• Title/Summary/Keyword: solvent system

Search Result 1,007, Processing Time 0.032 seconds

A Development on the Non-Photomask Plate Making Technology for Screen Printing (III) (포토마스크가 필요 없는 스크린 제판 기술 개발(III))

  • Kang, Hyo-Jin;Park, Kyoung-Jin;Kim, Sung-Bin;Nam, Su-Yong;Ahn, Byung-Hyun
    • Journal of the Korean Graphic Arts Communication Society
    • /
    • v.26 no.2
    • /
    • pp.55-64
    • /
    • 2008
  • We designed a UV-LED exposure system which has 365nm dominant wavelength due to the environment-friendly and economical maskless screen plate making. And the photoresist applied on the screen stretched was exposed without mask by beam projector with UV-LED light source. Then it was developed by air spray with $1.7\;kgf/cm^2$ of injection pressure. The pencil hardness and solvent resistance of curing photoresist film were excellent as those of conventional photoresist film and the maximum resolution of line image formed by maskless screen plate making. was $100{\mu}m$, so we could establish the possibility of environment-friendly maskless screen plate making technology. But the sharpness of the patterns were ${\pm}40{\mu}m$ since the exposure system for maskless plate making has weak light intensity and the diffusion of light.

  • PDF

Determination of Uranyl Nitrate with Several Ligands by Spectrophotometry

  • Showkat, Ali Md.;Zhang, Yu-Ping;Kim, Min Seok;Kim, Sang-Ho;Choi, Seong-Ho;Lee, Kwang-Pill
    • Analytical Science and Technology
    • /
    • v.17 no.1
    • /
    • pp.23-28
    • /
    • 2004
  • Trace amount of uranyl (II) has been determined spectrophotometrically by measuring the optical density of the light blue yellowish coloured solutions formed by reaction between the metal ion and nicotinohydroxamic acid (NHx) in presence of different secondary ligands in strong isoamyl alcohol alkaline medium. The absorption maxima for both aqueous and extracted systems measured at their respective optimum pH were found to be 360 and 559 nm (DETA), 375 and 358 nm (EDA), 369 and 362 nm (piperidine), 354 and 341 nm (pyridine) and 363 and 336 nm (3 piperidine), 354 and 341 nm (pyridine) and 363 and 336 nm (3 - picoline), respectively at which Beer's law was obeyed. Effect of pH, reagent concentration, order of addition of reagent, time, temperature and solvent media on the absorption spectra have also been studied. Among the different systems studied, the shortest concentration range of uranyl(II) adhering to Beer's Law was 2.4 - 10.5 ppm observed for $UO_2(II)$ - NHx - DETA system in aqueous medium and also for iso amyl alcohol(IAA) extracted $UO_2$ - NHx - pyridine system was 2.4 - 7.8.

Coaxial Nozzle Electrospraying of Polymer Solutions: Use of Dispersant Flow (고분자 용액의 동축 이중노즐 전기분무: 분산제 흐름의 사용)

  • Kim, Min-Young;Lee, Jong-Hwi
    • Polymer(Korea)
    • /
    • v.35 no.3
    • /
    • pp.254-259
    • /
    • 2011
  • In electrospraying of polymer solutions, metal sample collectors are often ineffective in fully removing solvent from sprayed particles and recovering redispersable sprayed particles. Herein, a novel electro spraying system, where sprayed particles were dispersed into laminar flow of dispersant (coagulation liquid), was designed for the nano-encapsulation of protein drugs. Chitosan and polyacrylic acid were used as the encapsulation materials. Aggregation of particles could be prevented by using this new electrospraying system, and unimodal size distribution was observed at an applied voltage between 4~16 kV and a low flow rate. The effects of the applied voltage on mean particle size were not significant on the other hand.

Identification of Differentially Expressed Genes by Exposure of Methylmercury in Neuroblastoma Cell Line Using Suppression Subtractive Hybridization (SSH)

  • Kim, Youn-Jung;Ryu, Jae-Chun
    • Molecular & Cellular Toxicology
    • /
    • v.2 no.1
    • /
    • pp.60-66
    • /
    • 2006
  • Methylmercury (MeHg), one of the heavy metal compounds, can cause severe damage to the central nervous system in humans. Many reports have shown that MeHg is poisonous to human body through contaminated foods and has released into the environment. Despite many studies on the pathogenesis of MeHg-induced central neuropathy, no useful mechanism of toxicity has been established so far. This study, using of suppression subtractive hybridization (SSH) method, was peformed to identify differentially expressed genes by MeHg in SH-SY5Y human neuroblastoma cell line. We prepared to total RNA from SH-SY5Y cells treated with solvent (DMSO) and $6.25\;{\mu}M\;(IC_{50})$ MeHg and performed forward and reverse SSH. Differentially expressed cDNA clones were screened by dot blot, sequenced and confirmed that individual clones indeed represent differentially expressed genes with real time RT-PCR. These sequences were identified by BLAST homology search to known genes or expressed sequence tags (ESTs). Analysis of these sequences may provide an insight into the biological effects of MeHg in the pathogenesis of neurodegenerative disease and a possibility to develop more efficient and exact monitoring system of heavy metals as ubiquitous environmental pollutants.

The Screening Condition for the Immune Regulatory Responsor Using Mouse Fetal Thymic Organ Culture (쥐의 태아 흉선 조직 배양을 이용한 면역조절제 검색방법 확립)

  • Lee, Seung-Gak;Song, Min-Dong;Lee, Kwang-Ho
    • Korean Journal of Pharmacognosy
    • /
    • v.28 no.4
    • /
    • pp.286-292
    • /
    • 1997
  • We studied the screening condition for immune regulatory responsor. We focused on the T-lymphocytes leer this purpose. Mouse fetal thymic organ culture (FTOC) system and flow cytometric analysis were mainly used in this experiment. Even if FTOC is carried out in vivo condition, the pattern of thymic development in the condition of FTOC is similar to that of in vivo condition. In this regard, FTOC system might be very powerful tool to screen the immune regulator, especially concerning on T cells. To establish the optimum condition of FTOC to screen the Immune regulator, we focused on the optimum amount of dose and culture period. The cell number and surface antigens on T cells were also analysed by using hemacytometer and flow cytometer. To monitor the differentiation event, anti-CD3, anti-CD4 and anti-CD8 antibodies were used. Alkoxyglycerol and Phellodendri Cortex were used fur positive and negative control, respectively. Astragalus membranceus was used as test sample. From our analysis, we reached to conclusions that the best dose of extract is $50\;{\mu}g/ml$ of culture medium, the best culture period is for 9 days, and ethanol used as solvent has no toxicity to FTOC.

  • PDF

Development and Analysis of Dry Forming System for Innovation of Papermaking Technology

  • Kim, Jong-Min;Lee, Hak-Lae;Youn, Hye-Jung;Hwang, Min-Gu
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
    • /
    • 2006.06b
    • /
    • pp.181-190
    • /
    • 2006
  • This study was conducted to develop dry forming technology and evaluate the properties of dry formed paper made from Hw-BKP. A dry forming mold (DFM) was developed to observe the phenomena of dry forming and evaluate the properties of formed papers. To upgrade the DFM a dry forming system (DFS) was developed. This DFS was designed to improve the formation of dry formed papers and enhance the productivity of dry forming. Dry forming gave papers with greater bulk and opacity than wet forming. Tensile strength of dry formed paper was greater than that of conventional wet formed handsheet when they were made from the same dry disintegrated fibers. But tensile strength of conventional wet formed handsheet made from beaten fiber was much greater than that of dry formed paper made from dry disintegrated fibers. When solvent dried beaten fibers were used in dry forming, the tensile strength of dry formed papers reached 73.5% of the wet formed handsheets made from beaten fiber. It showed that dry forming has a significant potential in improving strength properties when proper preparation of fibers and appropriate humidification, pressing, and drying processes are employed.

  • PDF

Factors Affecting the Grafting of Aminopropyltriethoxysilane in Swelling Clay Materials (Clay의 Aminopropyltriethoxysilane 그라프트에 영향을 미치는 인자)

  • Shanmugharaj, A.W.;Lee, Kyong-Yop;Ryu, Sung-Hun
    • Elastomers and Composites
    • /
    • v.41 no.4
    • /
    • pp.238-244
    • /
    • 2006
  • Functionalization of montmorillonite clay has been done using 3-aminopropyltriethoxy silane using water as a dispersing medium. Qualitative evidence of the presence or silane attached to the clay surface has been identified using Fourier transform infrared spectroscopy (FT-IR). Increase in silane concentration decreases the adsorbed/intercalated ratio calculated using differential thermogravimetric analysis (DTG). Average d-spacing calculated using X-ray diffraction initially increases with silane concentration and decreases slightly at higher silane concentration. The influence of processing temperature on the silane functionalization of clay has also been investigated and it shows that chemical grafting of silane on the clay surface is observed with increasing processing temperature.

Aliphatic radiofluorination using TBAHCO3 eluate in hydrous organic medium

  • Kwon, Young-Do;Son, Jeongmin;Chun, Joong-Hyun
    • Journal of Radiopharmaceuticals and Molecular Probes
    • /
    • v.4 no.2
    • /
    • pp.51-56
    • /
    • 2018
  • Azeotropic drying process is routinely applied to enhance nucleophilicity of $[^{18}F]$fluoride ion during the nucleophilic production of PET radiotracers; however, the drying process requires usually 15-25 min. Due to the high demand of employing fluorine-18 ($t_{1/2}=109.8min$) in PET radiopharmaceutical production, several research groups have focused on the method development, obviating tedious removal process of the residual target water ($[^{18}O]H_2O$) for $[^{18}F]$fluoride ion complex to be used in radiofluorination. Some development in radiofluorination in a mixed organic solvent system was demonstrated with various aliphatic substrates, but only kryptand as a phase transfer agent was utilized in the reported method. Here, we extend to investigate the development scope of applicability with basic alkyl ammonium salt as a phase transfer agent through the extensive elution efficiency study and radiofluorination outcome for aliphatic radiofluorination.

Production of 3-Ketosteroid-delta-1-Dehydrogenase by a Two-stage Continuous Culture

  • Ryu, D.Y.;Lee, B.K.;Thoma, R.W.
    • Microbiology and Biotechnology Letters
    • /
    • v.2 no.1
    • /
    • pp.29-35
    • /
    • 1974
  • We have studied the applicability of the principles and inherent advantages of the two-stage dontinuous uclture technique to an enzyme process for the purpose of improving and optimizing the productivity of 3-ketosteroid-delta-1-dehydrogenase. By using a two-stage continuous culture system, the growth st ageand enzyme produdtion stage are separated. In each stage an optimal set of toperaing conditions was determined, and this was tested for feasibility for the period of 10 days. During this period, at least 70% of the maximum enzyme productivity could be maintained. The important design parameters studied are: (1) optimal specific growth rate in the first stage which corresponds to the maximal cell productivity, (2) the optimal dilution rate in the second stage which in turn determines the size of second stage fermentor and the mean residence time of cells in the second stage, (3) cell concentration in both stages, add (4) the specific enzyme productivity and enzyme productivity of the second stage. In addition, by using two-stage continuous culture system we have been able to reduce or eliminate the effect of catabolite repression due to high medium concentration and the adverse effect of the solvent used to dissolve the inducer. We have found the balance between the opposing effects of induction and repression in the second stage judging from the observation that the enzyme productivity goes through a maximum.

  • PDF

Technologies for Next-Generation Metal-Ion Batteries Based on Aqueous Electrolytes (수계전해질기반 차세대 금속이온전지 기술)

  • D.O. Shin;J. Choi;S.H. Kang;Y.S. Park;Y.-G. Lee
    • Electronics and Telecommunications Trends
    • /
    • v.39 no.1
    • /
    • pp.83-94
    • /
    • 2024
  • There have been continuous requirements for developing more reliable energy storage systems that could address unsolved problems in conventional lithium-ion batteries (LIBs) and thus be a proper option for large-scale applications like energy storage system (ESS). As a promising solution, aqueous metal-ion batteries (AMIBs) where water is used as a primary electrolyte solvent, have been emerging owing to excellent safety, cost-effectiveness, and eco-friendly feature. Particularly, AMIBs adopting mutivalence metal ions (Ca2+, Mg2+, Zn2+, and Al3+) as mobile charge carriers has been paid much attention because of their abundance on globe and high volumetric capacity. In this research trend review, one of the most popular AMIBs, zinc-ion batteries (ZIBs), will be discussed. Since it is well-known that ZIBs suffer from various (electro) chemical/physical side reactions, we introduce the challenges and recent advances in the study of ZIBs mainly focusing on widening the electrochemical window of aqueous electrolytes as well as improving electrochemical properties of cathode, and anode materials.