• 제목/요약/키워드: standard calibration

검색결과 1,148건 처리시간 0.034초

사과 경도의 비파괴측정을 위한 검량식 개발 및 정확도 향상을 위한 연구 (Development of Calibration Model for Firmness Evaluation of Apple Fruit using Near-infrared Reflectance Spectroscopy)

  • 손미령;조래광
    • 한국식품저장유통학회지
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    • 제6권1호
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    • pp.29-36
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    • 1999
  • Using Fuji apple fruits cultivated in Kyungpook prefecture, the calibration model for firmness evaluation of fruits by near infrared(NIR) reflectance spectroscopy was developed, and the various influence factors such as instrument variety, measuring method, sample group, apple peel and selection of firmness point were investigated. Spectra of sample were recorded in wavelength range of 1100∼2500nm using NIR spectrometer (InfraAlyzer 500), and data were analyzed by stepwise multiple linear regression of IDAS program. The accuracy of calibration model was the highest when using sample group with wide range, and the firmness mean values obtained in graph by texture analyser(TA) were used as standard data. Chemometrics models were developed using a calibration set of 324 samples and an independent validation set of 216 samples to evaluate the predictive ability of the models. The correlation coefficients and standard error of prediction were 0.84 and 0.094kg, respectively. Using developed calibration model, it was possible to monitor the firmness change of fruits during storage frequently. Time, which was reached to firmness high value in graph by TA, is possible to use as new parameter for freshness of fruit surface during storage.

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암석영상분석의 신뢰도 향상을 위한 컬러보정기법 연구 (Color Calibration Method for Improvement of Reliability on Image Analysis of Rock)

  • 장윤섭;박형동
    • 터널과지하공간
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    • 제12권1호
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    • pp.1-9
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    • 2002
  • 최근 암반공학 분야에서 영상분석기법 및 상용 영상분석장비의 활용이 활발히 이루어지는 추세이다. 그러나 영상의 획득 및 분석 단계에서 발생 가능한 오차들의 문제에 대해서 많은 부분 무시되어 왔으며 관련 연구 또한 미비하였다. 객관적인 암석영상의 분석 및 신뢰도 향상을 위해서는 암석영상에 적합한 컬러보정기법의 마련이 필요하다. 이에 본 연구에서는 암석영상에 대하여 표준컬러차트를 이용한 컬러보정기법을 도입하였으며, 화강암 시료를 대상으로 획득된 영상에 대하여 컬러보정과 오차분석을 수행하였다. 그 결과 암석영상들간의 상호 비교분석이 가능하였으며 또한 영상 획득 및 분석 단계의 신뢰도 향상을 꾀할 수 있었다.

근적외 분광분석법을 이용한 나프록센 정제의 정량분석 (Quantification of Naproxen in Pharmaceutical Formulation using Near-Infrared Spectrometry)

  • 김도형;우영아;김효진
    • 약학회지
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    • 제49권1호
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    • pp.1-5
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    • 2005
  • Near-infrared (NIR) spectroscopy has been widely applied in various field, since it is nondestructive and no sample preparation is required. In this paper, NIR spectroscopy was used for the determination of naproxen in a commercial pharmaceutical preparation. NIR spectroscopy was used to determine the content of naproxen in intact naproxen tablets containing 250 mg ($65.8\%$ nominal concentration) by collecting NIR spectra in the range of $1100{\sim}1750nm$. The laboratory-made samples had $46.1{\sim}85.5\%$ nominal naproxen concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR). Model validation was performed by randomly splitting the data set into calibration and validation data set (63 samples as a calibration data set and 42 samples as a validation data set). The developed NIR calibration gave results comparable to the known values of tablets in a laboratorial manufacturing process with standard error of calibration (SEC) and standard error of prediction (SEP) of $1.06\%\;and\;1.04\%$, respectively. The NIR method showed good accuracy and repeatability. NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.

오염총량관리지역내 소하천에 대한 BASINS 4.0 및 WinHSPF의 적용과 유전알고리즘을 이용한 매개변수의 보정 (Application of BASIN 4.0 and WinHSPF to a Small Stream in Total Water Pollution Load Management Area and Calibration of Model Parameter using Genetic Algorithm)

  • 조재현;윤승진
    • 환경영향평가
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    • 제21권1호
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    • pp.161-169
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    • 2012
  • Recently various attempts have been made to apply HSPF model to calculate runoff and diffuse pollution loads of stream and reservoir watersheds. Because the role of standard flow is very important in the water quality modelling of Total Water Pollution Load Management, HSPF was used as a means of estimating standard flow. In this study, BASINS 4.0 and WinHSPF was applied to the Gomakwoncheon watershed, genetic algorithm(GA) and influence coefficient algorithm were used to calibrate the runoff parameters of the WinHSPF. The objective function is the sum of the squares of the normalized residuals of the observed and calculated flow and it is optimized using GA. Estimates of the optimum runoff parameters are made at each iteration of the influence coefficient algorithm. The calibration results showed a relatively good correspondence between the observed and the calculated values. The standard flow(Q275) of the Gomakwoncheon watershed was estimated using the ten years of weather data.

황색종 담배중 전알카로이드와 환원당 분석에 대한 불확도 측정 (Uncertainty of Total Alkaloids and Reducing Sugar Determination in Flue-cured Tobacco)

  • 백순옥;장기철;이운철;한상빈
    • 한국연초학회지
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    • 제23권1호
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    • pp.45-52
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    • 2001
  • This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

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카운터 기반 디지털 보상 기법을 이용한 위상 고정 루프 (Phase-Locked Loops using Digital Calibration Technique with counter)

  • 정찬희;;이관주;김훈기;김수원
    • 전기학회논문지
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    • 제60권2호
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    • pp.320-324
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    • 2011
  • A digital technique is adopted to calibrate the current mismatch of the charge pump (CP) in phase-locked loops. A 2 GHz charge pump PLL (CPPLL) is used to justify the proposed calibration technique. The proposed digital calibration technique is implemented simply using a counter. The proposed calibration technique reduces the calibration time by up to a maximum of 50% compared other with techniques. Also by using a dual-mode CP, good current matching characteristics can be achieved to compensate $0.5{\mu}A$ current mismatch in CP. It was designed in a standard $0.13{\mu}m$ CMOS technology. The maximum calibration time is $33.6{\mu}s$ and the average power is 18.38mW with 1.5V power supply and effective area is $0.1804mm^2$.

식품의 근적외선 반사분광분석법에서 균질의 정도가 흡광도에 미치는 영향 및 수학적 처리방법에 관한 연구 (Influence of the homogenizing grade and meathematical treatment on the determination of ground beef components with near infrared reflectance spectroscopy)

  • 오은경
    • 한국식품과학회지
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    • 제24권5호
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    • pp.408-413
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    • 1992
  • 신속간편법으로서 식품의 성분함량 측정에 이용되는 근적외 반사분광분석에서 문제가 되고 있는 시료의 균질도의 차이가 흡광도에 미치는 영향을 조사하고 흡광도로 나타난 수치를 수학적으로 처리함으로써 예측의 오차는 다음과 같이 감소하였다. 1. 세절도가 일정한 시료의 흡광도를 무변형, 1차 미분 및 2차 미분하여 calibration한 후 세절도가 다양한 시료의 성분을 예측한 결과 예측오차(standard error of prediction)는 수분함량에 있어서 1.478%, 0.658% 및 0.580%, 지방함량의 예측오차 0.949%, 0.637%, 및 0.527%이었으며 단백질 측정시 각각 0.514%, 0.493% 및 0.394%로 2차 미분의 예측오차가 모든 성분측정에서 가장 낮음을 알 수 있었다. 2. 세절도가 다양한 시료의 무변형, 1차 미분 및 2차 미분처리한 calibration을 이용하여 세절도가 다양한 시료의 성분을 예측한 결과 수분함량 예측오차는 각각 1.026%, 0.589% 및 0.568%, 지방함량 예측오차는 각각 0.828%, 0.639% 및 0.602% 이었으며 단백질함량 예측오차는 0.860%, 0.557% 및 0.399%로서 역시 2차 미분, 1차 미분, 무변형의 순으로 정확성이 높았다. 결과를 종합할 때 흡광도를 수학적으로 처리하여 calibration에 이용하므로서 calibration시료의 세절도에 관계없이 측정결과의 정확성은 높아졌다.

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Absolute Radiometric Calibration for KOMPSAT-3 AEISS and Cross Calibration Using Landsat-8 OLI

  • Ahn, Hoyong;Shin, Dongyoon;Lee, Sungu;Choi, Chuluong
    • 한국측량학회지
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    • 제35권4호
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    • pp.291-302
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    • 2017
  • Radiometric calibration is a prerequisite to quantitative remote sensing, and its accuracy has a direct impact on the reliability and accuracy of the quantitative application of remotely sensed data. This paper presents absolute radiometric calibration of the KOMPSAT-3 (KOrea Multi Purpose SATellite-3) and cross calibration using the Landsat-8 OLI (Operational Land Imager). Absolute radiometric calibration was performed using a reflectance-based method. Correlations between TOA (Top Of Atmosphere) radiances and the spectral band responses of the KOMPSAT-3 sensors in Goheung, South Korea, were significant for multispectral bands. A cross calibration method based on the Landsat-8 OLI was also used to assess the two sensors using near simultaneous image pairs over the Libya-4 PICS (Pseudo Invariant Calibration Sites). The spectral profile of the target was obtained from EO-1 (Earth Observing-1) Hyperion data over the Libya-4 PICS to derive the SBAF (Spectral Band Adjustment Factor). The results revealed that the TOA radiance of the KOMPSAT-3 agree with Landsat-8 within 5.14% for all bands after applying the SBAF. The radiometric coefficient presented here appears to be a good standard for maintaining the optical quality of the KOMPSAT-3.

수동형 원격탐지 FTIR 분광계의 Radiometric Calibration (Radiometric Calibration of FTIR Spectrometer For Passive Remote Sensing Application)

  • 김대성;박도현;최승기;나성웅
    • 한국광학회지
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    • 제17권5호
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    • pp.391-395
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    • 2006
  • 본 논문에서는 온도 제어가 가능한 blackbody를 이용하여 수동형 FTIR 분광계의 radiometric calibration을 수행하고 타당성을 살펴보았다. Radiometric calibration은 분광계로 입사되는 radiance의 온도 변화에 대한 광 검출기의 파장 별 응답특성과 기기 내부에서 발생되는 온도 및 반사율에 의해 발생되는 측정 오차를 보정하여 Planck radiance로 변환하는 기법이다. 시료에 대한 calibration 과정을 수행한 스펙트럼을 spectral library와 비교한 결과, 흡수 스펙트럼의 파장 별 선폭과 상대적인 intensity가 매우 유사하게 나타났으며 입사 광원의 온도차와 비례하여 spectral intensity가 일정하게 증가됨을 확인할 수 있었다.