• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.568-569
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• 2006

The use of the nickel free, high nitrogen stainless steel powder and nitriding during sintering of iron based materials have been shown as an alternative way to the conventional PM stainless steels containing nickel. Nitrogen as an alloying element for iron improves in an effective way the properties of sintered alloyed steels. The powder metallurgy route is a suitable way to introduce nitrogen into these alloys and, in particular, to produce high nitrogen (close to the solubility limit) stainless steels. The paper presents and discusses the nitriding behavior of nickel-free stainless steels produced by powder metallurgy method. Alloyed melt was atomized by nitrogen and in this way nitrogen was introduced into the powder. Further nitriding occurred during sintering in a nitrogen atmosphere. For comparison, compacts having the same composition as an alloyed powder were produced from elemental powders mixture. Sintering-nitriding behaviour of investigated materials has been controlled by dilatometry, chemical and X-Ray phase analysis and metallography. Mechanical properties of sintered compacts were also measured.

• Journal of Acupuncture Research
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• 제31권2호
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• pp.21-30
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• 2014

Objectives : Manufacturing and manipulation techniques of acupuncture can be interpreted as an induced electromagnetic viewpoint, as proposed in previous study. Considering from this point of view, the magnetization of needles should be essential to enhance the electromagnetic effects during the behavior of the acupuncture needling. Methods : The current disposable needles are made of non-magnetic stainless steels, so ferromagnetic materials were searched as suitable substitutes. Meanwhile, at the practical view, stainless steels are very available for the several superior properties like as corrosion resistance, strength, etc., magnetic stainless steels were first investigated. Some types of them still preserved the ferromagnetic properties of iron, so trial needles were made with them. And then magnetization of them were followed. Results : Among the hundreds types of stainless steels, martensitic or ferritic ones are ferromagnetic. The needles made with these ferromagnetic wires were magnetized, and polarized by magnetizer, and their magnetic properties were improved. Moreover, in addition to the superiority of the magnetism, the electrical and thermal conductivities of them were even better than those of the current austenitic stainless steels. Conclusions : Through the developmental study based on the electromagnetic viewpoint, the magnetized and polarized acupuncture needles were completed. This means that these needles having improved magnetism can be used to improve the electromagnetic needling effects, and moreover, their superiorities in the electrical and thermal conductivities can also give another benefits in treatments of electrical or warm needling.

• International Journal of Korean Welding Society
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• 제3권1호
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• pp.29-33
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• 2003

The ferritic stainless steels are generally considered to have poor weldability compared with that of the austenitic stainless steels. However the primary advantages of ferritic stainless steels include lower material cost than the more commonly used austenitic stainless steels and a greater resistance to stress corrosion cracking. Thus, the weldability of ferritic stainless steels was investigated in this study. In concerning the weldability, Grain size measurement test, Erichsen test and Varestraint test were involved. full penetration welds were produced by autogeneous direct current straight polarity (DCSP) and pulsed currents gas tungsten arc welding (GIAW) and the effect of pulsed currents welding on the welds was compared to that of DCSP welding. The results showed that pulsed current was effective to refine grain size in the weld metal and the finest grain size was obtained at the frequency of 150Hz. In addition, the ductility of welds was lower than that of base metal. Finally, autogeneous type 444 welds were less susceptible to macro solidification cracks, but more sensitive to micro cracks; SEM/EDS analysis indicated that all the inclusions in the crack showed enrichment of Mn, Si, O and S.

• 열처리공학회지
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• 제15권2호
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• pp.57-64
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• 2002

The 22%Cr-5%Ni-3%Mo duplex and 18%Cr-8%Ni austenitic stainless steels have been nitrogen permeated under the $1Kg/cm^2$ nitrogen gas atmosphere at the temperature range of $1050^{\circ}C{\sim}1150^{\circ}C$. The nitrogen-permeated duplex and austenitic stainless steels showed the gradual decrease in hardness with increasing depth below surface. The duplex stainless steel showed nitrogen pearlite at the outmost surface and austenite single phase in the center after nitrogen permeation treatment, while the obvious microstructural change was not observed for the nitrogen-permeated austenitic stainless steel. After solution annealing the nitrogen-permeated stainless steels(NPSA treatment) at $1200^{\circ}C$ for 10 hours, the hardness of the duplex and austenitic stainless steels was constant through the 2 mm thickness of the specimen, and the ${\alpha}+{\gamma}$ phase of duplex stainless steel changed to austenite single phase. Tensile strengths and elongations of the NPSA-treated duplex stainless steel remarkably increased compared to those of solution annealed (SA) duplex stainless steel due to the solution strengthening effect of nitrogen and the phase change from a mixture of ferrite and austenite to austenite single phase, while the NP-treated austenitic stainless steel displayed the lowest value in elongation due to inhomogeneous deformation by the hardness difference between surface and interior.

• 한국표면공학회지
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• 제37권2호
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• pp.119-127
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• 2004

In order to develop the corrosion and wear resistance of stainless steels, effects of plasma-nitriding on the surface characteristics of stainless steels containing Nb were investigated by utilizing a potentiostat. It was found that plasma nitriding at $350^{\circ}C$, compared with $500^{\circ}C$, produced a good corrosion resistance as nitriding time increased, whereas stainless steel containing low Nb content showed that pitting potential and corrosion potential decreased.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 1995년도 추계학술강연 및 발표대회 강연 및 발표논문 초록집
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• pp.9-9
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• 1995

MATERIAL AND PROCESS VARIABLES THAT STRONGLY AFFECT THE CORROSION RESISTANCE OF PA4 STAINLESS STEELS, INCLUDE : ALLOY COMPOSITION, POWDER CLEANLINESS, NITROGEN, OXYGEN AND GARBON CONTENTS, CHROMIUM DEPLETION DUE TO SURFACE EVAPORATION AND SINTERED DENSITY. THE OPTIMUM PROCESS PARAMETERS FOR DELUBRICATION AND SINTERING THAT RESULT IN LOWEST LEVELS OF NITROGEN, OXYGEN AND CARBON AND MINIMUM LEVELS OF CHROMIUM DEPLETION WILL BE PRESENTED, FOR A NUMBER OF AUSTENTIC AND FERRITIC STAINLESS STEELS. THE EFFECT OF SINTERED DENSITY ON THE CORROSION RESISTANCE OF BOTH AUSTENITIC AND FERRITIC GRADES OF STAINLESS STEEL WILL ALSO BE COVERED.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.107-112
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• 2002

Ferritic stainless steels would be the most important alloys under the chloride environment. They are a cheaper alternative to austenitic stainless steels [1]. The present study is related to gas tungsten arc welding (GTAW) characteristics of Type 444 stainless steels. The heat of welding leads to grain coarsening in the HAZ and in the weld metal of ferritic stainless steels because they solidify directly from the liquid to the ferritc phase without any intermediate phase transformation. It is therefore recommended that these alloys be welded with a low heat input and at high welding speeds. Attempts to improve weldability were made by using of direct current straight polarity (DCSP) and pulsed current GTAW processes in this study. Measuring weld bead, grain size and Erichsen test were performed and the effects of heat input, pulse frequency on the weld metal and HAZ were studied. The main results were obtained as followings: decreasing heat input was effective to control the width of weld both in DCSP welding and in pulsed current welding; pulsed current welding was found to refine the grain size effectively and the finest grain size was found at the frequency of 150Hz in pulsed current welding; it was found that decreasing heat input also refine the HAZs effectively and the frequency had no different effect on HAZ at the same heat input; the ductility could be improved effectively in pulsed current welding.

• Journal of Welding and Joining
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• 제30권5호
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• pp.13-15
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• 2012

Stainless steels is widely used in various industries due to its high strength and excellent corrosion resistance. However, in the case of fusion welding for stainless steel, chromium deficiency layer produced by chromium carbide precipitation during welding process causes corrosion-resistance to be lower and formation of intergranular corrosion. It requires a inevitable complex procedure such as pre-heating and post-heating process etc. to prevent such weld defects. From this viewpoint, the new welding process such as a solid state welding method is suited for welding of stainless steels due to its advantages over the fusion welding. Therefore this paper intends to investigate the research trend on friction stir welding, one of solid state welding processes for stainless steels.

• 열처리공학회지
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• 제17권5호
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• pp.278-282
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• 2004

Effect of pre-treatment on the gas nitriding process of austenitic stainless steels has been investigated and the following results were obtained. Minimum pre-treatment time was decreased to 5min with increasing treatment temperature from $200^{\circ}C$ to $600^{\circ}C$. Surface activation effect by the pre-treatment was maintained in the air up to holding time of 64hr, judging from the analysis result of gas nitrided specimens. The Depth of nitrided layer of STS 304 and 316 stainless steels were ranged from $5{\mu}m$ to $90{\mu}m$ at $440^{\circ}C{\sim}600^{\circ}C$. The X-ray diffraction intensity for austenitic stainless steels were increases as nitriding temperature from $440^{\circ}C$ to $600^{\circ}C$.

• Corrosion Science and Technology
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• 제15권2호
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• pp.92-107
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• 2016

Graphene was coated on austenitic and martensitic stainless steels to simulate the metallic bipolar plate of proton exchange membrane fuel cell (PEMFC). Graphene oxide (GO) was synthesized and was reduced to reduced graphene oxide (rGO) via a hydrazine process. rGO was confirmed by FE-SEM, Raman spectroscopy and XPS. Interfacial contact resistance (ICR) between the bipolar plate and the gas diffusion layer (GDL) was measured to confirm the electrical conductivity. Both ICR and corrosion current density decreased on graphene coated stainless steels. Corrosion resistance was also improved with immersion time in cathodic environments and satisfied the criteria of the Department of Energy (DOE), USA. The total concentrations of metal ions dissolved from graphene coated stainless steels were reduced. Furthermore hydrophobicity was improved by increasing the contact angle.