• Journal of Powder Materials
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• v.22 no.1
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• pp.1-5
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• 2015

Powder injection molding is an important manufacturing technology to mass produce superalloy components with complex shape. Injection molding step is particularly important for realizing a desired shape, which requires much time and efforts finding the optimum process condition. Therefore computer aided engineering can be very useful to find proper injection molding conditions. In this study, we have conducted a finite element method based simulation for the spiral mold test of superalloy feedstock and compared the results with experimental ones. Sensitivity analysis with both of simulation and experiment reveals that the melt temperature of superalloy feedstock is the most important factor for the full filling of mold cavity. The FEM based simulation matches well the experimental results. This study contributes to the optimization of superalloy powder injection molding process.

• Resources Recycling
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• v.4 no.1
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• pp.52-59
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• 1995

Treating bulk superalloy scrap with molten zinc has been studled to facililate recycling and recovery- of cobalt.Superalloys investigated were the cobalt-base Mar-M-509 and X45 and the nickel-base Rene 80. Charges withZnlscrap ratlos of 1.5-6.5 were heated to 750-9002 far 1-7.5 hours in a nitrogen atmosphere. The moltenzinc dissolved superalloy scrap and zinc was removed by vacuum distillation at 850-Wk for 4-6 hours. Ithas been concluded that the optimum conditions of decomposition for Mar-M-509 and Rene 80 \"ere dissolutiontemperature of about 850k, Znlscrap ratlo of about 5, and dissalution time of about 5.5 hours. The zinc-treatedsuperalloy prouducts were friable and reacted rapidly with acid solutions. Leaching 9mm pieces of unalloyedMar-M-509 or Rene 80 with 5 times the stolchlometric amount oi 6N HCI at 90t ior 3 hours dissolved about1.5-7.270, while leachmg of the minus 20-mesh products dissolved about 89.0-93.0%.ved about 89.0-93.0%.

• Korean Journal of Metals and Materials
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• v.49 no.7
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• pp.535-540
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• 2011

The tensile and creep behaviors of Alloy 263, which is a wrought Ni-base superalloy used for gas turbine combustion systems, was studied. Anomalous increase of yield strength and abrupt decrease of elongation with increasing temperature were observed after tensile testing at an intermediate temperature. Elongation of the superalloy decreased as the temperature increased to and above 540$^{\circ}C$, and it reached a minimum value at 760$^{\circ}C$. It was found that creep strain was also very low at the same temperature. Inhomogeneous deformation with intensive slip bands was observed in the specimens tested at low temperature. A thermally-assisted dislocation climb process was regularly conducted at high temperature. Twinning was found to be an important mechanism of both tensile and creep deformations of the superalloy at an intermediate temperature where ductility minimum was observed.

• Journal of Power System Engineering
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• v.7 no.3
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• pp.18-22
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• 2003

A Study has been made to investigate the effects of hot isostatic press(HIP) and post-HIP heat treatment on microstructures and mechanical properties of Ni-based single crystal superalloy CMSX-4. HIP process was found to heal and close micropores significantly, but did not affect the morphologies of. The elimination of as-cast micropores obtained by HIP process resulted in improved stress-rupture lives of Ni-base single crystal superalloy by 185%.

• Proceedings of the KSME Conference
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• 2005.11a
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• pp.117.2-117.2
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• 2005

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2012.10a
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• pp.545-546
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• 2012

• Journal of the Korean Society for Heat Treatment
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• v.19 no.2
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• pp.103-108
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• 2006

Microstructural evolution of Pt-aluminide coated Ni-based superalloy has been investigated with ductilization heat treatment. The Pt coat was prepared on the superalloy and then aluminide coating was conducted using a pack cementation process. Samples were heat-treated at $1050^{\circ}C$ for 2 hrs and the microstructure and element analysis were preformed. A various precipitated compounds were observed within the coating layer and the diffusion region in the Pt-aluminide coating and heat treatment, indicating that the bi-phase compounds of $PtAl_2$ and NiAl were performed during the Pt-aluminide coating, whereas $M_{23}C_6$, MC, $Ni_3Al$ and ${\sigma}$ phases were precipitated in the inter-diffusion region. The bi-phase compounds of $PtAl_2$ and NiAl were transformed into the single phase compound of $PtAl_2$ with the heat treatment, increasing the amount of carbide and ${\sigma}$ phase.

• Journal of Powder Materials
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• v.31 no.3
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• pp.255-262
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• 2024

Nano-oxide dispersion-strengthened (ODS) superalloys have attracted attention because of their outstanding mechanical reinforcement mechanism. Dispersed oxides increase the material's strength by preventing grain growth and recrystallization, as well as increasing creep resistance. In this research, atomic layer deposition (ALD) was applied to synthesize an ODS alloy. It is useful to coat conformal thin films even on complex matrix shapes, such as nanorods or powders. We coated an Nb-Si-based superalloy with TiO₂ thin film by using rotary-reactor type thermal ALD. TiO₂ was grown by controlling the deposition recipe, reactor temperature, N₂ flow rate, and rotor speed. We could confirm the formation of uniform TiO₂ film on the surface of the superalloy. This process was successfully applied to the synthesis of an ODS alloy, which could be a new field of ALD applications.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.89-92
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• 2009

As a class of materials, Ni-base superalloys are among the most difficult metal alloys to forge together with refractory metals and cobalt-base superalloys. The mechanical properties of Ni-base superalloys depend very much on grain size and the strengthening phases, $\gamma$' ($Ni_3$(Al,Ti)-type) and $\gamma$".($Ni_3$Nb-type). Especially, the control of grain size remains as a sole means for the control of mechanical properties. The grain size and distribution changes of the wrought superalloys during hot working and heat treatment are mainly controlled by the recrystallization and grain growth behaviors. In this presentation, prediction technology of grain size through the computer-aided process design, and numerical modeling for predicting the microstructure evolution of Ni-base superalloy during hot working were introduced. Also, some case studies were dealt with actual forming processes of Ni-base superalloys.

• Proceedings of the KSME Conference
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• 2001.06c
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• pp.627-632
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• 2001

Nimonic 80A superalloy with high-temperature strength and high corrosion-resistance is used in jet engine for aircraft, gas turbine for power plant and marine diesel engine, etc. To develop the manufacturing process of exhaust valve for large diesel engine using Nimonic 80A, various mechanical tests, such as hot compression, microstructure and hardness test have been performed. This results effectively used to set the reasonable forging conditions while hot forging of Nimonic 80A superalloy. Open die and closed die forging experiments are carried out from ESR ingot and finally get a good shaped exhaust valve product.