificially aged in the chewing simulator with 120,000 cycles, and the antagonist's volume loss after aging was calculated. The fracture load for each crown group was measured before and after hydrothermal aging. The intaglio trueness was evaluated with Welch's ANOVA and the antagonist's volume loss was assessed by the Kruskal-Wallis tests. The effects of manufacturing and aging on the fracture resistance of the tested zirconia crowns were determined by two-way ANOVA. RESULTS. The trueness analysis of the crown intaglio surfaces showed surface deviation (RMS) within 50 ㎛, regardless of the manufacturing methods (P = .053). After simulated mastication, no significant differences in the volume loss of the antagonists were observed among the zirconia groups (P = .946). The manufacturing methods and simulated chewing had statistically significant effects on the fracture resistance (P < .001). CONCLUSION. The intaglio surface trueness, fracture resistance, and antagonist's wear volume of the additively manufactured 3Y-TZP crown were clinically acceptable, as compared with those of the 4Y- or 5Y-PSZ crowns produced by subtractive milling.

• Structural Engineering and Mechanics
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• 제76권6호
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• pp.725-736
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• 2020

In this work the mixed mode I/III fracture of sandstone has been studied experimentally and numerically. The experimental work used three-point bending specimens containing pre-existing cracks, machined at various inclination angles so as to achieve varying proportions of mode I to mode III loading. Dimensionless stress intensity factors were calculated using the extended finite element method (XFEM) for and compared with existing results from literature calculated using conventional finite element method. A total of 28 samples were used to conduct the fracture test with 4 specimens for each of 7 different inclination angles. The fracture load and the geometry of the fracture surface were obtained for different mode mixities. Prediction of the fracture loads and the geometry of the fracture surface were made using XFEM coupled with a cohesive zone model (CZM) and showed a good comparison with the experimental results.

• 한국음향학회지
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• 제10권3호
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• pp.13-18
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• 1991

본 연구에서는 취약한 고체의 표면에 존재하는 crack에 탄성표면파를 입사 시켰을 때 발생하는 반사계수를 측정하여 파괴응력을 해석하는 방법을 연구 분석하였다. Crack이 존재하는 취약한 고체에서의 파괴응력은 임계응력확대계수와 정규화된 최대응력확대계수의 함수로써 나타나며, 이 때 정규화된 최대응력확대계수는 탄성표면파의 반사계수를 측정하여 구할 수 있었다. 실험을 위하여 Pyrex glass원판 중앙에 깊이가 0.5mm~0.9mm인 crack을 제작하였고, SAW wedge transducer를 피치캐치(pitch-catch) 모드로 구성하여 반사계수를 측정하고 파괴응력값을 산출하였으며 UTM(Universal Testing Machine)으로 측정한 값과 비교 분석하였다.