• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.8
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• pp.1398-1408
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• 2003

Tensile and LCF(low cycle fatigue) tests were carried out in air at wide temperature range 20$^{\circ}C$-750$^{\circ}C$ and strain rates of 1${\times}$10$\^$-4//s-1${\times}$10$\^$-2/ to ascertain the influence of strain rate on tensile and LCF properties of prior cold worked 316L stainless steel, especially focused on the DSA(dynamic strain aging) regime. Dynamic strain aging induced the change of tensile properties such as strength and ductility in the temperature region 250$^{\circ}C$-600$^{\circ}C$ and this temperature region well coincided with the negative strain rate sensitivity regime. Cyclic stress response at all test conditions was characterized by the initial hardening during a few cycles, followed by gradual softening until final failure. Temperature and strain rate dependence on cyclic softening behavior appears to result from the change of the cyclic plastic deformation mechanism and DSA effect. The DSA regimes between tensile and LCF loading conditions in terms of the negative strain rate sensitivity were well consistent with each other. The drastic reduction in fatigue resistance at elevated temperature was observed, and it was attributed to the effects of oxidation, creep and dynamic strain aging or interactions among them. Especially, in the DSA regime, dynamic strain aging accelerated the reduction of fatigue resistance by enhancing crack initiation and propagation.

• Journal of the Korean Chemical Society
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• v.40 no.1
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• pp.81-86
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• 1996

The physical properties of epoxy molding compound (EMC) according to the change of softening point of epoxy resin have been investigated in order to study the relationship between the properties of o-cresol novolac epoxy resin, which is main component of EMC for semiconductor encapsulation, and EMC. The softening points of used epoxy resin are 65.1 $^{\circ}C$, 72.2 $^{\circ}C$, and 83.0 $^{\circ}C$, respectively. The flexural strength and flexural modulus as mechanical properties were measured, and thermal expansion coefficient, thermal conductivity and glass transition temperature (Tg) as thermal properties, and spiral flow as moldability have been investigated to see the change of physical properties of EMC. The flexural modulus, thermal expansion coefficients in the glass state (${\alpha}_1$), and thermal conductivity of EMC were found to be keep constant value irrespective of the change of softening point, but Tg increased with softening point of epoxy resin, and the spiral flow decreased with that. It can be considered that these phenomena are due to the increase of crosslinking density of EMC according to the increase of softening point. The transition points were found out in the thermal expansion coefficient data in the rubbery state (${\alpha}_2$) and the flexural strength data. These can show the decrease of filler dispersion according to increase of epoxy resin viscosity.

• Journal of the Korean Society for Heat Treatment
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• v.9 no.4
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• pp.229-233
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• 1996

This work has been carried out to reduce the softening of heat affected zone on laser surface alloying. Iron based rapid solidification material with $Cr_{5-10}$, $V_{1-3}$, $Mo_{3-7}$, $W_{2-5}$, $B_{7-8}$, $C_{2-3}$, $Si_{0.5-1}at%$ was alloyed on the surface of SM45C steel. The excellent softening resistance in alloyed and heat affected zone showed, which could be attributed to the formation of stable high temperature precipitates.

• Proceedings of the KWS Conference
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• 2006.05a
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• pp.274-276
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• 2006

Weldability of high Cr ferritic steel for $620^{\circ}C$ grade turbin casing were investigated. The effect of carbon content on the cold and hot cracking susceptibility and HAZ softening was determined. The cast steel with higher carbon content showed higher HAZ hardness because of the dissolution of cabonitrides during welding thermal cycle. Moreover, it showed higher solidification cracking sensitivity because of the little S-ferrite formation in weld metal. Both steels showed HAZ softening at $900^{\circ}C$ peak temperature after PWHT.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.11 no.1
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• pp.33-38
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• 2015

The effects of post weld heat treatment(PWHT) on the mechanical properties of 2.25Cr-1Mo steels were investigated. As the PWHT temperature or holding time increased, the strength of low alloy steels progressively decreased due to softening process. After the conventional PWHT, the strength was larger than the minimum value of materials specification. The Charpy impact energy was hardly affected by the conventional PWHT. The trend of mechanical properties was analyzed in terms of tempering parameter. Most materials replaced from a power plant met the requirements of materials specification except for one heat. Same heat of materials with low impact energy were attributed to the voids formed during casting process.

• Journal of the Korean Society for Precision Engineering
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• v.20 no.2
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• pp.66-75
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• 2003

This paper describes about the estimation method of die lift by wear and plastic deformation in hot forging process. The thermal load and the thermal softening are happened by the high temperature in hot forging process. Tool lift decreases considerably due to the softening of the surface layer of a tool caused by high thermal load and long contact time between tool and billet. Also, tool life is to a large extent limited by wear, heat crack and plastic deformation in hot forging process. Above all, the main factors which affects die accuracy and tool lift are wear and the plastic deformation of a die. The new developed technique for predicting tool life applied to estimate the production quantity for a spindle component and these techniques assist to improve the tool life in hot forging process.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.254-257
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• 2007

In this paper, anisotropic tensile properties of the AZ31B Mg-alloy sheet are obtained with the tensile test at elevated temperatures. Change of microscopic structures and the hardness is inspected after the solution heat treatment process in order to confirm the micro-structural stability of the used sheet metal. Results obtained from tensile tests show that it is very difficult to apply the conventional modeling scheme with the assumption of strain hardening to the forming analysis of the magnesium alloy sheet which shows the strain-softening behavior at the elevated temperature.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2007.11a
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• pp.45-46
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• 2007

One of the major problems faced by the overhead conductor engineer is in the estimation of the loss in strength of conductors caused by long and short term exposures over a period years to elevated temperature. From the standpoint that the life of conductor is influnced by softening of Al wire, the life assessment of conductor was carried out. The aluminum components will be affected most in majority of conductors. The steel core if present will not be affected by temperatures below $225^{\circ}C$. The detailed description will be presented in the text.

• Applied Biological Chemistry
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• v.34 no.4
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• pp.379-385
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• 1991

Morphological changes of starch granules from 12 different varieties of rice were examined by scanning electron microscopy during heating at 2.5% (w/v) concentration. Rice starch granules proceeded through a similar pattern of progressive morphological changes daring heating, regardless of variety. Rice starch granules began to swell radially in the initial stage of gelatinization and then undergo radial contraction and random tangential expansion to form complex structures in the latter stage of gelatinization temperature range. At higher temperatures, starch granules softened and melted into thin flat discs, and then stretched into thin filaments to form three-dimensional networks. These progressive morphological changes were reflected in the changes of swelling power, solubility and amylograph viscosity of starch. During the transition of melting or softening, swelling power, solubility and amylograph viscosity increased rapidly. The time of loss of granular structure of starch depended on gelatinization temperature range. The ratio of amylose to amylopectin was largely responsible fur the rate of melting or softening and the fineness of a three-dimensional filamentous network above the gelatinization temperature range. Therefore, both the gelatinization temperature range and amylose content of starch affect the rate of cooking, and amylose content of starch affects the final texture of cooked starch paste.

• Korean Chemical Engineering Research
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• v.43 no.6
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• pp.745-750
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• 2005

Naphtha cracking bottoms(NCB) oil was reformed by varying the heat treatment temperature, treatment time, and nitrogen flow rate in preparation of precursor pitch for isotropic pitch-based carbon fibers and activated carbon fibers. The reformed pitches were investigated in the yield, softening point, elementary analysis, and molecular weight distribution, and then the precursors reformed were melt spun to certify the optimum reforming conditions. The optimum precursor pitch was prepared when the NCB oil was reformed at $380^{\circ}C$, 3 h and 1.25 vvm $N_2$, and it's the softening point was around $240^{\circ}C$. The reforming resulted in product yield of 21 wt％. The C/H mole ratio of the precursor pitch increased from 1.07 to 1.34, the aromaticity increased from 0.85 to 0.88. The insolubles in benzene and quinoline were 30.0 wt％ and 1.5 wt％, respectively. The spinning temperature was about $50^{\circ}C$ higher than the softening point. The molecular weights of the precursor components were distributed from 250 to 1250, and 80％ of them were in the range of 250 to 700.