• Journal of the Korean Ceramic Society
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• v.39 no.7
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• pp.687-692
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• 2002

Preparation of spherical single-perovskite phase PMN-PT powder was tried by surface modification of the precursor powder with magnesia sol. The ball-milled mixed powder was heat treated at 550$\^{C}$/l h to remove any volatiles. The calcined powder was treated with the magnesia sol of 0.3-1.0 wt% and followed by calcination at 800$\^{C}$/l h to give rise to single phase perovskite PMN-PT powders. The powder with a binary size of <0.3 ㎛ and -2 ㎛ was obtained for MgO(0.3), but the spherical, agglomerate-free powder of 0.5-0.8 ㎛ was obtained for MgO(0.6) as well as for MgO(1.0).

• Journal of Powder Materials
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• v.19 no.2
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• pp.122-126
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• 2012

The Fe-based self-fluxing alloy powders and TiC particles were ball-milled and subsequently compacted and sintered at various temperatures, resulting in the TiC particle-reinforced Fe self-fluxing alloy hybrid composite, and the microstructure and micro-hardness were investigated. The initial Fe-based self-fluxing alloy powders and TiC particles showed the spherical shape with a mean size of approximately 80 ${\mu}m$ and the irregular shape of less than 5 ${\mu}m$, respectively. After ball-milling at 800 rpm for 5 h, the powder mixture of Fe-based self-fluxing alloy powders and TiC particles formed into the agglomerated powders with the size of approximately 10 ${\mu}m$ that was composed of the nanosized TiC particles and nano-sized alloy particles. The TiC particle-reinforced Fe-based self-fluxing alloy hybrid composite sintered at 1173 K revealed a much denser microstructure and higher micro-hardness than that sintered at 1073 K and 1273 K.

• Journal of Powder Materials
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• v.21 no.2
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• pp.97-101
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• 2014

The 304 stainless steel powders were prepared by high energy ball milling and subsequently sintered by spark plasma sintering, and the microstructural characteristics and micro-hardness were investigated. The initial size of the irregular shaped 304 stainless steel powders was approximately 42 ${\mu}m$. After high energy ball milling at 800 rpm for 5h, the powders became spherical with a size of approximately 2 ${\mu}m$, and without formation of reaction compounds. From TEM analysis, it was confirmed that the as-milled powders consisted of the aggregates of the nano-sized particles. As the sintering temperature increased from 1073K to 1573K, the relative density and micro-hardness of sintered sample increased. The sample sintered at 1573K showed the highest relative density of approximately 95% and a micro-hardness of 550 Hv.

• Korean Journal of Materials Research
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• v.31 no.12
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• pp.677-681
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• 2021

The Mn-Zn ferrite powders were prepared by high energy ball milling, then compacted and sintered at various temperatures to assess their sintering behavior and magnetic properties. The initial ferrite powders were spherical in shape with the size of approximately 70 ㎛. After 3 h of ball milling at 300 rpm, aggregated powders ~230 nm in size and composed of ~15 nm nanoparticles were formed. The milled powders had a density of ~70 % when compacted at 490 MPa for 3 min. In the samples subsequently sintered at 1,273 K ~ 1,673 K for 3 h, the MnZnFe₂O₄ phase was detected. The density of the sintered samples had a tendency to increase with increasing sintering temperature up to 1,473 K, which produced the highest density of 98 %. On the other hand, the sample sintered at 1,373 K had the highest micro-hardness of approximately 610 Hv, which is due to much finer grains.

• Nuclear Engineering and Technology
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• v.54 no.4
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• pp.1343-1354
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• 2022

Experiments were performed to measure the critical heat flux (CHF) on a vertical surface abutting a coarse packed bed of spherical particles. This geometry is representative of a CANDU reactor calandria tubesheet facing the end shield cavity during the in-vessel retention (IVR) phase of a severe accident. Deionized light water was used as the working fluid. Low carbon steel shielding balls with diameters ranging from 6.4 to 12.7 mm were used, allowing for the development of an empirical correlation of CHF as a function of shielding ball diameter. Previously published data is used to develop a more comprehensive empirical correlation accounting for the impacts of both shielding ball diameter and heating surface height. Tests using borosilicate shielding balls demonstrated that the dependence of CHF on shielding ball thermal conductivity is insignificant. The deposition of iron oxide particles transported from shielding balls to the heating surface is verified to increase CHF non-trivially. The results presented in this paper improve the state of the knowledge base permitting quantitative prediction of CHF in the CANDU end shield, refining our ability to assess the feasibility of IVR. The findings clarify the mechanisms governing CHF in this scenario, permitting identification of potential future research directions.

• Journal of the Microelectronics and Packaging Society
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• v.21 no.4
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• pp.133-137
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• 2014

As a preceding process for preparing several micrometer sized Ag-coated Cu flakes, ball milling of submicrometer-sized Cu particles synthesized through a wet chemical method was performed in order to convert the particles into flakes. To suppress oxidation and aggregation of the particles during ball milling, ethylene glycol and ethyl acetate were used as a medium and a surface modifying agent, respectively. Results obtained with different rotation speeds of a jar indicated that the rotation speed changes a rotating mode, and strikingly alters the final shapes and shape uniformity of Cu particles after milling. The diameter of zirconia ball was also confirmed. Although there was aggregates in the initial submicrometer-sized Cu particles, therefore, well-dispersed Cu flakes with a size of several micrometers were successfully prepared by ball milling through optimization of rotation speed, amount of ethyl acetate, and diameter of zirconia ball.

• Proceedings of the KSME Conference
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• 2004.11a
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• pp.956-961
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• 2004

This paper proposes a study on the spherical lens manufacturing by simultaneous 3 axis for NC lathe. We use friction drive system for moving system in experimental diamond turing machine. The diamond turning machine use manufacturing for high quality lens, mirror and many optics products. Especially, the high tech industry require a lot of lens. For example, optical engineering. medical science, space engineering and material engineering etc. The friction drive system is very simple and quiet, compared to ball screw system. We find a problem at the simultaneous 3 axis and suggest a solution. Also, when we manufactured a micro lens. find a problem and solution.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1995.04b
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• pp.52-57
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• 1995

In order to suggest the proper cutting conditions of the CNC milling machining for the free-from surface, some experiments were carried out. In experiments, the influence of cutting conditions on the inclined spherical surface were examined by geometrical anlysis. In thos study, the roundness and cutting force were measured to know the effect of several cutting conditions on the machined surface and the cutting characteristics were carefully investigated. As the result, it was appeared that rigidder tool must be used and the cutting speed must be maintained constantlyfor more effective machining. It can be also known from the experiments that the improved machining surface obtained under about 80 degree, but coarse surface obtained over about 80 degree because of the existance of immproper shape of ball-end mill at the extreme portion.

• Journal of Powder Materials
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• v.7 no.1
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• pp.19-26
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• 2000

Al-Cr-Zr metal powders were prepared by cryo-milling(-75$^{\circ}C$),ambi-milling(25$^{\circ}C$) and warm-milling(200$^{\circ}C$) to investige the effect of milling temperature. The morphogical changes and microstructural evolution of Al-6wt.%Cr-3wt.%Zr metal powder ball milling were investigated by SEM, OM and XRD. The cryo-milling at -75$^{\circ}C$ caused the more refinement of powder particle size than ambi-milling and warm-milling. The partic morpholgy of Al-Cr-Zr metal powders changed changes into spheroidal particles at 25$^{\circ}C$and spherical particles at 200$^{\circ}C$The spherical particles were formed by agglomertion and contiuous wrapping of the spheroidal particles. The calculated Al crystallite size in Al-Cr-Zr metal powders by the Scherer equation were refined rapidly for short milling time -75$^{\circ}C$compared with milling at 25$^{\circ}C$ and 200$^{\circ}C$.

• Korean Chemical Engineering Research
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• v.54 no.6
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• pp.786-791
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• 2016

Spherical graphene balls were fabricated by an aerosol spray drying process after reduced graphene oxide was prepared by the liquid phase reaction using glucose as an environment-friendly reducing agent. Spherical morphology of the as-fabricated particles was observed by FE-SEM analysis. Diffraction patterns of spherical particles were found as graphene by XRD analysis. Sphericity of GB was controlled by the variation of operating temperature, amount of glucose, and addition of $NH_4OH$. Higher sphericity of GB was prepared at higher operating temperature in the presence of $NH_4OH$. As the amount of glucose in the liquid phase reaction increased in the presence of $NH_4OH$, sphericity of GB increased. The highest sphericity of GB was 1.1. GB of higher sphericity showed lower aggregation property than that of lower sphericity. Furthermore, as-prepared GBs were found as a potential electrode material for capacitor.