• 제목/요약/키워드: specimen condition

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An Electrochemical Evaluation on the Crevice Corrosion of 430 Stainless Steel with Variation of Crevice Wide by Micro Capillary Tubing Method (Micro Capillary Tube 방법을 이용한 430 스테인레스강 틈의 폭변화에 따른 틈부식의 전기화학적 평가)

  • Na, Eun-Young
    • Journal of the Korean Electrochemical Society
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    • v.6 no.4
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    • pp.250-254
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    • 2003
  • In this study, the IR drop theory was adopted to explain the initiation of crevice corrosion in the framework of IR drop in crevice electrolyte. Furthermore, the electrochemical polarization was measured to study the mechanism of crevice corrosion for type STS430 stainless steel. lest method adopts under condition that the size of specimen is $10\times20\times5mm,\;in\;1N\;H_2SO_4+0.1N\;NaCl$ solution, and the artificial crevice gap sizes are three kinds, the Micro capillary tube size is inner diameter 0.04 mm, outer diameter 0.08 mm. Crevice corrosion is measured under the applied voltage of passivation potential -200mV/SCE, resulted from anodic potentio-dynamic polarization to the external surface along the crevice. The potential difference was measured by depth profile by Micro capillary tube which inserted in the crevice. The obtained results of this study showed that 1) As artificial crevice gap size became narrow, the current density was increased, whereas no crevice corrosion was found in the crevice gap size $3\times0.5\times16mm\;in\;1N\;H_2SO_4+0.1N\;NaCl\;solution\;at\;20^{\circ}C$ 2) potential of the crevice was about from -220 to -358mV which is lower than that of external surface potential of -200mV The results so far confirmes that the potential drop(so-called IR drop) in the crevice is one of the major mechanisms the process of crevice corrosion for 430 stainless steel.

E-cadherin Expression in Colonic Epithelium of Various Colitis in Children (소아에서 발생한 대장의 염증성 질환에서 E-cadherin의 발현)

  • Lee, Na-Young;Park, Do-Youn;Park, Jae-Hong
    • Pediatric Gastroenterology, Hepatology & Nutrition
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    • v.12 no.2
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    • pp.177-182
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    • 2009
  • Purpose: Colitis is a condition associated with a spectrum of altered morphologic changes and cellular adhesion. E-cadherin plays a key role in the establishment and maintenance of epithelial tissue structure and cell-cell adhesion. The purpose of this study is to evaluate E-cadherin expression in colonic epithelium of various colitis in children. Methods: The expressions of E-cadherin were examined in 39 cases of colonic mucosal biopsy specimen using immunohistochemical staining. When more than 50 percent of cells exhibited uniformly the same intensity and pattern of immunostaining as the adjacent normal mucosa, the antigen expression was considered normal. Abnormal expression was defined when less than 50 percent of cells stained, when cells showed a heterogeneously weak or altered distribution, or when complete absence of staining was observed. Results: Fifteen cases with non-specific colitis (38.5%), 7 cases of with Crohn's disease (17.9%), 5 cases of infectious colitis and milk protein sensitive proctocolitis (12.8%), 3 cases of ulcerative colitis (7.7%), 2 cases of Henoch-Schonlein purpura colitis (5.1%), one case of Behcet's disease and ischemic colitis (2.6%) were included in this study. E-cadherin expression was decreased in all kinds of colitis. Reduced expression of E-cadherin was observed in 77 percent of cases. E-cadherin was weaker or no expression in reparative epithelium and "ulcer associated cell lineage". Conclusion: Altered expression of E-cadherin occurs during mucosal inflammation in any kinds of colitis. These changes may be involved in promoting cell migration during epithelial restitution of the gastrointestinal mucosa.

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Comparisons of Effectiveness of the Supercritical Fluid Extraction Dewaxing on the Beeswax-Treated Paper with Different Aging Degrees (열화율이 상이한 밀랍지의 초임계유체추출 탈랍처리효과 비교분석)

  • Jeong, Hye Young;Kang, Young Suk;Go, In Hee;Yang, Eun Jeong;Choi, Kyoung Hwa
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.46 no.6
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    • pp.56-62
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    • 2014
  • This study aims to investigate the applicability of supercritical fluid extraction as a dewaxing technique to restore the beeswax-treated volume of the Annals of the Joseon Dynasty in various deterioration and damage conditions. Thus, this study analyzed the dewaxing efficiency and changes in physical and morphological properties before and after dewaxing, by applying the optimal supercritical fluid extraction dewaxing condition ($70^{\circ}C$, 40 MPa, $CO_2$, Co-solvent 20% DCM, 2 hour) to 3 kinds of beeswax-treated paper with different deterioration rates (dry artificial aging of 10, 20 and 30 days at $120^{\circ}C$). After dry artificial aging at $120^{\circ}C$ for 30 days, the average molecular weight of the beeswax-treated specimen was $1.856{\times}10^5g/mol$, showing deterioration about 80% of the beeswax-treated paper before dewaxing. It was a similar level to the molecular weight of the bees-waxed volume of the Annals of the Joseon Dynasty that has a higher degree of damage. As a result of analyzing the dewaxing efficiency through FT-IR analysis, this study discovered that it was possible to effectively dewax beeswax-treated paper in the range of deterioration 20 to 80% with this supercritical fluid extraction dewaxing technique applied. As a result of analyzing changes in the physical and morphological properties before and after dewaxing, the viscosity tended to decrease to a slight degree, and since no morphological deformation or damage of stencil fibers was found, it was concluded possible to conduct stable dewaxing through this supercritical fluid extraction technique.

Study on Application of Filling Material for Reinforcement of Soil Murals in Buddhist Temple (토벽화 균열부 보강에 사용되는 충전제 적용 연구)

  • Lee, Kyeong Min;Lee, Hwa Soo;Han, Kyeong Soon
    • Journal of Conservation Science
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    • v.29 no.4
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    • pp.395-406
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    • 2013
  • The conservation of damaged object should be restored by the similar material with the original and they have to reversibility as possible as. The characteristics of Buddhist mural paintings composed of clay are with soft material. So far, there have been a number of researches done on filling material that reinforces cracks and exfoliation of mural painting. Based on the application of traditional materials, it was found that they are appropriate to various applications. However, only based on those research results, there are some constraints to the application in the field. In addition, there has been only a few researches done on physical characteristics of filling materials. A major issue is that there is not any standard established on various mixing ratio, which is required for treatment of mural painting. This study was carried out to understand the physical characteristics of filling materials on clay mural painting. The 1st test was conducted to analyze test specimen in twelve different conditions by varying soil mixing ratio and organic medium. The 2nd test was conducted to manufacture filling materials appropriate to the mural painting, based on the result of stable condition from the 1st test, and which was applied to treatment in field.

Development of Rustling Sound Generator Using Reciprocating Motion and Evaluation of Its Fabric Sound (왕복운동에 의한 직물마찰음발생장치의 개발 및 이를 이용한 직물소리 평가)

  • Kim Chun-Jeong;Cho Gil-Soo
    • Science of Emotion and Sensibility
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    • v.9 no.2
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    • pp.133-140
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    • 2006
  • In order to investigate the sensation of the fabric sound simulating the real wear-condition, the fabric sound simulator using reciprocating friction was developed. Fabric sounds from 5 specimen were generated by the fabric sound simulator and recorded using high performance microphone. Physical sound parameters of fabrics including level pressure of total sound (LPT), level range (${\Delta}L$), and frequency differences (${\Delta}f$) were calculated. For psychological evaluation, seven adjectives for sound (softness, loudness, sharpness, clearness, roughness, highness, and pleasantness) were used as the semantic differential scale. Fabric sounds by reciprocating friction of nylon taffeta and polyester leno had the highest value of LPT and evaluated as loud, sharp, rough, and unpleasant while polyester ultra suede and silk crepe de chine haying the lower LPT and ${\Delta}f$ were perceived as soft and quite. Comparing with fabric sound by one-way friction, fabric sound by reciprocation friction was perceived as more sharp, loud, and rough. LPT was also the most important factor affecting the sensation of the fabric sound by reciprocating friction.

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Evaluation on the Behavior of Slip Critical Joints with TS High Strength Bolts Subjected to a Size of Bolt Holes (볼트 구멍 크기에 따른 TS 고력볼트 접합부 거동 평가)

  • Lee, Hyeon Ju;Kim, Kang Seok;Nah, Hwan Seon;Lee, Kang Min;Kim, Hyun Chul
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.15 no.2
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    • pp.136-143
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    • 2011
  • The oversized and slotted holes are frequently required for the built-up in construction sites. The foreign provisions specify the reduction of the slip load subjected to the size of bolt holes and the direction of load. There are no domestic building codes and researches on the bolt holes. Therefore, it is necessary to evaluate a change of joint strength quantitatively according to the bolt-hole size and surface condition by means of experiment. This study was conducted to evaluate the slip load subjected to the size of bolt holes, and measured on a change of clamping force of high strength bolts during 168 and 800 hours to analyze the trend of relaxation after fastening bolts. Torque shear bolts defined on KS B 2819 was used for the specimen. Test results exhibit that the variation on the slip load of the others was below 10% by contrast with the standard hole and the highest rate of relaxation was 2.66% of the initial clamping force at the case of the long-slotted hole of 2.5D.

A Study on the Elastic Restoration Characteristics According to Environmental Resistance Condition of Structural Sealing Finishing Materials (구조용 실링마감재의 내환경 조건에 따른 탄성복원 특성 연구)

  • Jang, Pil-Sung;Kang, Dong-Won;Hong, Soon-Gu;Kim, Young-Geun;Kim, Sung-Rae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.1
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    • pp.6-12
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    • 2018
  • Recently, The use of the curtain wall method is increasing in construction. The curtain wall construction is widely applied to the exterior wall of the building for shortening construction period and economical efficiency. However, the replacement of deterioration of the weather resistance and structural behavior of the sealing material connecting the curtain wall method and the glass frame is necessary for introduction of the stable curtain wall method and quality improvement in accordance with KS F 4910 standard. In this study, the elastic restoring force test was performed in the external environment. In this study, the deterioration of the sealant was evaluated for structural sealants. In Korea, studies on the variable displacement behavior of structural sealants are lacked. In this study, the reproduced results in laboratory conditions are compared with the deteriorating conditions exposed to the external environment, and they are reflected in the design of sealing materials in the future. According to the results of the study, it was confirmed that the existing structure sealant meets the quality standard of KS F 4910, but in the conditions performed in this study, adhesion failure of the specimen and cracking of the surface occurred. Especially, in the weather resistance test, it is necessary to evaluate the long-term durability performance of the structural sealant used in the curtain wall method by checking the insoluble state of all the test pieces. Therefore, in order to apply a conventional structural sealant to the site, it is necessary to introduce another durability performance evaluation.

A STUDY ON THE COLOR STABILITY OF RESIN MODIFIED GLASS IONOMERS (레진 강화형 글라스아이오노머의 색 안정성에 관한 연구)

  • Koo, Dae-Hoi;Lee, Yong-Keun;Son, Ho-Hyun;Im, Mi-Kyung
    • Restorative Dentistry and Endodontics
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    • v.22 no.1
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    • pp.358-373
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    • 1997
  • Resin modified glass ionomers were introduced in 1988 to overcome the problems of moisture sensitivity and low early mechanical strength of conventional glass ionomers and to maintain their clinical advantages. The purpose of this study was to evaluate the color stability of four resin modified glass ionomers(Fuji II LC, Vitremer, Dyract and VariGlass), one resin composite material(Z-100), and one conventional glass ionomer(GC Fuji II) under several conditions. These conditions were as follows: 1) before curing, 2) after curing, 3) after polishing, 4) after 500 thermocycling, 5) after 1,000 thermocycling, 6) after 1,500 thermocycling and 7) after 2,000 thermocycling. Three specimens of each material/shade combination were made. Materials were condensed into metal mold with a diameter of 10 mm and a thickness of 2.0 mm, and were pressed between glass plates. The material was polymerized using a light polymerizing unit(Visilux II, 3M, USA). After removal of excess, the surface was polished sequentially on wet sandpapers. A reflection spectrophotometer(Model TC-6FX, Tokyo Denshoku Co., Japan) was used to determine CIELAB coordinates($L^*,a^*$ and $b^*$) of each specimen. CIE standard illumination C was used as the light source. The results were as follows : 1. In comparing different shades of same material, CIELAB color difference(${\Delta}E^*$) value was not significantly different from each other(p>0.05). 2. CIELAB color difference(${\Delta}E^*$) values between after-curing and after-polishing were ranged from 5.53 to 27.08. These values were higher than those of other condition combinations. 3. CIELAB color difference(${\Delta}E^*$) values between before-thermocycling and after-thermocycling were ranged from 1.40 to 7.81. Despite the number of thermocycling increased, CIELAB color difference(${\Delta}E^*$) value was low. 4. The color stability of resin modified glass ionomers was more stable than that of conventional glass ionomers but less stable than that of Z100.

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Experimental Study on the Load Transfer Behavior of Steel Grid Composite Deck Joint (격자형 강합성 바닥판 이음부의 하중전달 거동에 관한 실험적 연구)

  • Shin, Hyun-Seop
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.4
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    • pp.10-21
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    • 2014
  • The joint of prefabricated steel grid composite deck is composed of concrete shear key and high-tension bolts. The flexural and shear strength of the joint were experimentally evaluated only by the bending and push-out test of the joint element. In this study the lateral load transfer behavior of the joint in deck structure system is experimentally evaluated. Several decks connected by the joint are prefabricated and loaded centrically and eccentrically. In the case of centrically loaded specimens, the analysis results show that for the same loading step the rotation angle of the joint with 4 high-tension bolts is larger than the case of the joint with 9 high-tension bolts. Consequently, flexural stiffness of deck and lateral load transfer decrease in the case of specimen with 4 high-tension bolts. But, in the case of eccentrically loaded specimens, it is found that there are no significant differences in the load transfer behavior. The further analysis results about the structural behavior of the joint show that lateral load transfer can be restricted by the load bearing capacity of the joint as well as punching shear strength of the slab. Furthermore, considering that high-tension bolts in the joint didn't reach to the yielding condition until the punching shear failure, increase in the number of high-tension bolts from 4 to 9 has a greater effect on the flexural stiffness of the joint and deck system than the strength of them.

The Deformation and Breaking Load of the Fishing Hook by the Tensile Test (인장시험에 의한 낚시의 변형과 파단하중)

  • KO Kwan-Soh;KIM Yong-Hae
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.14 no.4
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    • pp.269-275
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    • 1981
  • The fishing hooks were tested for breaking and unbending due to plastic deformation of the material. Study of tensile test is not complicated, but has not even worked out fully enough, especially when the test specimen is subjected to plastic deformation. The fishing hook is subjected to unbending stress and the critical section is a Point which is furthest from the line of action of the forces. The dynamic force of fish during jerks depends on their speed of movement and body weight, the kinetic energy corresponding to it and also on the rlastic displacement of the rigging which absorb the energy. Six kinds of hook were tested by the dynamometer under tensile speed 290mm/min (subscript s) and 780mm/min (subscript f). According to their results, the breaking load(B: kg) can be induced with the formula $B={\alpha}wd^2+\beta$ where w(mm) is the distance between the barb base and the lower shank and d(mm) is diameter. The coefficients of the formula for the round hooks(R) and the angular hooks(A) are approximately as follows: $$R:\;\alpha_{s}=0.5,\;\beta_{s}=1.6,\;\alpha_{f}=0.4,\;\beta_{f}=1.4$$ $$A:\;\alpha_{s}=1.1,\;\beta_{s}=2.0,\;\alpha_{f}=1.0,\;\beta_{f}=0.9$$ The ratio of $B_{f}\;to\;B_{s}$ is corresponding to 0.8. The ratio of deformation(X) that is moved distance of barb base at break to the distance(H) between head base and barb base is about $50\%$. Further study should be carried out on the subject of impact and fatigue test under the same condition which is exerted force by the hooked fish.

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