• Title/Summary/Keyword: surface energy effects

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A study on the electrom beam weldability of 9%Ni steel (II) - Effect of $a_b$ parameter on bead shape - (9%Ni 강의 전자빔 용접성에 관한 연구 II -비이드형상에 미치는$a_b$parameter의 영향)

  • 김숙환;강정윤
    • Journal of Welding and Joining
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    • v.15 no.3
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    • pp.88-98
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    • 1997
  • Welding defects, such as porosity and spike, have sometimes occurred in deep penetration electron beam welds. These defects are known to be one of the serious problem in electron beam welds. So, effects of active parameters ($a_b$) on bead shape and occurrence of defects in electron beam welds of heavy section 9%Ni steel plates were investigated. Partial penetration welding in flat position, and deep penetration welding of 10 ~ 28mm depth were investigated in this study. It is desirable to select low accelerating voltage and above the surface focus position $a_b$$\geq$1.2 at which a wine-cup shaped bead is obtained to avoid the welding defects such as spike and root porosity. When the accelerating voltage of electron beam was low (90kV), active parameter ($a_b$) did not influence on the bead width, penetration depth and weld defects significantly. However, in case of high voltage ($\geq$120kV), active parameter ($a_b$) was sensitively associated with penetraton depth and weld defects, i.e. when the active parameter (($a_b$) was in the range of 0.6 to 1.0, the depth of penetration was always over the target (23mm), while the depth of penetration was dramatically decreased with further increase of active parameter ($a_b$). The weld defects were decreased with the increase of active parameter $a_b$ resulting in the decrease of energy density of the focused beam in the root part of fusion zone.

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COG(chip-on-glass) Mounting Using a Laser Beam Transmitting a Glass Substrate (유리 기판을 투과하는 레이저 빔을 사용한 COG(chip-on-glass) 마운팅 공정)

  • 이종현;문종태;김원용;김용석
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.4
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    • pp.1-10
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    • 2001
  • Chip-on-glass(COG) mounting of area array electronic packages was attempted by heating the rear surface of a contact pad film deposited on a glass substrate. The pads consisted of an adhesion (i.e. Cr or Ti) and a top coating layer(i.e. Ni or Cu) were healed by the UV laser beam transmitted through the glass substrate. The lather energy absorbed on the pad raised the temperature of a solder ball which is in physical contact with the pad, and formed a reflowed solder bump. The effects of the adhesion and top coating layer on the laser reflow soldering were studied by measuring temperature profile of the ball during the laser heating process. The results were discussed based on the measurement of reflectivity of the adhesion layer. In addition, the microstructures of solder bumps and their mechanical properties were examined.

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Comparison of Passivation Property on Hydrogenated Silicon Nitrides whose Antireflection Properties are Identical (반사방지 특성을 통일시킨 실리콘 질화막 간의 패시베이션 특성 비교)

  • Kim, Jae Eun;Lee, Kyung Dong;Kang, Yoonmook;Lee, Hae-Seok;Kim, Donghwan
    • Korean Journal of Materials Research
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    • v.26 no.1
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    • pp.47-53
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    • 2016
  • Silicon nitride ($SiN_x:H$) films made by plasma enhanced chemical vapor deposition (PECVD) are generally used as antireflection layers and passivation layers on solar cells. In this study, we investigated the properties of silicon nitride ($SiN_x:H$) films made by PECVD. The passivation properties of $SiN_x:H$ are focused on by making the antireflection properties identical. To make equivalent optical properties of silicon nitride films, the refractive index and thickness of the films are fixed at 2.0 and 90 nm, respectively. This limit makes it easier to evaluate silicon nitride film as a passivation layer in realistic application situations. Next, the effects of the mixture ratio of the process gases with silane ($SiH_4$) and ammonia ($NH_3$) on the passivation qualities of silicon nitride film are evaluated. The absorption coefficient of each film was evaluated by spectrometric ellipsometry, the minority carrier lifetimes were evaluated by quasi-steady-state photo-conductance (QSSPC) measurement. The optical properties were obtained using a UV-visible spectrophotometer. The interface properties were determined by capacitance-voltage (C-V) measurement and the film components were identified by Fourier transform infrared spectroscopy (FT-IR) and Rutherford backscattering spectroscopy detection (RBS) - elastic recoil detection (ERD). In hydrogen passivation, gas ratios of 1:1 and 1:3 show the best surface passivation property among the samples.

Recent Progress in Qantum Dots Containing Thin Film Composite Membrane for Water Purification (양자점이 합체된 복합 박막을 이용한 정수의 최근 발전)

  • Park, Shinyoung;Patel, Rajkumar
    • Membrane Journal
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    • v.30 no.5
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    • pp.293-306
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    • 2020
  • Increasing harmful effects of climate change, such as its effect on water scarcity, has led to a focus on developing effective water purification methods to obtain pure water. Additionally, rising levels of water pollution is increasing levels of environmental degradation, calling for sources of water treatment to remove contaminants. To purify water, osmotic processes across a semipermeable membrane can take place, and recent studies are showing that incorporating nanoparticles, including carbon quantum dots (CQDs), graphene carbon dots (GQDs), and graphene oxide quantum dots (GOQDs) are making thin film composite (TFC) membranes more effective by increasing water flux while maintaining similar levels of salt rejection, increasing the hydrophilicity of the membrane surface, showing bactericidal properties, exhibiting antifouling properties to prevent accumulation of bacteria or other microorganisms from reducing the effectiveness of the membrane, and more. In the review, the synthesis process, applications, functionality, properties, and the role of several types of quantum dots are discussed in the composite membrane for water purification.

The Effects of Water-Absorbent Softner Treatment on the End-Use Properties of Polyester Knitted Fabrics (흡습유연 처리에 의한 PET 소재의 성능 변화 분석)

  • Kwon, Young-Ah
    • The Korean Fashion and Textile Research Journal
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    • v.12 no.5
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    • pp.676-682
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    • 2010
  • Superior hydrophilic properties will allow varieties of polyester(PET) fiber materials, fabrics and industrial materials a broader scope of use. The purpose of this study was to investigate the effect of water-absorbent softener treatment on the end-use properties and the hand of polyester knitted fabrics. Two different fabrics were knitted for the summer ladies' outwear; PET jersey and PET mesh. Variables were softner treatment and stitch type(jersey and mesh). Mechanical properties of the fabric samples were measured by KES-FB system. From these, primary hand values(HV) were evaluated by the conversion equation (KW-403-KTU) and the total hand value(T.H.V.) was calculated according to the KN-304 Summer. Both water-absorbent softner treatment and stitch types affected mechanical properties and hand values of PET fabrics. Mesh were thicker than single jersey stitch. As they became thicker, tensile, shear, and compressional energy increased. It appeared that coefficient of friction of mesh stitch was larger than that of single jersey stitch. The coefficient of friction and the mean deviation of surface roughness were decreased by softener treatment. After softner treatment KOSHI and SHARI of the both PET jersey and PET mesh decreased. However, FUKURAMI values of PET jersey increased and that of PET mesh decreased. The T.H.V. of the treated PET jersey was lower than that of the untreated one, while the T.H.V. of the treated PET mesh was higher than that of the untreated one. Overall T.H.V. of the single jersey was better than that of the mesh before and after softner treatment.

Effects of Rapid Thermal Annealing on the Properties of AZO Thin Films Grown by Radio-frequency Magnetron Sputtering (라디오파 마그네트론 스퍼터링으로 증착된 AZO 박막의 특성에 대한 급속 열처리 효과)

  • Cho, Shin-Ho
    • Journal of the Korean Vacuum Society
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    • v.18 no.5
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    • pp.377-383
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    • 2009
  • Aluminum-doped zinc oxide (AZO) thin films were deposited on sapphire substrate by using radio-frequency magnetron sputtering and were performed in the temperature range of $600-900^{\circ}C$ by rapid thermal annealing (RTA). The crystallographic structure and the surface morphology were investigated by using X-ray diffraction and scanning electron microscopy, respectively. The crystallinity of the films was improved with increasing the annealing temperature and the average size of crystalline grains was found to be 50 nm. All the thin films showed an average transmittance of 92% in the wavelength range of 400-1100 nm. As the annealing temperature was increased, the bandgap energy was decreased and the violet photoluminescence (PL) signal at 400 nm replaced the ultraviolet PL signal. The electrical properties of the thin films showed a significant dependence on the annealing temperature.

Characteristics of Virtual Reflection Images in Seismic Interferometry Using Synthetic Seismic Data (합성탄성파자료를 이용한 지진파 간섭법의 가상반사파 영상 특성)

  • Kim, Ki Young;Park, Iseul;Byun, Joongmoo
    • Geophysics and Geophysical Exploration
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    • v.21 no.2
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    • pp.94-102
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    • 2018
  • To characterize virtual reflection images of deep subsurface by the method of seismic interferometry, we analyzed effects of offset range, ambient noise, missing data, and statics on interferograms. For the analyses, seismic energy was simulated to be generated by a 5 Hz point source at the surface. Vertical components of particle velocity were computed at 201 sensor locations at 100 m depths of 1 km intervals by the finite difference method. Each pair of synthetic seismic traces was cross-correlated to generate stacked reflection section by the conventional processing method. Wide-angle reflection problems in reflection interferometry can be minimized by setting a maximum offset range. Ambient noise, missing data, and statics turn to yield processing noise that spreads out from virtual sources due to stretch mutes during normal moveout corrections. The level of processing noise is most sensitive to amplitude and duration time of ambient noise in stacked sections but also affected by number of missing data and the amount of statics.

Wetting improvement of SiC/Al Metal Matrix Composite by Cu Surface Treatment (보강재에 도금된 Cu층이 Al/SiC복합재료의 젖음성에 미치는 영향)

  • Lee, Gyeong-Gu;Jo, Gyu-Jong;Lee, Do-Jae
    • Korean Journal of Materials Research
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    • v.11 no.5
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    • pp.398-404
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    • 2001
  • Effects of coating treatment of metallic Cu film on SiC for Al/SiC composite were studied. The Copper was deposited on SiC by electroless plating method. Al/sic composite was fabricated at temperature range of $670^{\circ}C$ to 90$0^{\circ}C$ under vacuum atmosphere. The wetting behavior of Al/SiC composite were analysed by SEM and XRD. The coating treatment on SiC improved wettability of Al melt on SiC considerably comparing to the non coated SiC. This improved wettability seems strongly concerned to the increase of chemical reactivity between coated layer and Al matrix. The improvement of wettability of Al melt on the Cu coated SiC was closely related to in the initial stage of reaction. The metallic film played an important role in reducing the interfacial free energy and breaking down the aluminum oxide film through the reaction with Al melt. The wetting behavior of the as-received SiC with Al melt was not uniform, indicated by the contact angles from less than $97^{\circ}$to more than $97^{\circ}$.

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Characterization of Co-AC/TiO2 Composites and Their Photonic Decomposition for Organic Dyes

  • Chen, Ming-Liang;Son, Joo-Hee;Park, Chong-Yun;Shin, Yong-Chan;Oh, Hyun-Woo;Oh, Won-Chun
    • Korean Journal of Materials Research
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    • v.20 no.8
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    • pp.429-433
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    • 2010
  • In this study, activated carbon (AC) as a carbon source was modified with different concentrations of cobalt chloride ($CoCl_2$) to prepare a Co-AC composite, and it was used for the preparation of Co-AC/$TiO_2$ composites with titanium oxysulfate (TOS) as the titanium precursor. The physicochemical properties of the prepared Co-AC/$TiO_2$ composites were characterized by $N_2$ adsorption at 77 K, X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray (EDX) analysis. The photocatalytic treatments of organic dyes were examined under an irradiation of visible light with different irradiation times. $N_2$ adsorption data showed that the composites had decreased surface area compared with the pristine AC, which was $389\;m^2/g$. From the XRD results, the Co-AC/$TiO_2$ composites contained a mixturephase structuresof anatase and rutile, but a cobalt oxide phase was not detected in the XRD pattern. The EDX results of the Co-AC/$TiO_2$ composites confirmed the presence of various elements, namely, C, O, Ti, and Co. Subsequently, the decomposition of methylene orange (MO, $C_{14}H_{14}N_3NaO_3S$) and rhodamine B (Rh.B, $C_{28}H_{31}ClN_2O_3$) in an aqueous solution, respectively, showed the combined effects of an adsorption effect by AC and the photo degradation effect by $TiO_2$. Especially, the Co particles in the Co-AC/$TiO_2$ composites could enhance the photo degradation behaviors of $TiO_2$ under visible light.

Thermal Stability and the Effect of Substrate Temperature on the Structural and Magnetic Properties of Pd/Co Multilayer Films (Pd/Co 다층박막의 구조 및 자기적 특성에 미치는 기판온도 및 열적안정성에 관한 연구)

  • 허용철;김상록;이성래;김창수
    • Journal of the Korean Magnetics Society
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    • v.3 no.4
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    • pp.298-304
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    • 1993
  • The effects of the substrate temperature and the Pd underlayer on the structure and the magnetic properties of Pd/Co multilayer films prepared by the thermal evaporation were studied. As the substrate temperature increases up to $150^{\circ}C$, the crystallinity of sublayers, (111) texture and the interface sharpness of Pd/Co multilayers were improved due to the enhanced mobility of adatoms. As results of that, the perpendicular and surface anisotropy energies were increased but the coercivity was decreased because the pinning sites of domain wall decreased due to the grain growth. The grain size of the multilayers increased with Pd underlyer thickness. Thermal degradation was enhanced at above $200^{\circ}C$ due to interdiffusion at the Pd/Co interface. The intensity of the main diffraction peak rapidly decayed in the initial stage of aging and then decreased slowly. The rapid change of the intensity in the initial stage was speculated to be due to the structural relaxation phenomena and the later stage change was due to the interdiffusion. The activation energy for the interdiffusion in Pd4/Co1 multilayers was 14.9 KCal/mole.K.

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