• Title/Summary/Keyword: standard measurement methods

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DC and AC Characterization of Metals Conductivity using the van der Pauw Measurement Method (Van der Pauw 측정법을 이용한 금속 도전율의 직류와 교류특성)

  • Kang, Jeon-Hong;Han, Sang-Ok
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.56 no.4
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    • pp.157-160
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    • 2007
  • The van der Pauw technique is one of the popular methods for determining the conductivity of flat metal samples. Traceability of the national standard for the conductivity has been achieved by direct current measurement techniques in national measurement institutes of many countries. But recently, alternative current measurement techniques for determining the conductivity of flat metal samples is also interested. In this study, we measured the conductivity of non-ferrous and ferrous flat metals at alternative current using van der Pauw technique. As measurement results, the conductivities of the samples were decreased according to increasing the test frequency even though the decreasing ratio was different.

Measurement of the Ice Packing Factor of an Aqueous Solution Using the Index of Refraction (굴절률을 이용한 수용액의 빙충전율 측정)

  • Peck Jong-Hyeon;Chung Dong-Yeol;Kang Chaedong;Hong Hiki
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.17 no.11
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    • pp.1088-1094
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    • 2005
  • In the present paper, a new method is proposed for the measurement of the ice packing factor (IPF) of an ice slurry using the index of refraction. The purpose of the new method is to improve the resolution of the measurement and to increase its resistance to electric noise as compared to the standard IPF measurement technique that relies on measurement of the freezing temperature. These two methods are similar in that they both obtain a concentration of aqueous solution from measured physical quantities and calculate the IPF using a relation between concentration and IPF. We experimented and compared the two methods, whose results were also compared with results from the calorimeter method obtaining the IPF directly They are in good agreement (within $5\%$), which demonstrates the validity of the newly proposed method.

New Standards for Measurement in Meridians & Acupoints by Taking the Size of Normal Male Legs (정상 성인 남자(男子) 하지부위(下肢部位)의 수혈(?穴) 정위(定位)를 위한 도량형(度量衡) 산출)

  • Yu, Shin-Jong;Kwon, Oh-Sang;Ahn, Seong-Hoon;Kim, Young-Jin;Kim, Kyung-Sik;Sohn, In-Chul;Kim, Jae-Hyo
    • Journal of Pharmacopuncture
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    • v.13 no.1
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    • pp.93-101
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    • 2010
  • Objective : Standard of measurement in Korean Medicine has been changed in dynasty and location. Thus, cun (寸) and chi (尺) as unit of measurement for meridians and acupoints could be recognized as the length of equally divided portions of a certain long bone or the distance between two anatomical landmarks and as an symbolical meaning to date. The goal of this study is to propose a new standard measurement in the metric system for the relative measurement of cun and chi as unit of measurement for meridians and acupoints in normal male legs. Methods : This study was conducted by gauging each parts of normal male legs in the metric system and comparing to the relative measurement of cun and chi as follows; to calculate 1 cun, the length of each parts was divided into the unit of cun referred to Measurement of the Bone in Neijing Lingshu (靈樞 骨度篇); it was compared the unit of cun referred to Measurement of the Bone in Neijing Lingshu with cun which was calculated by dividing subject's height into 75 cun, respectively. Result : There has no significant difference in length of 1 cun among each leg's areas based on a standard of subject's height. The unit of cun by the metric length in the legs was similar to the unit of cun referred to Measurement of the Bone in Neijing Lingshu based on each subject's height. Conclusion : It is suggested that an unit of cun as the measurement for meridians and acupoints in the male legs should be considered to the ranges from 2.4cm to 2.6cm.

Choice of Statistical Calibration Procedures When the Standard Measurement is Also Subject to Error

  • Lee, Seung-Hoon;Yum, Bong-Jin
    • Journal of the Korean Statistical Society
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    • v.14 no.2
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    • pp.63-75
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    • 1985
  • This paper considers a statistical calibration problem in which the standard as wel as the nonstandard measurement is subject to error. Since the classicla approach cannot handle this situation properly, a functional relationship model with additional feature of prediction is proposed. For the analysis of the problem four different approaches-two estimation techniques (ordinary and grouping least squares) combined with two prediction methods (classical and inverse prediction)-are considered. By Monte Carlo simulation the perromance of each approach is assessed in term of the probability of concentration. The simulation results indicate that the ordinary least squares with inverse prediction is generally preferred in interpolation while the grouping least squares with classical prediction turns out to be better in extrapolation.

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Experimental Measurement and Monte Carlo Simulation the Correction Factor for the Medium-Energy X-ray Free-air Ionization Chamber

  • Yu, Jili;Wu, Jinjie;Liao, Zhenyu;Zhou, Zhenjie
    • Journal of the Korean Physical Society
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    • v.73 no.10
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    • pp.1466-1472
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    • 2018
  • A key comparison has been made between the air-kerma standards of the National Institute of Metrology (NIM), China, and other Asia Pacific Metrology Programme (APMP) members in the medium-energy X-ray. This paper reviews the primary standard Free-air ionization chamber correction factor experimental method and Monte Carlo simulation method in the NIM. The experimental method and the Monte Carlo simulation method are adopted to obtain the correction factor for the medium-energy X-ray primary standard free-air ionization chamber at 100 kV, 135 kV, 180 kV, 250 kV four CCRI reference qualities. The correction factor has already been submitted to the APMP as key comparison data and the results are in good agreement with those obtained in previous studies. This study shows that the experimental method and the EGSnrc simulation method are usually used in the measurement of the correction factor. In particular, the application of the simulation methods is more common.

Analytical method for analyzing formaldehyde using 2, 4-DNPH and gas chromatography/FID, NPD (2,4-DNPH와 가스크로마토그래프를 이용한 포름알데히드 분석방법)

  • Jeong, Jee Yeon;Park, Seung Hyun;Yi, Gwang Yong;Oh, Se Min
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.10 no.1
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    • pp.126-146
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    • 2000
  • To develop and evaluate formaldehyde measurement method using 2,4-dinitro-phenylhydrazine (2,4-DNPH) coated sampler and gas chromatography, laboratory test and field test were conducted. Results of this study are as follows. Limit of detection(LOD) of measurement methods, HPLC-UVD, GC-NPD and GC-FID, is $0.008{\mu}g/m{\ell}$ $0.060{\mu}g/m{\ell}$, $0.472{\mu}g/m{\ell}$ respectively. Coefficiency of measurement methods, HPLC-UVD, GC-NPD and GC-FID, is 0.008, 0.009, 0.020 respectively. Desorption efficiency of sep-pak xposure aldehyde sampler and sorbent sample tube is 1.05(range : 0.99 - 1.12), 1.02(range : 0.99 - 1.06) respectively. Samples of sorbent sample tube and sep-pak xposure aldehyde sampler turned out to be stored at refrigerator, according to storage test results. Measurement methods of HPLC-UVD, GC-NPD, GC-FID, according to results of precision for the combined sampling and analytical procedure, became acceptable to OSHA evaluation standard. Field test using exposure chamber met the NIOSH overall uncertainty recommendation(less than 25%). Overall uncertainty of Sepak-HPLC(UVD), Tube-GC(NPD), Tube-GC(FID) is 11.0% - 17.0%. Consequently gas chromatography(GC-NPD, GC-FID) and high performance liquid chromatography(EPA TO-11) using 2,4-DNPH coated sampler for formaldehyde measurement turned out to be suitable to measure personal formaldehyde exposure at workplaces.

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Study on Calibration Methods of Discharge Coefficient of Sonic Nozzles using Constant Volume Flow Meter

  • Jeong, Wan-Seop;Sin, Jin-Hyeon;Gang, Sang-Baek;Park, Gyeong-Am;Im, Jong-Yeon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.17-17
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    • 2010
  • This paper address technical issues in calibrating discharge coefficients of sonic nozzles used to measure the volume flow rate of low vacuum dry pumps. The first challenging issue comes from the technical limit that their calibration results available from the flow measurement standard laboratories do not fully cover the low vacuum measurement range although the use of sonic nozzles for precision measurement of gas flow has been well established in NMIs. The second is to make an ultra low flow sonic nozzlesufficient to measure the throughput range of 0.01 mbar-l/s. Those small-sized sonic nozzles do not only achieve the noble stability and repeatability of gas flow but also minimize effects of the fluctuation of down stream pressures for the measurement of the volume flow rate of vacuum pumps. These distinctive properties of sonic nozzles are exploited to measure the pumping speed of low vacuum dry pumps widely used in the vacuum-related academic and industrial sectors. Sonic nozzles have been standard devices for measurement of steady state gas flow, as recommended in ISO 9300. This paper introduces two small-sized sonic nozzles of diameter 0.03 mm and 0.2 mm precisely machined according to ISO 9300. The constant volume flow meter (CVFM) readily set up in the Vacuum center of KRISS was used to calibrate the discharge coefficients of the machined nozzles. The calibration results were shown to determine them within the 3% measurement uncertainty. Calibrated sonic nozzles were found to be applicable for precision measurement of steady state gas flow in the vacuum process. Both calibrated sonic nozzles are demonstrated to provide the precision measurement of the volume flow rate of the dry vacuum pump within one percent difference in reference to CVFM. Calibrated sonic nozzles are applied to a new 'in-situ and in-field' equipment designed to measure the volume flow rate of low vacuum dry pumps in the semiconductor and flat display processes.

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Development of a Model System of Uncertainty Evaluations for Multiple Measurements by Isotope Dilution Mass Spectrometry: Determination of Folic Acid in Infant Formula

  • Kim, Byung-Joo;Hwang, Eui-Jin;So, Hun-Young;Son, Eun-Kyung;Kim, Yong-Seong
    • Bulletin of the Korean Chemical Society
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    • v.31 no.11
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    • pp.3139-3144
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    • 2010
  • A model system has been established for the evaluation of the uncertainty of the value from measurements of multiple subsamples by isotope dilution mass spectrometry (IDMS). In this report, we apply this model system for the evaluation of measurement uncertainty in determination of folic acid in infant formula. Five subsamples were analyzed by IDMS. The mean of the measurement results of the five subsamples was assigned as the final measurement value. The standard deviation (s) of the results from five subsamples was attributable to repeatability of the measurement. The uncertainty components in the IDMS measurement methods were categorized into two groups. Group I includes uncertainty components which give common systematic effects to all subsamples and do not contribute to the variation among multiple measurements (repeatability). Group II includes uncertainty components that give random effects on the measurement results, and are related with the measurement repeatability. These random effects are attributed to s. Therefore, the uncertainty of the final value was calculated by combining the standard deviation of the mean of multiple measurements, $s/{\surd}n$ (where n = 5), and the measurement uncertainty associated with the uncertainty components that give systematic effects.

Improving Strontium Isotope Ratio Analysis Using MC-ICP-MS (다검출기 유도결합 플라즈마 질량분석기를 이용한 스트론튬 동위원소비 분석법 개선)

  • Lee, Sin-Woo;Park, Jaeseon;Park, Hyun-Woo;Hwang, Jong Yeon;Kim, Kumhee;Chung, Hyun-Mi;Choi, Jong-Woo
    • Journal of Environmental Analysis, Health and Toxicology
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    • v.21 no.4
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    • pp.237-242
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    • 2018
  • Strontium (Sr) commonly exists in rock, groundwater, soil, plants, and animals. The Sr isotope ratio offers important information as a tracer on nature because the Sr isotopic composition is not fractionated by any biological process in these ecosystems. Hence, Sr isotope ratio has been used in several studies on tracing the Sr source for contaminated sites and human migration. In this study, we developed a separation method for Sr content, and then improved Sr isotope analysis using multi-collector inductively coupled plasma mass spectrometry (MC-ICP-MS). A powdered rock standard (NIST 2710a) was used to determine the removal of interference elements (Rb and Ca) and the recovery rate of Sr content. The results ranged from 98% to 106%. Additionally, three standard samples (NBS 987, IAPSO and NIST 1486) were analyzed to evaluate the precision and accuracy of the results. The measured $^{87}Sr/^{86}Sr$ ratio for all the samples were consistent with the reported values, within an error. These results indicate that our established Sr separation and Sr isotope measurement methods are reliable and can hence be useful in the fields of environmental and forensic sciences.

STUDIES ON THE METHOD OF MEASUREMENT OF FRAGILITY OF KOREA TOBACCO (한국산 잎담배의 부스러짐 특성 측정방법에 관하여)

  • 김기환;주영석;최영현;유광근
    • Journal of the Korean Society of Tobacco Science
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    • v.10 no.1
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    • pp.65-73
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    • 1988
  • The fragilities of the tobacco has been considered to be one of the most Important factor in determing not only the quality of the tobacco but also the economic effect to cigarettes manufacturing. The three blender methods to determine relative fragilities were compared with the Korea Tabacco & Ginseng Research Institute Standared Fragilities Test in order to established a suitable method for measuring the fragilities of Korea tobacco leaves. Fragilities measurement by the blender methods expressed either sieve aperture or fineness index and a statistical comparison of the three blender methods was made to short the mirror variance, standard deviation, coefficient of variation, slope, correlation, sensitivity index, etc.

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