• 한국식품과학회지
• /
• 제12권4호
• /
• pp.305-312
• /
• 1980

우리나라에서 처음 재배(栽培)를 시작한 elderberry anthocyanin의 화학구조(化學構造)를 동정하고 함량(含量)을 측정(測定)하였다. Elderberry열매에서 1% HCl MeOH로 추출(抽出)하여 얻은 색소농축액(色素濃縮液)을 Amberlite IRC-50 양(陽)이온교환수지관을 통과시켜 정제(精製)하고 paper chromatography로 개별색소(個別色素)를 분리(分離)하였다. 각(各) 개별색소(個別色素)에 대해 부분산가수분해(部分酸加水分解), acyl group, 결합당(結合糖), aglycone의 확인(確認), paper chromatography로 얻은 $R_f$값, spectral data 등을 기초로 구조를 확인(確認)하였다. 확인(確認)된 elderberry중(中)의 5가지 색소(色素)는 cyanidin-3-glucoside, cyanidin-3,5-diglucoside, cyanidin-3,5-diglucoside with p-coumaric arid, cyanidin-3-xyloglucoside-5-glucoside, cyanidin-3-xyloglucoside-5-glucoside with p-coumaric acid이었다. 총 anthocyanin양은 elderberry 1g당 3.13mg이고 개별색소(個別色素)의 비(比)는 cyanidin-3-glucoside 4.3%, cyanidin-3,5-diglucoside 28.3%, cyanidin-3,5-diglucoside with p-coumaric arid 12.9%, cyanidin-3-xyloglucoside-5-glucoside 38.3%, cyanidin-3-xyloglucoside-5-glucoside with p-coumaric acid가 16.2%이었다.

• 한방재활의학과학회지
• /
• 제19권2호
• /
• pp.241-250
• /
• 2009

Objectives : To study autonomic nervous system dysfunction of Low Back Pain(LBP) patients, using spectral analysis of Heart Rate Variability(HRV). Methods : HRV of 190 patients was measured and seperated into two groups, those with LBP(n=95) and healthy controls(n=95). HRV was measured by SA-6000(Medicore, Korea) for 5 minutes after 5 minutes' resting. Results : 1. Mean heart rate(MHRT) of the experimental group was slightly higher than that of the control group, but did not show significant difference(P=0.428). The square root of the mean squared differences of successive normal-to-normal intervals(RMSSD), logarithmic very low frequency power(Ln VLF) and low frequency power/high frequency power ratio(LH/HF ratio) were not significantly low between experimental group and control group(P=0.16, 0.130, 0.537). 2. The standard deviation of all the normal-to-normal intervals(SDNN), logarithmic total power(Ln TP), logarithmic low frequency power(Ln LF) and logarithmic high frequency power(Ln HF) were significantly low between experimental group and control group(P=0.03, 0.005, 0.001, 0.007). 3. Ln LF of acute group was significantly low compared with those of chronic group(P= 0.039). Conclusions : This study suggests the activity and imbalance of autonomic nervous system in LBP is low. Also sympathetic nervous system of acute LBP is lower than that of chronic LBP. Further study of HRV related to LBP is needed in the clinical medicine.

• 대한치과기공학회지
• /
• 제39권3호
• /
• pp.145-152
• /
• 2017

Purpose: This study sought to identify changes in the mechanical characteristics and color of zirconia according to different sintering temperatures of the substance. Methods: This study processed some specimens of zirconia into those of $8mm(H){\times}10mm(W){\times}50mm(L){\pm}0.1$ each, and sintered them at $1450{\sim}1600^{\circ}C$ on a $50^{\circ}C-interval$ basis in order to examine how their mechanical characteristics and color are changed. Each specimen sintered using the spectral colorimetric apparatus (Easyshade, VITA, Germany) was observed for each of the color change by sintering temperature. Results: When those specimens were sintered at $1450{\sim}1600^{\circ}C$, they were 0% in absorption ratio and porosity, 20% in shrinkage ratio and $6.10g/cm^3$ in specific gravity. Absorption ration, porosity, shrinkage ratio and specific gravity all didn't vary depending on the sintering temperature. The fracture strength of the specimens was highest or 1037MPa at the sintering temperature of $1550^{\circ}C$ and a little lower or 989MPa at that of $1600^{\circ}C$. No variation in L* value was found depending on the sintering temperature of the specimens, while c* value was highest at that of $1450^{\circ}C$. In addition, h* value was highest when the specimens was sintered at $1550^{\circ}C$. Conclusion: This study could determine how zirconia shows changes in mechanical characteristics and color in accordance with different temperatures of its sintering. It is necessary to supplement the physical data of colored transparent zirconia block which is expected to be widely used in clinical practice.

• Structural Engineering and Mechanics
• /
• 제59권3호
• /
• pp.455-473
• /
• 2016

Methods for the seismic demands evaluation of structures require iterative procedures. Many studies dealt with the development of different inelastic spectra with the aim to simplify the evaluation of inelastic deformations and performance of structures. Recently, the concept of inelastic spectra has been adopted in the global scheme of the Performance-Based Seismic Design (PBSD) through Capacity-Spectrum Method (CSM). For instance, the Modal Pushover Analysis (MPA) has been proved to provide accurate results for inelastic buildings to a similar degree of accuracy than the Response Spectrum Analysis (RSA) in estimating peak response for elastic buildings. In this paper, a simplified nonlinear procedure for evaluation of the seismic demand of structures is proposed with its applicability to multi-degree-of-freedom (MDOF) systems. The basic concept is to write the equation of motion of (MDOF) system into series of normal modes based on an inelastic modal decomposition in terms of ductility factor. The accuracy of the proposed procedure is verified against the Nonlinear Time History Analysis (NL-THA) results and Uncoupled Modal Response History Analysis (UMRHA) of a 9-story steel building subjected to El-Centro 1940 (N/S) as a first application. The comparison shows that the new theoretical approach is capable to provide accurate peak response with those obtained when using the NL-THA analysis. After that, a simplified nonlinear spectral analysis is proposed and illustrated by examples in order to describe inelastic response spectra and to relate it to the capacity curve (Pushover curve) by a new parameter of control, called normalized yield strength coefficient (${\eta}$). In the second application, the proposed procedure is verified against the NL-THA analysis results of two buildings for 80 selected real ground motions.

• Safety and Health at Work
• /
• 제11권2호
• /
• pp.207-214
• /
• 2020

Background: Prolonged sitting at work can lead to adverse health outcomes. The health risk of office workers is an increasing concern for the society and industry, with prolonged sitting work becoming more prevalent. Objective: This study aimed to explore the variation in muscle activities during prolonged sitting work and found out when and how to take a break to mitigate the risk of muscle symptoms. Methods: A preliminary survey was conducted to find out the prevalence of muscle discomfort in sedentary work. Firstly, a 2-h sedentary computer work was designed based on the preliminary study to investigate the variation in muscle activities. Twenty-four participants took part in the electromyography (EMG) measurement study. The EMG variations in the trapezius muscle and latissimus dorsi were investigated. Then the intervention time was determined based on the EMG measurement study. Secondly, 48 participants were divided into six groups to compare the effectiveness of every break type (passive break, active break of changing their posture, and stand and stretch their body with 5 or 10 mins). Finally, data consisting of EMG amplitudes and spectra and subjective assessment of discomfort were analyzed. Results: In the EMG experiment, results from the joint analysis of the spectral and amplitude method showed muscle fatigue after about 40 mins of sedentary work. In the intervention experiment, the results showed that standing and stretching for 5 mins was the most effective break type, and this type of break could keep the muscles' state at a recovery level for about 30-45 mins. Conclusions: This study offers the possibility of being applied to office workers and provides preliminary data support and theoretical exploration for a follow-up early muscle fatigue detection system.

• Journal of Ginseng Research
• /
• 제40권3호
• /
• pp.245-250
• /
• 2016

Background: Ginsenosides are the major effective ingredients responsible for the pharmacological effects of ginseng. Malonyl ginsenosides are natural ginsenosides that contain a malonyl group attached to a glucose unit of the corresponding neutral ginsenosides. Methods: Medium-pressure liquid chromatography and semipreparative high-performance liquid chromatography were used to isolate purified compounds and their structures determined by extensive one-dimensional- and two-dimensional nuclear magnetic resonance (NMR) experiments. Results: A new saponin, namely malonyl-ginsenoside Re, was isolated from the fresh flower buds of Panax ginseng, along with malonyl-ginsenosides Rb1, Rb2, Rc, Rd. Some assignments for previously published $^1H$- and $^{13}C$-NMR spectra were found to be inaccurate. Conclusion: This study reports the complete NMR assignment of malonyl-ginsenoside Re, $Rb_1$, $Rb_2$, Rc, and Rd for the first time.

• 대한화학회지
• /
• 제22권4호
• /
• pp.239-244
• /
• 1978

Stilbene 유도체인 trans-1,2-bispyrazylethylene에 대한 분광학적 연구를 행하였다. 보통의 자외선 흡수스펙트럼에서는 $n{\rightarrow}{\pi}^*$ 흡수밴드는 에너지가 비슷한 ${\pi}{\rightarrow}{\pi}^*$ 흡수밴드에 가려져서 나타나지 않는데 2차 미분 스펙트럼과 저온(77˚K)에서의 스펙트럼으로 부터 $n{\rightarrow}{\pi}^*$ 흡수 밴드를 확인할 수가 있었다. 또한 ${\pi}{\rightarrow}{\pi}^*$ 흡수밴드들의 전이에너지를 PPP-SCF-CI MO 방법으로 계산한 결과 스펙트럼에서 얻은 값과 잘 일치했다. 형광스펙트럼, 형광편광스펙트럼, 그리고 PPP-SCF-CI MO 방법에 의한 계산으로부터 형광을 내는 상태는 $^1({\pi},\;{\pi}^*)$ 상태임을 알 수가 있었으며 이것은 형광에 대한 alkaline salt effect의 결과와 일치한다.

• 대한한방부인과학회지
• /
• 제20권1호
• /
• pp.199-213
• /
• 2007

Purpose : This research was designed to determine whether HRV can be used as an assessment index in weakly postpartum women. Methods : The subjects were 232 women who admitted for postpartum care in Oriental Hospital of Woosuk University from 19, December 2005 to 21, July 2006. They took the test of CBC and HRV. And then we selected 200 cases of postpartum women. The SPSS 10.0 for windows was used to analyse the data and the simple correlation coefficient and the independent samples t-test were used to verify the results. Results : The following results were obtained : 1. There were positive correlations between items of CBC(RBC, Hb, Hct) and SDSD, RMSSD, SDNN, and also between items of CBC and log-transformed index of spectral analysis. There were negative correlations between items of CBC and Mean-HRV, pNN50. 2. SDNN of anemic postpartum women group significantly decreased compared with that of normal postpartum women group. HRV-Index, RMSSD and SDSD of anemic postpartum women group significantly decreased compared with that of normal postpartum women group. pNN50 of anemic postpartum women group significantly increased compared with that of normal postpartum women group. 3. Ln(TP), Ln(VLF), Ln(LF) and Ln(HF) of anemic postpartum women group significantly decreased compared with that of normal postpartum women group. Conclusion : The results suggest that the function of heart of anemic postpartum women group significantly decreased compared with that of normal postpartum women group.

• 대기
• /
• 제26권1호
• /
• pp.1-18
• /
• 2016

Eleven Tropical Cyclone (TC) intensity guidance models in the western North Pacific have been validated over 2008~2014 based on various analysis methods according to the lead time of forecast, year, month, intensity, rapid intensity change, track, and geographical area with an additional focus on TCs that influenced the Korean peninsula. From the evaluation using mean absolute error and correlation coefficients for maximum wind speed forecasts up to 72 h, we found that the Hurricane Weather Research and Forecasting model (HWRF) outperforms all others overall although the Global Forecast System (GFS), the Typhoon Ensemble Prediction System of Japan Meteorological Agency (TEPS), and the Korean version of Weather and Weather Research and Forecasting model (KWRF) also shows a good performance in some lead times of forecast. In particular, HWRF shows the highest performance in predicting the intensity of strong TCs above Category 3, which may be attributed to its highest spatial resolution (~3 km). The Navy Operational Global Prediction Model (NOGAPS) and GFS were the most improved model during 2008~2014. For initial intensity error, two Japanese models, Japan Meteorological Agency Global Spectral Model (JGSM) and TEPS, had the smallest error. In track forecast, the European Centre for Medium-Range Weather Forecasts (ECMWF) and recent GFS model outperformed others. The present results has significant implications for providing basic information for operational forecasters as well as developing ensemble or consensus prediction systems.

• 한국지능시스템학회논문지
• /
• 제17권7호
• /
• pp.945-951
• /
• 2007

잡음의 제거는 음성을 인터페이스로 하는 기기들에 필수적이라고 할 수 있다. 실질적으로 통화 품질이나 음성 인식률은 음성 입력부의 주변에서 들어오는 원치 않는 가산성 잡음에 의해서 크게 열화된다. 본 논문에서는 기본적으로 두 개의 마이크로폰을 이용한 잡음제거 방법을 제안한다. 마이크를 여러 개 사용했을 때의 장점은 방향 정보를 이용할 수 있다는 것인데 이는 사람 목소리, 음악 소리 등의 비정상성 잡음을 제거하는 데에 유용하다. 제안된 잡음제거 알고리즘은 위너필터에 기반 한다고 볼 수 있다. 위너필터에 의한 잡음제거를 위해서는 검출하고자 하는 음성과 제거하고자 하는 잡음의 주파수 응답이 동시에 추정 가능해야 한다. 이를 위해서 주파수 영역에서 스펙트럼 분류를 시행하여 위너필터 기반의 잡음제거에 필요한 정보를 얻는다. 제안된 알고리즘을 이용한 성능은 잘 알려진 프로스트 (Frost) 알고리즘 및 적응 모드 컨트롤러를 갖는 generalized sidelobe canceller (GSC)와 비교하였다. 성능의 지표로는 객관적 음질 평가의 방법 중에서 널리 쓰이고 있는 perceptual evaluation of speech quality (PESQ) 및 음성 인식률이 사용되었다.