• Title/Summary/Keyword: spray forming

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Optimization of powder compaction parameters for the pressureless sintered ZTA (상압소결 ZTA의 분말 성형 공정 최적화)

  • 신동우;김경도;박삼식;임창성;이수완
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.2
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    • pp.356-364
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    • 1998
  • The dependence of green and sintered densities of Zirconia-Toughened Alumina ($ZTA:\;Al_2O_3/\;15\;vol{%}\;ZrO_2$) on the properties of spray-dried granules was studied thoroughly to establish the optimum compaction condition leading to high reproducibility in the light of sintered density. The sphericity, mean size, degree of hollow occurrence and moisture content of spray-dried granules were largely different in between the granule containing binder and the ones with no binder. The effect of these differences in the characteristic of granules on the compaction behavior was examined in terms of the compaction pressure from 80 MPa to 120 MPa 10 MPa increment and the compaction method, i.e., uniaxial and cold isostatic pressing. This work confirmed that the reproducibility of sintered density caused by the variation of granule property could be improved by the optimization of compaction process. The variation of sintered density was controlled within 1 % deviation by compacting the granules under a relatively low pressure of 80 MPa in an uniaxial forming and subsequent cold isostatic pressing at high pressure of 500 MPa.

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A Study on the Welds Characteristics of 200 Grade Stainless Steel for Application of Street Pole Material (가로등주 소재 적용을 위한 200계 스테인리스강의 용접부 특성 연구)

  • Lee, B.W.;Lee, D.K.;Kim, H.S.;Hong, S.H.
    • Journal of Power System Engineering
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    • v.13 no.3
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    • pp.33-39
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    • 2009
  • The aim of this study is to analyze the welds characteristics of the 205 stainless steel pipe for application of street pole material. The welds corrosion behavior of STS 205 pipe in 0.1 N sulphuric acid solution and 5% NaCl solution at room temperature was studied using both salt spray test and potentiodynamic polarization experiment. The morphology and components of corrosion products on surface of STS 205 pipe welds were investigated using SEM/EDX. The tensile strength and yield strength values of STS 205 plate were 715 MPa and 369 MPa respectively. The microvickers hardness values of STS 205 pipe welds were slightly increased than that of STS 304 pipe welds. Corrosion current density($I_{corr.}$) and critical current density($I_{crit.}$) values of STS 205 pipe welds in 3.5% NaCl solution were $1.89{\times}10^{-6}$ $A/cm^2$ and $15.8{\times}10 ^{-6}$ $A/cm^2$. The corrosion resistance of SIS 205 pipe welds was similar to its STS 304 pipe welds. The STS 205 and 304 pipe welds passive films were chromium oxide. Especially, the STS 205 pipe welds showed good corrosion resistance in 0.1 N sulphuric acid. This is attributed to the forming of protective chromium oxide on the surface of STS 205 pipe welds.

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Research on the Rheological Properties of Aqueous Film Forming Foam to Respond to Ship Oil Fires (함정 유류화재 대응을 위한 수성막포의 유변학적 특성 연구)

  • Kil-Song Jeon;Hwi-Seong Kim;Jung-Hoon You;Yong-Ho Yoo;Jin-Ouk Park
    • Applied Chemistry for Engineering
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    • v.34 no.6
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    • pp.603-607
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    • 2023
  • Aqueous film forming foam (AFFF) is a critical fire suppression agent used in combating hydrocarbon fires. This type of fire suppressant is highly effective due to its ability to form a protective film, dissipate heat, inhibit combustion, and utilize a blend of chemical substances to extinguish fires. While these properties offer significant advantages in responding to hydrocarbon fires, AFFF is distinct in its deployment as it is dispensed in the form of foam. Therefore, the rheological analysis of AFFF foam using a rheometer plays a crucial role in predicting the spray characteristics of AFFF for combating hydrocarbon fires, and this is closely associated with effective fire suppression. In this study, we conducted rheometer experiments to confirm the non-Newtonian behavior (shear-thinning) of AFFF foam and obtained data on the form's stability. These experimental data are expected to contribute to enhancing the efficiency of fire suppression systems utilizing AFFF.

Influence of Manufacturing Conditions on the Reflectance and Life Time of the Gold Protected IR Mirror (금 증착 적외선 반사판의 반사율 및 수명에 미치는 제조공정 변수의 영향)

  • Choi, Yong-Sun;Lee, Young-Ki;Lee, You-Kee
    • Korean Journal of Materials Research
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    • v.28 no.4
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    • pp.201-207
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    • 2018
  • Infrared(IR) heating has many advantages, such as energy efficiency, reduced heating time, cleanliness, equipment compactness, high drying rate and easy automation. These features of IR heating provide widely industrial applications, such as surface heat treatment in semiconductor fabrication, thermoforming of polymers, drying and disinfection of food products, heating to metal forging, and drying of wet materials. In this study, the characteristics of a protected gold mirror were examined by spectrophotometer and the lifetime of the coating layers were evaluated by a cross-cutting method and salt spray test. The effects of manufacturing conditions on the protected gold mirror were seen and remedies for these effects were noted in order to improve the properties of the protected gold mirror in the drying process. The reflectance and lifetime of the protected gold mirror was influenced by manufacturing conditions, such as surface roughness and forming conditions of the anti-oxide layer, the adhesion layer, the reflecting layer and the protection layer. The results of this study showed that the protected gold mirror manufactured using a buffing method for pre-treatment resulted in the most effective reflectance. In addition, $Al_2O_3$ coating on an Al substrate as an anti-oxide layer was more effective than the anodizing process in the test of reflectance. Furthermore, the protected gold mirror manufactured by layers forming of various materials resulted in the most effective reflectance and lifetime when coated with $Al_2O_3$ as the anti-oxide layer, coated Cr as the adhesion layer, and coated $MgF_2$ as the protection layer.

Physicochemical properties and microencapsulation process of rice fermented with Bacillus subtilis CBD2 (Bacillus Subtilis CBD2로 배양된 백미 발효물의 미세캡슐 제조 및 물리화학적 특성)

  • Lee, Dae-Hoon;Park, Hye-Mi;Hong, Joo-Heon
    • Food Science and Preservation
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    • v.22 no.2
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    • pp.225-231
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    • 2015
  • This study was conducted to examine the physicochemical properties and micro-encapsulation process of rice fermented with Bacillus subtilis CBD2. The viable bacterial cell, pH, and amylase activity of the rice liquid culture were 7.61 log CFU/mL, pH 5.08 and 159.43 units/mL, respectively. The micro-encapsulated rice liquid culture was manufactured via spray drying with different forming agents: i.e., alginic acid 1.0% and chitosan 0.3%, 0.5%, and 1.0%. The moisture contents of the spray-dried powders were approximately 2.90~3.68%. The color of the L and a value decreased whereas that of the b and ${\Delta}E$ value increased. The particle size and outer topology of the spray-dried rice liquid culture were $48.13{\sim}68.48{\mu}m$ and globular, respectively. The water absorption index of the spray-dried powder (2.40~2.65) was lower than that of the freeze-dried powder (2.66). The water solubility index of the spray-dried powder (9.17~10.89%) was higher than that of the freeze-dried powder (7.12%). The in vitro dissolution was measured for five hours in pH 1.2 simulated gastric fluid, and pH 6.8 and pH 7.4 simulated intestinal fluids, using a dissolution tester at $37^{\circ}C$ with 50 rpm agitation. The amylase survival in the fermented rice was 85.93% through the spray-drying and it was very effectively controlled.

Luminescence Characterization of SrAl2O4:Ho3+ Green Phosphor Prepared by Spray Pyrolysis (분무열분해법으로 제조된 SrAl2O4:Ho3+ 녹색 형광체의 발광특성)

  • Jung, Kyeong Youl;Kim, Woo Hyun
    • Korean Chemical Engineering Research
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    • v.53 no.5
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    • pp.620-626
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    • 2015
  • $Ho^{3+}$ doped $SrAl_2O_4$ upconversion phosphor powders were synthesized by spray pyrolysis, and the crystallographic properties and luminescence characteristics were examined by varying activator concentrations and heattreatment temperatures. The effect of organic additives on the crystal structure and luminescent properties was also investigated. $SrAl_2O_4:Ho^{3+}$ powders showed intensive green emission due to the $^5F_4/^5S_2{\rightarrow}^5I_8$ transition of $Ho^{3+}$. The optimal $Ho^{3+}$ concentration in order to achieve the highest luminescence was 0.1%. Over this concentration, emission intensities were largely diminished via a concentration quenching due to dipole-dipole interaction between activator ions. According to the dependence of emission intensity on the pumping power of a laser diode, it was clear that the upconversion of $SrAl_2O_4:Ho^{3+}$ occurred via the ground state absorption-excited state absorption processes involving two near-IR photons. Synthesized powders were monoclinic as a major phase, having some hexagonal phase. The increase of heat-treatment temperatures from $1000^{\circ}C$ to $1350^{\circ}C$ led to crystallinity enhancement of monoclinic phase, reducing hexagonal phase. The hexagonal phase, however, did not disappear even at $1350^{\circ}C$. When both citric acid (CA) and ethylene glycol (EG) were added to the spray solution, the resulting powders had pure monoclinic phase without forming hexagonal phase, and led to largely enhancement of crystallinity. Also, N,N-Dimethylformamide (DMF) addition to the spray solution containing both CA and EG made it possible to effectively reduce the surface area of $SrAl_2O_4:Ho^{3+}$ powders. Consequently, the $SrAl_2O_4:Ho^{3+}$ powders prepared by using the spray solution containing CA/EG/DMF mixture as the organic additives showed about 168% improved luminescence compared to the phosphor prepared without organic additives. It was concluded that both the increased crystallinity of high-purity monoclinic phase and the decrease of surface area were attributed to the large enhancement of upconversion luminescence.

Dyeing Technique and Aesthetics of Diffusing Image Pattern in Fashion Collection (패션 컬렉션에 나타난 번지는 이미지 문양의 염색기법과 조형미)

  • Ryu, Hyun-Jung
    • Journal of the Korea Fashion and Costume Design Association
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    • v.14 no.3
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    • pp.1-10
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    • 2012
  • This study has purpose to understanding recent trends and image effect of textile in fashion by looking to dyeing technique and aesthetics of diffusing image pattern. Further the study will hope to provide basic data for fashion and textile designer fashion. The methods of this study are academic literatures as well as practical study through case studies about actual works. Dyeing techniques and aesthetics of diffusing image pattern since 2000 fashion collection and their results are as follows. First, Dyeing techniques of diffusing image pattern are wet-dyeing and printing. There are plangi dyeing, salt dyeing, alcohol dyeing and ikat dyeing in the wet-dyeing and spray dyeing, discharge dyeing in the printing. There are tie-dyeing, rumpling-dyeing and plank-dyeing in the plangi. Second, Forming of the diffusing image pattern are due to uneven seeping and the contingency of a chemical reaction by reducing the pressure and intensity. Third, Aesthetics of diffusing image pattern are extracted purity missing childhood, fantasy escaping facts of the situation and abstraction representing informal world from formative characteristics of diffusing image pattern.

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Fire Resistance of U-shape Hybrid Composite Beam (신형상 U형 하이브리드 합성보의 내화성능에 관한 연구)

  • Kim, Sung Bae;Kim, Sang Seup;Ryu, Deog Su;Choi, Seng Kwan
    • Journal of Korean Society of Steel Construction
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    • v.25 no.4
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    • pp.379-388
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    • 2013
  • This paper aims to experimentally investigate the fire resistance of U-shaped hybrid composite beams protected by spay and paint insulations. Subjected to two and three hours of the Standard ISO fire, the flexural performance of 4.4m beams with/without imposed loadings was examined with respect to failure criteria such as deflection and deflection rate of the mid-span and temperatures measured in the steel section. The results demonstrated that the proposed configuration of the composite beam is able to achieve a very competitive 3-hour fire resistance rating in economical aspects.

Nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles of high brightness

  • Lee, Chang-Hee;Roh, Hyun-Sook;Kang, Yun-Chan;Park, Hee-Dong;Park, Seung-Bin
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.791-794
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    • 2003
  • To synthesize $Gd_{2}O_{3}:Eu$ phosphor powder of nano size and high luminescence efficiency under UV (ultraviolet) and VUV (vacuum ultraviolet) light, organic additives such as citric acid and ethylene glycol and $Na_{2}CO_{3}$ flux were introduced in large-scale spray pyrolysis and critical conditions for forming nano-sized particles were investigated. The $Gd_{2}O_{3}:Eu$ phosphor particles prepared from solutions with organic additives such as citric acid and ethylene glycol had micron size and spherical shape. However, the particles prepared from polymeric precursor solution with $Na_{2}CO_{3}$ flux had nano size and non-aggregation characteristics. The as-prepared spherical particles with micron size turned into nano-sized particles during post-treatment by recrystallization process. The nano-sized $Gd_{2}O_{3}:Eu$ phosphor particles showed higher brightness than the commercial $Y_2O_3:Eu$ phosphor product under both UV light of 254nm and VUV light of 147 nm.

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Atomization Improvement of a Liquid Jet with Wall Impingement and its Application to a Jet Engine Atomizer

  • Shiga, Seiichi
    • Journal of ILASS-Korea
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    • v.11 no.3
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    • pp.176-189
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    • 2006
  • In the present study, capability of improving the liquid atomization of a high-speed liquid jet by using wall impingement is explored, and its application to a jet engine atomize. is demonstrated. Water is injected from a thin nozzle. The liquid jet impinges on a wall positioned close to the nozzle exit, forming a liquid film. The liquid film velocity and the SMD were measured with PDA and LDSA, respectively. It was shown that the SMD of the droplets was determined by the liquid film velocity and impingement angle, regardless of the injection pressure or impingement wall diameter. When the liquid film velocity was smaller than 300m/s, a smaller SMD was obtained, compared with a simple free jet. This wall impingement technique was applied to a conventional air-blasting nozzle for jet engines. A real-size air-blasting burner was installed in a test rig in which three thin holes were made to accommodate liquid injection toward the intermediate ring, as an impingement wall. The air velocity was varied from 41 to 92m/s, and the liquid injection pressure was varied from 0.5 to 7.5 MPa. Combining wall impinging pressure atomization with gas-blasting produces remarkable improvement in atomization, which is contributed by the droplets produced in the pressure atomization mode. Comparison with the previous formulation for conventional gas-blasting atomization is also made, and the effectiveness of utilizing pressure atomization with wall impingement is shown.

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