• Title/Summary/Keyword: spectral methods

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Microscopical and chemical surface characterization of CAD/CAM zircona abutments after different cleaning procedures. A qualitative analysis

  • Gehrke, Peter;Tabellion, Astrid;Fischer, Carsten
    • The Journal of Advanced Prosthodontics
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    • v.7 no.2
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    • pp.151-159
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    • 2015
  • PURPOSE. To describe and characterize the surface topography and cleanliness of CAD/CAM manufactured zirconia abutments after steaming and ultrasonic cleaning. MATERIALS AND METHODS. A total of 12 ceramic CAD/CAM implant abutments of various manufacturers were produced and randomly divided into two groups of six samples each (control and test group). Four two-piece hybrid abutments and two one-piece abutments made of zirconium-dioxide were assessed per each group. In the control group, cleaning by steam was performed. The test group underwent an ultrasonic cleaning procedure with acetone, ethyl alcohol and antibacterial solution. Groups were subjected to scanning electron microscope (SEM) analysis and Energy-dispersive X-ray spectroscopy (EDX) to verify and characterize contaminant chemical characterization non- quantitatively. RESULTS. All zirconia CAD/CAM abutments in the present study displayed production-induced wear particles, debris as well as organic and inorganic contaminants. The abutments of the test group showed reduction of surface contamination after undergoing an ultrasonic cleaning procedure. However, an absolute removal of pollutants could not be achieved. CONCLUSION. The presence of debris on the transmucosal surface of CAD/CAM zirconia abutments of various manufacturers was confirmed. Within the limits of the study design, the results suggest that a defined ultrasonic cleaning process can be advantageously employed to reduce such debris, thus, supposedly enhancing soft tissue healing. Although the adverse long-term influence of abutment contamination on the biological stability of peri-implant tissues has been evidenced, a standardized and validated polishing and cleaning protocol still has to be implemented.

Measurement of Gamma-ray Yield from Thick Carbon Target Irradiated by 5 and 9 MeV Deuterons

  • Araki, Shouhei;Kondo, Kazuhiro;Kin, Tadahiro;Watanabe, Yukinobu;Shigyo, Nobuhiro;Sagara, Kenshi
    • Journal of Radiation Protection and Research
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    • v.42 no.1
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    • pp.16-20
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    • 2017
  • Background: The design of deuteron accelerator neutron source facilities requires reliable yield estimation of gamma-rays as well as neutrons from deuteron-induced reactions. We have so foar measured systematically double-differential thick target neutron yields (DDTTNYs) for carbon, aluminum, titanium, copper, niobium, and SUS304 targets. In the neutron data analysis, the events of gamma-rays taken simultaneously were treated as backgrounds. In the present work, we have re-analyzed the experimental data for a thick carbon target with particular attention to gamma-ray events. Materials and Methods: Double-differential thick target gamma-ray yields from carbon irradiated by 5 and 9 MeV deuterons were measured using an NE213 liquid organic scintillator at the Kyushu University Tandem accelerator Laboratory. The gamma-ray energy spectra were obtained by an unfolding method using FORIST code. The response functions of the NE213 detector were calculated by EGS5 incorporated in PHITS code. Results and Discussion: The measured gamma-ray spectra show some pronounced peaks corresponding to gamma-ray transitions between discrete levels in residual nuclei, and the measured angular distributions are almost isotropic for both the incident energies. Conclusion: PHITS calculations using INCL, GEM, and EBITEM models reproduce the spectral shapes and the angular distributions generally well, although they underestimate the absolute gamma-ray yields by about 20%.

Sound Transmission Loss Measurement for Sound Isolation Sheets by Two-Microphone Impedance Tube Method (두 개의 마이크로폰의 부착된 임피던스관법을 이용한 차음시트의 음향투과손실 측정)

  • Lee, Dong-Hoon;Yong, Ho-Taek;Lee, Seung
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.14 no.1
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    • pp.63-72
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    • 2002
  • The main objective of this study is to propose a practical two-microphone impedance tube method to measure the sound transmission loss for flexible sound isolation sheets without the use of the time-consuming and expensive reverberation room. This method was based on the sound decomposition theory developed by Seybert using the spectral density functions of the incident and reflected sound waves. In order to verify the validity of the experimental results, the measured sound transmission losses from the proposed method were compared with the measured data from the reverberation room method and the calculated data from the theory satisfying the mass law of sound isolation material. The resulted trends of the sound transmission losses versus frequencies for several different sound isolation sheets were almost same for each other and agreed quite well in both methods except at some low frequency region. From the experimental results, it was found that the accuracy of sound isolation capability obtained by two-microphone impedance tube method depends upon the microphone spacing, the distance from the first microphone to the test sample surface and the test sample location.

Theoretical Modeling of Surface Wave Propagation for SASW Testing Method (수중 주파수영역표면파괴기법의 역해석 과정에서 적용되는 파동해석기법)

  • Lee, Byung-Sik
    • Journal of the Korean Geophysical Society
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    • v.3 no.4
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    • pp.251-260
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    • 2000
  • Applicabilities of two numerical methods, the 2-dimensional and the 3-dimensional method, are evaluated to inverse test results obtained from the underwater SASW(Spectral -Analysis-of-Surface-Waves) method. As a result of this study, it has been found that the 2-dimensional method can supposed to be applicable for the cases where stiffness of soil layer increases gradually with depth, and the stiffness is relatively low. For the other cases, however, it has been concluded that the 3-dimensional method needs to be applied to determine realistic theoretical dispersion curves. An example is also shown that in situ soil profile underwater is estimated from experimental dispersion curves using the 3-dimensional method. As a results, it can be concluded that the underwater SASW method can be effectively applied to explore the underwater soil condition.

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The Effect of Acupuncture at PC7(Daereung) on EEG in Normal Human Subject (대릉(大陵)(PC7) 침자가 뇌파에 미치는 영향)

  • Park, Cheol-Jin;Lee, Sang-Ryong
    • Korean Journal of Acupuncture
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    • v.27 no.2
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    • pp.141-157
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    • 2010
  • Objectives : The aim of this study is to examine the effects of acupuncture at PC7(Daereung) on normal human EEG using power spectral analysis. Methods : EEG power spectrum exhibits site-specific and state-related differences in specific frequency bands. In this study, power spectrum was used as a measure of complexity. 30 subjects (16 males and 14 females; averaged age = 23.4 years) were engaged with thirty channel EEG study. Results : In $\alpha$(alpha) band, the power values at Fp1, Fp2, F7, F8 channels(p<0.05) during PC7 treatment were significantly decreased. But, the power values at Fz channel(p<0.05) during non-acupoint treatment was significantly decreased. In $\beta$(beta) band, the power values at Fp1, Fp2 channels(p<0.05) during PC7 treatment were significantly decreased. But, the power values at Fz channel(p<0.05) during non-acupoint treatment was significantly decreased and at F8, TCP2 channels(p<0.05) during non-acupoint treatment were increased. In $\theta$(theta) band, the power values at Fp1, Fp2, F7, F8 channels(p<0.05) during PC7 treatment were significantly decreased. But, the power values at Fz channel(p<0.05) during non-acupoint treatment was significantly decreased. In $\delta$(delta) band, the power values at Fp1, Fp2, F7, Fz, F8 channels (p<0.05) during PC7 treatment were significantly decreased. But, the power values at Fz channel (p<0.05) during non-acupoint treatment was significantly decreased. $\alpha/\beta$ values during PC7 treatment were decreased. $\beta/\theta$ values during PC7 treatment were decreased. Conclusion : These results suggest that acupuncture at PC7 induce the change on $\alpha$(alpha), $\beta$(beta), $\theta$ (theta), $\delta$(delta) wave values being decreased and and bothe $\alpha/\beta$ and $\beta/\theta$ values being decreased respectively. This is considered that acupuncture at PC7 affects the activity of cerebral cortex and endocrine system.

Spherical Harmonics Power-spectrum of Global Geopotential Field of Gaussian-bell Type

  • Cheong, Hyeong-Bin;Kong, Hae-Jin
    • Journal of the Korean earth science society
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    • v.34 no.5
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    • pp.393-401
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    • 2013
  • Spherical harmonics power spectrum of the geopotential field of Gaussian-bell type on the sphere was investigated using integral formula that is associated with Legendre polynomials. The geopotential field of Gaussian-bell type is defined as a function of sine of angular distance from the bell's center in order to guarantee the continuity on the global domain. Since the integral-formula associated with the Legendre polynomials was represented with infinite series of polynomial, an estimation method was developed to make the procedure computationally efficient while preserving the accuracy. The spherical harmonics power spectrum was shown to vary significantly depending on the scale parameter of the Gaussian bell. Due to the accurate procedure of the new method, the power (degree variance) spanning over orders that were far higher than machine roundoff was well explored. When the scale parameter (or width) of the Gaussian bell is large, the spectrum drops sharply with the total wavenumber. On the other hand, in case of small scale parameter the spectrum tends to be flat, showing very slow decaying with the total wavenumber. The accuracy of the new method was compared with theoretical values for various scale parameters. The new method was found advantageous over discrete numerical methods, such as Gaussian quadrature and Fourier method, in that it can produce the power spectrum with accuracy and computational efficiency for all range of total wavenumber. The results of present study help to determine the allowable maximum scale parameter of the geopotential field when a Gaussian-bell type is adopted as a localized function.

Prediction of Precipitated Wax Amounts Using FTIR Spectroscopy (FTIR을 이용한 왁스 침전의 정량적 예측)

  • Oh, Kyeongseok
    • Korean Chemical Engineering Research
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    • v.51 no.3
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    • pp.376-381
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    • 2013
  • High molecular weight paraffinic waxes dissolved in oil phases can be precipitated when the surrounding temperature becomes lower than the wax appearance temperature (WAT). While the various methods of WAT determination have been developed, the determination of precipitated wax amount has not been comparably popular at temperatures below the WAT. It is important to predict how much solid wax content precipitates in temperature variance. The study develops the previous method which uses integrated areas determined at a wavenumber range of 735~715 $cm^{-1}$. This method uses two different wavenumber ranges, 735~715 $cm^{-1}$ and 1,402~1,324 $cm^{-1}$. The study shows how the method provides reliable data in the variety of applications regardless of FTIR spectral instability often occurred, such as volume reduction during cooling procedure and existence of emulsified water in oil phase.

Applications of Discrete Wavelet Analysis for Predicting Internal Quality of Cherry Tomatoes using VIS/NIR Spectroscopy

  • Kim, Ghiseok;Kim, Dae-Yong;Kim, Geon Hee;Cho, Byoung-Kwan
    • Journal of Biosystems Engineering
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    • v.38 no.1
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    • pp.48-54
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    • 2013
  • Purpose: This study evaluated the feasibility of using a discrete wavelet transform (DWT) method as a preprocessing tool for visible/near-infrared spectroscopy (VIS/NIRS) with a spectroscopic transmittance dataset for predicting the internal quality of cherry tomatoes. Methods: VIS/NIRS was used to acquire transmittance spectrum data, to which a DWT was applied to generate new variables in the wavelet domain, which replaced the original spectral signal for subsequent partial least squares (PLS) regression analysis and prediction modeling. The DWT concept and its importance are described with emphasis on the properties that make the DWT a suitable transform for analyzing spectroscopic data. Results: The $R^2$ values and root mean squared errors (RMSEs) of calibration and prediction models for the firmness, sugar content, and titratable acidity of cherry tomatoes obtained by applying the DWT to a PLS regression with a set of spectra showed more enhanced results than those of each model obtained from raw data and mean normalization preprocessing through PLS regression. Conclusions: The developed DWT-incorporated PLS models using the db5 wavelet base and selected approximation coefficients indicate their feasibility as good preprocessing tools by improving the prediction of firmness and titratable acidity for cherry tomatoes with respect to $R^2$ values and RMSEs.

Possibility of Wood Classification in Korean Softwood Species Using Near-infrared Spectroscopy Based on Their Chemical Compositions

  • Park, Se-Yeong;Kim, Jong-Chan;Kim, Jong-Hwa;Yang, Sang-Yun;Kwon, Ohkyung;Yeo, Hwanmyeong;Cho, Kyu-Chae;Choi, In-Gyu
    • Journal of the Korean Wood Science and Technology
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    • v.45 no.2
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    • pp.202-212
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    • 2017
  • This study was to establish the interrelation between chemical compositions and near infrared (NIR) spectra for the classification on distinguishability of domestic gymnosperms. Traditional wet chemistry methods and infrared spectral analyses were performed. In chemical compositions of five softwood species including larch (Larix kaempferi), red pine (Pinus densiflora), Korean pine (Pinus koraiensis), cypress (Chamaecyparis obtusa), and cedar (Cryptomeria japonica), their extractives and lignin contents provided the major information for distinction between the wood species. However, depending on the production region and purchasing time of woods, chemical compositions were different even though in same species. Especially, red pine harvested from Naju showed the highest extractive content about 16.3%, whereas that from Donghae showed about 5.0%. These results were expected due to different environmental conditions such as sunshine amount, nutrients and moisture contents, and these phenomena were also observed in other species. As a result of the principal component analysis (PCA) using NIR between five species (total 19 samples), the samples were divided into three groups in the score plot based on principal component (PC) 1 and principal component (PC) 2; group 1) red pine and Korean pine, group 2) larch, and group 3) cypress and cedar. Based on the chemical composition results, it was concluded that extractive content was highly relevant to wood classification by NIR analysis.

Characteristics on the rolling response of a small fishing boat according to the waves and the ship's speed (파랑의 조우각과 선속 변화에 따른 어선의 횡동요 특성)

  • Kang, Il-Kwon;Kim, Hyung-Seok;Kim, Min-Seok;Lee, Yoo-Won;Kim, Jung-Chang;Jo, Hyo-Jae;Lee, Chun-Ki
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.43 no.1
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    • pp.62-70
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    • 2007
  • Marine casualties of vessel are serious problems on social and national aspects, because it results in sacrifice of lives, a great lose of properties and marine pollution. According to recent statistics of marine casualties of vessel, fishing boats are more likely to be ended in the casualty, and especially, small fishing boats cause much more accidents than any other big vessels. Most of marine casualties were caused by the human factors such as poor watch keeping, inadequate manoeuvering and negligent action for engine, etc. This study is intended to provide navigator of small fishing boat with a specific information of necessary to assist both the manoeuvering and the avoidance of capsizing. The manoeuvering characteristics of ship can be adequately judged by the results of typical ship trials manoeuvres. For this purpose, the author measured the roll responses of a small fishing boat in waves using the real sea experimental measuring system, and analyzed the experimental data by the statistical and spectral analyzing methods to get the characteristics of the roll motion responses of the small boat through the wave directions and the ship's speed.